Abstract
The use of differential scanning calorimetry as a means to identify diastereoisomeric salts with a clear eutectic composition that is needed for effective resolution is described and forms the basis of a resolving agent screening process. Automated salt synthesis using an Advanced ChemTech robot is also described. Rapid data analysis is facilitated using an in-house software package, Resolution Companion, which also enables identification of the optimum crystallization conditions following a trial crystallization experiment.
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