Abstract
With the application of thermogravimetry under quasi-isothermal-isobaric conditions, the reaction course of the calcination of Mn(H2PO4 · H2O to give dimanganese cyclotetraphosphate has been studied. Isothermal calcination was also carried out in an electric furnace at various temperatures (200 min). The reaction products were analyzed by chromatography, IR and NMR spectrocopy, and X-ray diffraction analysis. The compositions of the calcinates were determined through extraction with various inorganic and organic solvents.
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