Abstract
The paper discusses experimental complex, which allowing to carry out high-temperature synthesis of mechanically activated powder reagents by a method of induction heating in vacuum and inert environment. On the basis of this complex conducted in situ synchrotron research of the specific features of phase formation dynamics in mechanically activated 3Ti + Al powder composition. High temperature synthesis carried out under conditions of high volume inflammation by means of inductive heating. The developed complex is adapted to the method of dynamic diffractometry in synchrotron radiation beams to register the kinetics of phase transformations in the solid-phase reaction of the components of the powder mixture.
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