The transportation industry aims to improve energy efficiency and reduce CO2 emissions, with a focus on reducing vehicle mass. A key method involves advanced lightweight construction techniques using materials like aluminum alloys. Research is concentrated on developing processes to combine different materials into reinforced hybrid components, such as aluminum and titanium. This study focuses on the lateral angular co‐extrusion (LACE) process to produce hybrid hollow profiles of EN AW‐6082 and Ti6Al4V, investigating the impact of the thermomechanical processing during extrusion and heat treatment (HT) on the resulting bond quality and material properties. Various HT routes are tested to see their impact on intermetallic phase formation, longitudinal weld seams, and bonding strength. Mechanical testing evaluates the tensile strength of the joining zone, while nondestructive ultrasonic testing (UT) assesses joining zone integrity and poor bonding detection. Results indicate that HT parameters significantly influence the bond quality and mechanical properties of hybrid profiles. UT data shows a strong correlation with tensile strength and intermetallic phase growth, providing a nondestructive way to evaluate bond quality. This study highlights the potential of LACE processes and optimized HT strategies to improve the performance and reliability of aluminum–titanium hybrid components.
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