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https://doi.org/10.1016/j.tetasy.2011.07.011
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Cite Journal: Tetrahedron: Asymmetry |  Publication Date: Jun 1, 2011 |
 Citations: 28 |
Affiliation: Fudan University
An efficient and highly enantioselective synthesis of florfenicol 1 was achieved with 37% overall yield starting from commercially available 4-methylthiobenzaldehyde. A key feature of the synthesis is the vanadium-catalyzed asymmetric epoxidation of allylic alcohol 5 with aq tert-butyl hydroperoxide to form (2 S,3 S)-epoxide 6.
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