Abstract
The reaction of tetrakis(2-tert-butyl-4, 5, 6-trimethylphenyl)digermene, which dissociates into germylene molecules in solution, with hexafluorobut-2-yne furnishes the corresponding germacyclopropene 3 by a [1+2] cycloaddition of the germylene to the C≡C triple bond. The X-ray structure analysis of 3 reveals a short C=C double bond length of 132.4(5) pm and an acute C—Ge—C bond angle of 39.93(14)°.
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