Abstract
1. A new method of synthesizing 3′- and 2′-O-aminoacylnucleosides and aminoeylnucleotides based on the activation of N-substituted amino acids with imidazole was developed. 2. In using this method, it is most convenient to use the o-nitrophenylsulfenyl protection for the amino acid when preparing O-aminoacylnueleosides, and the tert-butyloxycarbonyl group in the case of 5′-nucleotides.
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