Abstract
A novel synthetic strategy to silyl-protected terminal alkynyl sulfides via reaction of lithium 2,2,2-tris(trimethylsilyl)ethanedithioate, produced by the reaction of tris(trimethylsilyl)methyllithium with carbon disulfide, and alkyl or benzyl halides has been developed. The scope of the reaction is broad, with a variety of benzylic and aliphatic halides and products were formed in good to excellent yields.
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