PurposeThis paper aims to determine the optimum parametric settings for yielding superior mechanical properties, namely, ultimate tensile strength (UTS), yield strength (YS) and percentage elongation (EL) of AZ91D/AgNPs/TiO2 hybrid composite fabricated by friction stir processing.Design/methodology/approachAn empirical model has been developed to govern crucial influencing parameters, namely, rotation speed (RS), tool transverse speed (TS), number of passes (NPS) and reinforcement fraction (RF) or weight percentage. Box Behnken design (BBD) with four input parameters and three levels of each parameter was used to design the experimental work, and analysis of variance (ANOVA) was used to check the acceptability of the developed model. Desirability function analysis (DFA) for a multiresponse optimization approach is integrated with response surface methodology (RSM). The individual desirability index (IDI) was calculated for each response, and a composite desirability index (CDI) was obtained. The optimal parametric settings were determined based on maximum CDI values. A confirmation test is also performed to compare the actual and predicted values of responses.FindingsThe relationship between input parameters and output responses (UTS, YS, and EL) was investigated using the Box-Behnken design (BBD). Silver nanoparticles (AgNPs) and nano-sized titanium dioxide (TiO2) enhanced the ultimate tensile strength and yield strength. It was observed that the inclusion of AgNPs led to an increase in ductility, while the increase in the weight fraction of TiO2 resulted in a decrease in ductility.Practical implicationsAZ91D/AgNPs/TiO2 hybrid composite finds enormous applications in biomedical implants, aerospace, sports and aerospace industries, especially where lightweight materials with high strength are critical.Originality/valueIn terms of optimum value through desirability, the experimental trials yield the following results: maximum value of UTS (318.369 MPa), maximum value of YS (200.120 MPa) and EL (7.610) at 1,021 rpm of RS, 70 mm/min of TS, 4 NPS and level 3 of RF.