In this paper, CuO nanosheets were successfully synthesized by a simple hydrothermal method. The synthesized CuO nanosheets were characterized by powder X-ray diffraction (XRD) scanning electron microscopy (SEM) Fourier Transform Infrared (FTIR) surface area analysis (BET). Several factors influencing the synthesis of material such as concentration of NaOH, hydrothermal temperature and hydrothermal time were studied. Scanning electron microscopy (SEM) investigation reveals that CuO nanosheets have the length of about 500 - 1000 nm. N2 adsorption–desorption isotherm experiment shows that the BET specific surface area of obtained CuO nanosheets is 12.78 m2/g.
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