Abstract
The reaction of Mn(O 2CPh) 2 · 2H 2O with the sodium salt of phenyl 2-pyridyl ketone oxime and sodium azide in MeOH gives a tetranuclear cage with a [ Mn 3 II Mn IV ( μ 4 - O ) ( η 1 , μ 2 - N 3 ) ] 7 + core. Magnetic and EPR studies show the cage has an S = 6 ground state.
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