Abstract
A reagent for the determination of phosphorus in sea water which contains Mo(VI) plus Mo(V) may be easily prepared by the reduction of Mo(VI) with metallic zinc in acid medium. This reagent is stable in the air for several months, and the development of the molybdenum blue colour is complete in 20 min at about 100°C; the colour is stable for at least a few months. The salt error is approximately 5 per cent with sea water of chlorinity 19 per milli. The interference due to either arsenate or silicate at their concentrations in sea water is negligible.
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