Abstract
The racemic title compound, C12H16O6S, possesses a five-membered ring that adopts an envelope-shaped conformation; the two hydroxy groups occupy quasi-axial positions. Adjacent molecules are linked by O—H⋯O hydrogen bonds to generate a ribbon that runs along the a axis of the orthorhombic unit cell. The crystal studied was an inversion twin.
Highlights
Adjacent molecules are linked by O—H O hydrogen bonds to generate a ribbon that runs along the a axis of the orthorhombic unit cell
The title compound is the product of the cyclization of xylitol in the presence of p-toluenesulfonyl chloride
We report here the single-crystal X-ray structure
Summary
R factor = 0.047; wR factor = 0.110; data-to-parameter ratio = 17.8. The racemic title compound, C12H16O6S, possesses a fivemembered ring that adopts an envelope-shaped conformation; the two hydroxy groups occupy quasi-axial positions. Adjacent molecules are linked by O—H O hydrogen bonds to generate a ribbon that runs along the a axis of the orthorhombic unit cell. The crystal studied was an inversion twin
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