Solid Loss Research Articles

Impact of debranning on the nutritional, cooking, microstructural characteristics of five Indian small millets

BackgroundMillets are underutilized grains rich in nutrients. This study aimed to investigate the impact of debranning on the nutritional, cooking, and microstructural properties of five Indian millets namely foxtail, little, kodo, barnyard, and proso millet.MethodsThe proximate composition, mineral content, cooking properties (cooking time, solid loss, water uptake, alkali score), Fourier Transform Infra Red (FTIR) spectra, X ray Diffraction (XRD) and microstructural characteristics (Scanning Electron Microscopy) of dehusked and debranned millet samples were examined and analysed.ResultsDebranning resulted in decrease in protein (except for little and barnyard millets), dietary fibre, fat, mineral and phytate content in all the millets while enhanced available carbohydrates and amylose content. The cooking times for dehusked millets were significantly higher while, the solid loss and water uptake during cooking of debranned millets were higher. On debranning, Fourier Transform Infra Red (FTIR) spectra showed changes in the pattern with increase in the intensity of amide II (1363 to 1367 cm−1) and amide III (1215 to 1231 cm−1) bands in the debranned foxtail, little, and kodo millets. The X-ray diffractogram (XRD) showed decrease in relative crystallinity on debranning. Scanning Electron Microscopic (SEM) examination revealed that debranning resulted in the loss of seed coat, aleurone layer and partial loss of germ in the millets.ConclusionDehusked millets are nutritious and should be promoted in Indian diets to improve diet quality, debranned millets are nutritionally inferior, can increase the glycemic load of Indian diets.

Impact of broiler litter and swine liquid manure on nutrient loss in runoff from three consecutive one acre-inch rainfall events

Manure is an important source of plant nutrients and organic matter that can benefit soil health over time. However, indiscriminate use of manure can lead to environmental problems including eutrophication of water bodies caused by nutrient runoff during precipitation events. There is a need to understand the effect of manure source and application rate on nitrogen (N) and phosphorus (P) forms and their losses during runoff events. In this study, we assessed the impact of application rate of broiler litter (BL) and swine liquid manure (SLM) on runoff volume, soil, N, and P losses using a rainfall simulator and three consecutive 2.45 cm rainfall events. Surface Decatur silty clay loam (0–0.06 m) was collected and packed in trays (0.55 x 0.30 × 0.06 m3). Manure was surface-applied to the soil at equivalent P rates ranging from 62 to 249 kg ha−1 for BL and 5–18 kg ha−1 for SLM, respectively. Rainfall events took place 7, 14, and 21 d after manure application. Results indicated that the runoff volume decreased at the highest manure application rate compared to the lowest manure application rate. The total suspended solids (TSS) loss was lower in control compared to BL and SLM treatments. The loss of nitrate-N (NO3-N) dissolved reactive P (DRP) and dissolved organic P (DOP) in runoff water was maximum at the highest application rates for both the BL and SLM with respect to control. Mehlich 3 extractable P (M3P) and water soluble P (WSP) increased with increasing P application rates for both manure types in soils following post rainfall simulation study. An increase in M3P and WSP, along with a decrease in soil P storage capacity following post-rainfall simulation for higher P application rates, indicates caution should be taken for considering the manure application rate to prevent environmental nutrient loss during runoff events.

Postharvest conservation of coquinho-azedo fruits under modified atmosphere

Coquinho-azedo (Butia capitata) fruits are highly valued for their rich content of fiber, minerals, vitamin C, and pro-vitamin A carotenoids. They are consumed in their natural state and used in various products, offering an alternative income source for rural communities. This study aimed to assess the postharvest characteristics of coquinho-azedo fruits stored under different modified atmosphere conditions. The fruits were stored at 13°C using PVC, PP, PET, and a Control group without packaging. Over 17 days, the fruits' physicochemical characteristics were evaluated. Packaging significantly improved senescence scores and reduced the loss of fresh mass, soluble solids, vitamin C, and firmness compared to the Control group. PVC packaging showed superior color and firmness performance, while PP packaging maintained consistent fruit color. PET packaging had the highest levels of soluble solids, vitamin C, and titratable acidity. Utilizing modified atmosphere packaging, particularly PVC, effectively preserved the quality of coquinho-azedo fruits during postharvest storage. These findings contribute to enhancing shelf life and marketability, benefiting both producers and consumers.

Effect of whey protein on the formation, structure and gastrointestinal breakdown of quinoa flour-based composite gels

Whole grain flour has captured increasing attention due to its health benefits. Herein, the quinoa flour-based composite gels were fabricated by heating quinoa flour dispersions containing 0-7 w/w% whey protein isolate (WPI). The thermal properties and gel formation of the dispersions were determined, along with the large deformation and fracture properties, microstructure, and molecular reorganization of the resulting gels. Protein hydrolysis, solid loss, glucose release and microstructural changes were monitored to characterize the gastrointestinal breakdown of the gels. Results showed that quinoa starch was gelatinized at 60-70 °C. Upon heating, quinoa starch was segregated into microparticles of ∼ 3 μm, which aggregated into the starch phase, whereas protein aggregates filled the gap of the starch gel network. A bicontinuous structure was formed with increasing WPI concentration to 7 w/w%. Meanwhile, the storage modulus, gel hardness and fracture stress of the gels increased by 5-8 times. The addition of WPI inhibited gel disintegration during in vitro digestion. However, intestinal glucose release was not delayed because of the phase-separated structure of the gels. With increasing WPI concentration, larger protein aggregates survived after 5 min of intestinal digestion, demonstrating that the enhanced protein network was the main contributor slowing down gel disintegration during in vitro digestion. This work would promote the development of quinoa flour-based products with controlled digestion.

Preserving snake fruit (Salacca zalacca) Voss) quality: Effective control of Peniophora salaccae SKRU002 with fungicides and biological agents

Peniophora salaccae (Russulales, Basidiomycota), a newly identified pathogen of Salacca zalacca, is a major cause of snake fruit rot, resulting in significant agricultural losses. This study evaluates the efficacy of chemical fungicides and biological controls against P. salaccae SKRU002, focusing on disease suppression and fruit quality preservation. Commercial fungicides (propiconazole®, prochloraz®, metalaxyl®, azoxystrobin®, thiram®) and Streptomyces philanthi strains RM-1-138 and RL-1-178 were tested. In vitro, prochloraz® (1000 μL mL−1) fully inhibited P. salaccae growth, outperforming other fungicides. Both S. philanthi strains exhibited strong antifungal activity through volatile and non-volatile compounds. Additionally, autoclaved (at 121 °C for 15 min) and diluted (1/1000) bacterial culture filtrates (BCF) from both strains achieved over 55 % inhibition of P. salaccae. In liquid culture, RM-1-138 (86.80 %) and RL-1-178 (80.86 %) demonstrated greater inhibition than metalaxyl® (9.34 %) and azoxystrobin® (56.84 %), though prochloraz® and propiconazole® remained the most effective (100 %). In vivo, untreated fruits inoculated with P. salaccae showed 100 % disease incidence, significant weight loss (13.28 %), color changes (L∗, a∗, and b∗), and reductions in total soluble solids, total phenolic content, and antioxidant activity, while titratable acidity remained unchanged. Both biological and chemical treatments effectively controlled the pathogen and preserved fruit quality. These findings highlight the potential of S. philanthi strains and fungicides in managing P. salaccae, offering promising strategies for snake fruit cultivation.

Biodegradation of glucose and paracetamol and process optimisation with open mixed microbial cultures in lab-scale sequencing batch reactors

In the context of biological wastewater treatment, this study investigated xenobiotics (man-made chemicals) biodegradation and process optimisation to maximise sustainability. Lab-scale sequencing batch reactors (SBRs) fed with paracetamol (model xenobiotic) and glucose (model biogenic substrate) each as only carbon source (feed concentration 1 g L−1) were run in a range of HRTs (hydraulic retention time, range 0.5–2 d) and SRTs (solids retention time, range 1–28 d). For both substrates, the removal of COD (chemical oxygen demand) increased as the SRT increased, reaching 97 % for glucose and 86 % for paracetamol. At the lowest HRT, the high solid losses with the effluent caused a reduction in the SRT with worse substrate removal. The fraction of the removed COD which was converted into biomass increased for lower SRT and overall the best performance for sustainability (compromise between substrate removal, energy consumption and plant footprint) was observed with HRT 1 d and SRT 11–12 d. The experimental data were modelled using two different approaches: linearisation of a continuous-flow model and non-linear parameter fitting with a periodic steady-state SBR model. The results indicated faster growth rate and slightly higher growth yield for glucose than for paracetamol.

Per- and polyfluoroalkyl substances behavior: Insights from autothermal thermophilic aerobic digestion - Storage nitrification-denitrification reactors

Per- and polyfluoroalkyl substances (PFAS) have emerged as significant environmental contaminants due to their persistence, bioaccumulative properties, and potential adverse impacts on health and ecosystems. Water Resource Recovery Facilities (WRRFs) play a crucial role in the management of PFAS, given their widespread presence in consumer products and subsequent reintroduction into the environment. This study investigated the dynamics of PFAS within the solids stream treatment processing that utilized autothermal thermophilic aerobic digestion (ATAD) followed by a storage nitrification-denitrification reactor (SNDR). PFAS analysis included 60 PFAS analyzed via liquid chromatography-triple quadrupole time-of-flight mass spectrometry of pre-ATAD, post-ATAD, and post-SNDR samples. Complexities such as volatile solids loss during the treatment processes were considered in assessing the effect of ATAD and SNDR on PFAS concentrations. Significant changes were observed in the relative contributions of various PFAS classes throughout the treatment processes due to biotransformation; similar changes were reflected in both 2019 and 2021. The relative contribution of perfluoroalkyl alkyl acids (PFAAs) increased while phosphorus-containing PFAS (e.g., di-substituted polyfluoroalkyl phosphate esters) and fluorotelomer carboxylic acids decreased. Shorter-chain PFAAs were enriched during ATAD, whereas most PFAS increased during SNDR except diPAPs and FTCAs, reflecting treatment conditions' impact. Overall, minor decreases in total PFAS concentrations during ATAD as well as SNDR were observed and hypothesized to be due to enhanced biotransformation to ultra-short PFAS that were not quantified. Even with up to 60 PFAS quantified in the samples, PFAS accounted for <1% of the total fluorine with <2% of that total fluorine being fluoride prompting interest in additional exploration.

Aqueous benzene, toluene, ethylbenzene and xylene (BTEX) removal using core-shell structure activated carbon ball as a permeable reactive barrier material

Permeable reactive barriers (PRBs) are passive and sustainable treatment systems for remediating the diffusion of contaminant plumes in groundwater. Several conventional reactive materials such as activated carbon (AC) have long been used as reactive media for PRBs. AC, which is known for its high adsorption capability and cost-effectiveness, is commonly used to remove multiple pollutants from groundwater. Unfortunately, among the reactive materials, AC can fill in the barrier and pose practical problems, such as a pressure drop, solid losses during handling, and safe disposal of filled sorbents, because of its low particle strength. In this study, AC balls were prepared using zeolite as the core and powdered AC, quartz, and calcite as the shell. AC ball with excellent mechanical strength and high permeability properties in the form of a core–shell layer is a good alternative to conventional reactive materials. The adsorption characteristics of benzene, toluene, ethylbenzene, and p-xylene (BTEX) from solutions using AC balls were investigated. The adsorption equilibrium is in the order of X > E > T > B. The adsorption capacity for B (4.90 mg/g), T (3.37 mg/g), E (1.16 mg/g) and X (0.46 mg/g) were observed at solution pH = 7. To validate the proposed models, batch experiments indicated that the pseudo-2nd-order (11.61 and 10.54 mg/g) and Langmuir models (8.81 and 5.27 mg/g) were the most suitable for describing the kinetics and equilibrium of benzene and toluene, respectively. Regeneration experiments were performed using chemical extraction (methanol) and microwave (MW) heating. When the AC ball was reused six times, the removal efficiency for benzene was maintained above 81 % using methanol, whereas that for benzene was increased to 91 % using MW. A series of experiments revealed that AC balls have considerable reusability. The AC ball can be effectively used as a medium for the removal of benzene in a continuous flow system such as column and sandbox. Based on these results, AC balls are a potential reactive medium for field-scale PRB practical remediation applications.

Use of Integral Forage Palm Flour as an Innovative Ingredient in New Fettuccine-Type Pasta: Thermomechanical and Technological Properties, and Sensory Acceptance.

Dehydrated integral forage palm cladode flour (FPF) presents a promising nutritional and functional approach to enriching fettuccine-type pasta. This study investigated the use of microwave-dehydrated FPF (at 810 W) as a partial wheat flour substitute (0, 5, 10, 15, and 20% w/w) in fresh and dry fettuccine-type pasta. The thermomechanical properties of flour blends and the technological and sensory attributes of the resulting pasta were evaluated. FPF displayed a high protein (15.80%), mineral (15.13%), dietary fiber (67.35%), and total soluble phenolic compound (251 mg EAG·100 g-1) content. While water absorption (~58%) and dough stability remained consistent across formulations, a decrease in maximum torque during heating was observed (p < 0.05). Fettuccine-type pasta containing 10% FPF exhibited an acceptable optimal cooking time, solid loss, weight gain, and textural properties for both fresh and dry pasta. Sensory evaluation revealed acceptability above 63% for pasta with 10% FPF, with a slight preference for the fresh version. Fresh pasta flavored with garlic and extra virgin olive oil (garlic and oil pasta) achieved a sensory acceptance rate of 79.67%. These findings demonstrate the potential of FPF for fettuccine-type pasta production, contributing desirable technological characteristics and achieving acceptable sensory profiles.

Effect of 1-MCP and KMnO4 treatments with different packaging on quality preservation of golden delicious apples

This study explored the impact of three packaging materials (wooden boxes, corrugated fiber boxes, shrink-wrapped boxes) combined with two ethylene scrubbers (1-MCP, KMnO4) on the shelf life of Golden Delicious apples. While previous research has extensively studied the effects of packaging and ethylene inhibitors independently, the novelty of this work lies in its combined evaluation of these factors under ambient storage conditions over an extended period of 160 days. The study specifically addresses a research gap by directly comparing the efficacy of 1-MCP and KMnO4 within different packaging environments, offering insights into their combined influence on key quality parameters such as firmness, juice yield, rot incidence, physiological loss in weight (PLW), acidity, and total soluble solids (TSS). Findings revealed that 1-MCP-treated apples, particularly when shrink-wrapped, experienced minimal reductions in firmness and juice yield, with significantly lower rot incidence and physiological loss in weight (PLW) compared to KMnO4-treated and control apples. Additionally, while acidity and juice content naturally declined over time, and TSS initially increased before decreasing, 1-MCP-treated apples exhibited more stable quality attributes. The study also noted a slower decline in organoleptic quality with 1-MCP and shrink-wrap packaging. The research concludes that the combination of 1-MCP treatment and shrink-wrap packaging most effectively extends the shelf life of Golden Delicious apples, highlighting the importance of integrated approaches to post-harvest management. This study provides a novel framework for improving storage techniques, particularly for ambient conditions where shelf life extension is most challenging.

Elucidating the Effect of Pre-Lithiation of Silicon Dominant Anodes on the Full Cell Performance

Over the last few years, there has been a high interest in increasing the energy density of lithium-ion batteries in order to increase the driving range of battery electric vehicles. On a material level, silicon is a promising anode active material candidate due to its high theoretical capacity of 3579 mAh g-1, which is approximately ten-fold higher than that of the currently used graphite anodes with a theoretical capacity of 372 mAh g-1.[1] However, the main drawbacks of silicon are its intrinsic volume expansion of +300 % upon lithiation.[2] This leads to rupturing of the passivating solid electrolyte interphase (SEI), particle cracking, and loss of electronic contact, limiting the lifetime of batteries with silicon based anodes, thus hindering their transition into application.As a possible solution, Jantke et al. proposed the concept of partial utilization of µm-sized crystalline silicon, where only one-third of the theoretical capacity is used for (de)lithiation. Thereby, a crystalline core remains, and the volume expansion on the particle-level is reduced to approximately + 100%.[3] In addition, it was shown that irreversible losses during the formation and upon cycling can be compensated by pre-lithiation of the anode, which increases the lifetime significantly.[4,5] In this study, we investigated a promising cell chemistry for high-energy applications, containing a Si-dominant anode and a cathode based on a Co-free lithium- and manganese-rich NMC. The here used anode consists of 70 wt% silicon, 20 wt% graphite, 2 wt% conductive C65, and 8 wt% LiPAA-binder. Note that graphite mainly acts as a conductive additive within the operating voltage window, with a negligible contribution to the overall anode capacity. The electrochemical testing was conducted at 25 °C in Swagelok® T-cells containing two glass fiber separators, a 1M LiPF6 in FEC:DEC (2:8, v:v) electrolyte and a lithium metal reference.Without pre-lithiation, these full-cells suffered from rapid capacity fading, reaching the 80 % state-of-health (SOH) criterion after ~100 cycles. As will be discussed, our analysis shows that the primary mode of failure in these cells is the loss of cyclable lithium, evidenced by an increase in the end-of-discharge potential at the anode. It was found that with increasing end-of-discharge potential at the anode, the anode resistance at low state-of-charge rises significantly.Therefore, silicon anodes were lithiated in coin half-cells to 25, 50, and 75 % of the reversible cathode capacity (corresponding to 300, 600, and 900 mAh gSi -1). Then, the anodes were harvested in the lithiated state and assembled in a Swagelok® T-cell with the same cathode, separator, and electrolyte as the non-pre-lithiated reference cells. Pre-lithiation leads to similar reversible charge/discharge capacities, but generates a cyclable lithium reservoir in the anode.Successively increasing the pre-lithiation of the anode increases the lifetime from 100 to 550 cycles. The onset of the above-described aging phenomena is delayed by 150 cycles for every additional 25 % pre-lithiation. Further, the influence of aging and lithium inventory on anode and cathode resistance will be discussed, showing that the increase in anode resistance is mainly a function of (de)lithiation rather than cycle number.Acknowledgments:The authors gratefully acknowledge the funding from the BMBF (Federal Ministry of Education and Research, Germany) in the ExZellTUM III project (grant number 03XP0255). We also kindly thank Wacker Chemie AG and BASF SE for providing the anode and cathode active materials.

Active Packaging Film Developed by Incorporating Starch Aldehyde-Quercetin Conjugate into SPI Matrix.

In this study, soy protein isolate (SPI) films incorporating quercetin-grafted dialdehyde starch (DAS-QR) and DAS/QR, respectively, were developed. The structural, physical, and functional properties of the composite films were determined. The results suggested that DAS-QR and DAS/QR formed hydrogen bonding with the SPI matrix, which improved the structural properties of the films. The light-blocking capacity, thermal stability, hydrophobicity, tensile strength, elongation at break, and antioxidant and antibacterial abilities of SPI films were improved by DAS-QR and DAS/QR. Notably, SPI films incorporated with DAS-QR exhibited better performance than those with DAS/QR in terms of antioxidant (SPI/DAS-QR: 79.8% of DPPH and 62.1% of ABTS scavenging activity; SPI/DAS/QR: 71.4% of DPPH and 56.0% of ABTS scavenging activity) and antibacterial abilities against S. aureus (inhibition rate: 92.7% for SPI/DAS-QR, 83.4% for SPI/DAS/QR). The composite coating film SPI/DAS-QR effectively maintained appearance quality, delayed the loss of weight and total soluble solids, postponed malondialdehyde accumulation, and decreased peroxidase activity and microbial contamination in fresh-cut potatoes. These good performances highlight SPI/DAS-QR as a promising active packaging material for fresh-cut product preservation.

Improvement of mechanical, barrier properties, and water resistance of konjac glucomannan/curdlan film by zein addition and the coating for cherry tomato preservation

The mechanical, barrier properties, and water resistance of packaging materials are crucial for the preservation of fruits and vegetables. In this study, zein was incorporated as a hydrophobic substance into the konjac glucomannan (KGM)/curdlan (KC) system. The KC/zein (KCZ) showed good compatibility with the zein aggregates uniformly distributed in the network formed by an entanglement of KGM and curdlan micelles based on hydrogen bonds. The presence of zein inhibited the extension of the KC entangled structure and enhanced the solid-like behavior. The high content of zein (>6 %) increased zein aggregation and negatively affected the structure and properties of KCZ. The zein addition significantly improved the water vapor permeability, tensile strength, and elongation at break. The hydrophobicity of the KCZ films was significantly enhanced, accompanied by the water contact angle increasing from 81° to 112°, and the moisture content, swelling, and soluble solid loss ratio decreasing apparently. The K56C40Z4 coating exhibited an excellent preservation effect to inhibit the respiration of cherry tomatoes, significantly reducing the water loss and firmness decline and maintaining the appearance, total solid, total acid, and ascorbic acid content. This work provided a strategy to fabricate hydrophobic packaging for the preservation of fruits and vegetables.

Microstructure and mechanical properties of Al2O3 ceramic and copper joints brazed with AgCuInTi brazing alloy

AbstractReliable metallurgical bonding between Al2O3 ceramic and copper was achieved by vacuum brazing using Ag–23Cu–14.5In–3.3Ti (wt.%) alloy. The representative interfacial structure of the joint was Al2O3/Ti3(Cu,Al)3O + γ‐TiO/Ag‐based solid solution + (Cu,Ag)7In3 + Ag–Cu eutectic + Cu‐based solid solution/copper. The interface microstructure evolved with process parameters, including the formation of γ‐TiO and Ti3(Cu,Al)3O, as evidenced by microstructural analysis and etched surface morphology. The relationship between fracture path and shear strength was established by observing the fracture morphology and performing shear strength tests on joints with various process parameters, utilizing the degree of the Ag‐based solid solution loss and the thickness of the reaction layer as evaluative factors. When brazed at 760 or 780°C for 20 min using a 100 µm brazing alloy foil, the brazed joints demonstrated a peak shear strength of 215 ± 25 MPa, and the fracture predominantly occurred in the Al2O3 matrix and Ti3(Cu,Al)3O layer.

Numerical investigation of laser powder bed fusion of glass

Additive manufacturing of glass using laser powder bed fusion has been recently developed, demonstrating its potential to be applied in small scale applications such as flow reactors for the chemical engineering and pharmaceutical manufacturing industries. While previous research demonstrated that complex 3-dimensional shapes can be manufactured, built parts are often brittle, exhibit high porosity and lack transparency. This study employs a transient, heat transfer finite element analysis to shed light on the thermal response of laser—glass powder bed interaction and the impact of processing parameters. Through this understanding, the research seeks to identify practical strategies that can be employed to improve the quality and properties of the built parts. Bulk solid and powder soda lime silica glass properties are used as input in the model, while the laser heat flux and scan strategy, conversion of powder feedstock to bulk solid glass and heat losses from convection and radiation effects are introduced in the model through Fortran coding. The study showed that effective powder consolidation, resulting in well-defined geometrical features, is achieved for temperatures near the glass melting point. Additionally, uniform consolidation depths and widths can be achieved by increasing laser power, elevating substrate temperature and reducing scan speed within certain limits, whilst ensuring hatch spacing is below the corresponding single scan track width for unidirectional adjacent laser trajectories.

Squash pulp as a source of carotenoids and dietary fiber in dried handmade spaghetti

The aim of this study was to evaluate the effect of different levels of dehydrated squash pulp (DSP) (0, 5, 10, 15, and 25 g·100 g-1 of flour) and drying temperatures (50 and 60 °C) on the quality characteristics of spaghetti, i.e., dietary fiber, total carotenoid content, color, cooking quality, texture parameters, and sensory acceptance. The results showed that DSP has a total carotenoid content of 44.42 to 277.90 µg·g-1 and fiber content of 2.45 to 12.40 g·100 g-1. Additionally, the DSP level decreased the cooking time, increased the loss of solids, and generated a decrease in the fracture, hardness, and elasticity of the spaghetti. Furthermore, the increase from 50 to 60 °C in the drying temperature increased the content of carotenoids up to 6.4%, improving the texture properties while not significantly affecting the cooking quality. The spaghetti formulations containing 5 and 10 g·100 g-1 of DSP resulted in improved sensory acceptance. It was possible to develop a new spaghetti type by adding dehydrated squash pulp with better nutritional characteristics such as high dietary fiber content and antioxidants.

Effect of parboiling treatment times on the physicochemical, cooking, textural, and pasting properties and amino acid, phenolic, and sugar profiles of germinated paddy rice from different rice varieties.

In this research, parboiling was carried out at different times (5 and 15min) on germinated paddy rice (GPR) from various basmati and non-basmati varieties. The results showed that as the parboiling time increased from 5 to 15min, E, ash content, total dietary fiber, mineral content, cooking time, and textural properties increased while L*, lipid content, total starch, gruel solid loss, water absorption, oil absorption, foaming capacity, sugar profile, and total phenolic and flavonoid content decreased as compared to GPR. All pasting properties of GPR increased except breakdown as the parboiling time increased from 5 to 15min. Parboiling altered the properties of GPR due to starch gelatinization. Total essential amino acid and gamma-aminobutyric acid decreased as the parboiling time (5 to 15min) increased. The germinated parboiled brown rice could create a highly nutritious alternative to regular brown rice as it offers improved texture and cooking qualities.

(1414) - Access to Transplant Through Novel Approaches to Weight Loss (ACTNOW): Implementation and Early Outcomes with Solid Organ Transplant Candidate-Targeted Weight Loss Clinic

(1414) - Access to Transplant Through Novel Approaches to Weight Loss (ACTNOW): Implementation and Early Outcomes with Solid Organ Transplant Candidate-Targeted Weight Loss Clinic

Determination of impregnation parameters and volatile components in vacuum impregnated apricots

An investigation was conducted to analyse the impact of vacuum impregnation (VI) on aroma profile of intermediate-moisture apricots. cv. Hacihaliloğlu and cv. Kabaaşı apricots were immersed in a variety of solutions, including citric acid and sucrose, as well as plant extracts like rosehip, roselle, and rhubarb. According to the results, solid loss and water gain were observed in all infused samples by VI, while osmotic dehydration occurred in the apricots after immersing in sucrose solution. After all process, a total of 71 volatile compounds were detected in the Hacihaliloglu variety and 66 in the Kabaasi variety. These components are aldehydes, ketones, esters, furan compounds, alcohols, terpenes, isoprenoids, and acids, collected in eight groups. Vacuum impregnation had positive effects on terpenes in both cultivars.

Non-linear frequency response analysis for assessment of the ageing history of lithium ion batteries: A combined simulation and experimental approach

In this work, we present a novel approach for identifying the ageing history of lithium-ion batteries based on experimental nonlinear frequency response analysis (NFRA) measurements. A regression model, trained on simulated NFRA data, is shown to be capable of quantifying degradation modes such as solid electrolyte interphase (SEI) growth, lithium plating, and loss of active material (LAM) with no a-priori knowledge of the cell’s historical duty. Our analysis, combining experimental and simulation approaches, demonstrates NFRA’s potential as a powerful tool for ageing diagnosis by capturing various degradation modes. Changes in NFRA response through life exhibit strong correlations with ageing paths, particularly in the frequency range of 0.2 to 10 Hz. Observations highlight a strong influence of the state of charge on the resultant NFRA response, emphasizing that measurements at a single open circuit voltage (OCV) and harmonics values from a single frequency are insufficient for comprehensive characterization. This analysis underscores the need for correlating NFRA at multiple OCVs and frequencies for detailed ageing assessment. Evaluation on commercially relevant cells enhanced the models’ reliability for industrial applications. This quantitative, data-driven approach using NFRA holds potential to enhance battery management strategies, extend lifespan and improve confidence in second-life applications of batteries. Future work should focus on improving regression analysis robustness, reducing dimensionality, and broadening testing conditions.