Abstract
A dynamic 1 H NMR study of the adamantylideneadamantane (Ad=Ad)/Br 2 system has been undertaken in d 4 -1,2-dichloroethane as a function of excess [Br 2 ] and temperature. Bromine site exchange rate constants (k NMR ) nvere determined by line shape analysis of the spectral region between 6 2.1 and 2.6. The temperature range betnveen the fast and slow exchange limits for a given [Br 2 ] is unusually narrow, being ∼15 o C
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