Abstract
Abstract The present study, for the first time, describes the application of 3D‐network polymer based on calix[4]resorcinarene, as an efficient heterogeneous and phase transfer catalyst for regioselective azidolysis of epoxides. The surface morphology and the structure of this polymer were investigated by atomic force microscopy (AFM). This method offers several advantages including clean reactions, ease of work-up and reusability of the catalyst.
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