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Abstract
The voltammetry method offers fast, efficient and simple preparation for the detection of the sample containing rare earth elements (REE). The combination of voltammetry with the experimental design provided more efficient analysis especially the solvent consumption. This study aims to determine the factors that have an optimum effect using the experimental design results on the analysis of Gadolinium (Gd) in acetonitrile by Differential pulse voltammetry. The tertabuthylammonium perchlorate (TBAP) was used as supporting electrolyte. The screening and optimization of the parameter were carried out by Plackett-Burman experimental design and Central Composite Design. The two significant parameters were obtained for the analysis of Gd in acetonitrile by Differential pulse voltammetry (DPV) which are TBAP concentration value 0.1166 M and deposition potential at -0.7929 V.
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