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Abstract
Some nitro and nitroso compounds have been determined by direct reduction with Ti(III) chloride without the necessity for degassing the analyte solutions. Methods have been developed for the determination of some binary mixtures by both enthalpimetry and catalytic thermometric titrimetry. The accuracy at the 0.1 mMole level is±1%, and the time taken for a single titration is less than 2 minutes.
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