Abstract

The use of a 0.25M CH 3OH CCl 4(1:1) solvent mixture under ultrasound for the selective deprotection of tert-butyldimethlysilyl ethers of benzyl alcohols is described. This method enables to deprotect tert-butyldimethlysilyl ethers of primary alcohols, whereas tert-butyldimethlysilyl ethers of secondary and tertiary alcohols were stable under the reaction condition.

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