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https://doi.org/10.1039/b305644a
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Cite Journal: Organic & biomolecular chemistry |  Publication Date: Jan 1, 2003 |
 Citations: 27 |
Affiliation: Health Sciences University of Hokkaido
The coupling reactions of cyclic sulfides with a silylated pyrimidine nucleobase using a hypervalent iodine reagent were investigated. The reaction of silylated uracil with cyclic sulfide 12 using PhI=O gave the desired beta-anomer 14 in moderate yield. 4'-Thiouridine (22) was obtained by deprotection of 14.
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