Abstract
A new mixed-valence copper(I,II) coordination polymer, {[Cu2ICu2III2L4]·4DMF}n1 (HL=N′-(2-methylene pyridine)isonicotinohydrazide), was synthesized by N′-((N-oxide- pyridin-2-yl)methylene)isonicotinohydrazide and cuprous iodide. Complex 1 exhibit a one-dimensional structure built up from mixed valence units of Cu2ICu2IIL4 linked by iodide anions. The coordinated environments of Cu(II) and Cu(I) are distorted octahedron and tetrahedron, respectively.
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