Abstract
Partially transferred basic chapter is shown necessary for better understanding the instrumental background and theory of methods of thermal analysis, starting with the determination of heat by classical thermometry and calorimetry. Some notes are devoted to the beginnings of methods of modern thermal analysis. The measurement of thermal diffusivity is analyzed in detail, including figures. In particular, the classification of thermoanalytical methods based on thermal balancing is mentioned. In particular, the DSC and DTA methods are specified, which are shown as quantitative tools, including their theoretical basis. The DTA calibration and the use of defined electrical pulses s well as the effect of thermal inertia are revealed. Practical cases are aimed at practical use in determining phase diagrams, measuring heat capacity and determining impurities. The temperature modulated mode and the specificity of the rapid scanning calorimetry are shown as well as enthalpy changes of selected the oxygen-containing and non-oxygen calibration substances are also presented.
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