Abstract
A novel organometallic oxide cluster [NBu n 4 ] 2 [{(η 5 -C 5 Me 5 )Rh} 2 Mo 6 O 20 (OMe) 2 ] 1 with multi-valley sites is synthesized by the reaction of [NBu n 4 ] 2 [Mo 2 O 7 ] and {(η 5 -C 5 Me 5 )RhCl(µ-Cl)} 2 ] in a molar ratio of 4:1 in methanol, and displays unique framework transformations upon treatment with organometallic and oxometalate compounds.
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