Abstract
An anionic weak acceptor, 2-sulfo-1,4-benzoquinone, has provided a new BEDT-TTF (bis(ethylenedithio)tetrathiafulvalene) salt (BEDT-TTF) 2(2-sulfo-1,4-benzoquinone)·H 2O. Single crystal X-ray analysis indicates that the unit cell has two crystallographically independent donor layers, one of which has a β″-type packing motif and the other being disordered. Population analysis and SQUID magnetometry suggests that non-β″-layer has an α‴-type packing motif. The dual-layered salt shows metallic behavior with a metal–insulator transition at 90 K.
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