Abstract
Abstract A new reactor system was designed a, and constructed for controlled gas-phase preparation of heterogeneous catalysts. The reactor operates at low temperatures (25–200°C) and under inert atmospheres, allowing the use of volatile, air-sensitive precursors like metal carbonyls. Accurate temperature control in the different parts of the reactor system, and effective particle mixing in the fluidized bed, enable controlled preparation. Test results confirmed the usefulness of the reactor in the preparation of Co/SiO2 samples from CD2(CO)8 precursor.
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