ABSTRACT Liquid-solid fluidized bed (LSFB) sorting has been widely used in coarse coal slurry sorting in coal preparation plants in China. In this paper, the vertical distribution of high-ash fine sludge in the LSFB column was studied in depth, and the results showed that in the vertical direction of the column, the gradient of ash change of the + 0.25 mm particles was obviously larger than that of the −0.25 mm particles. For + 0.25 mm particles, the low-density fine coal particles accumulate in the middle and upper parts, while the high-density particles accumulate in the middle and lower parts, and the overflow −0.25 mm particles are basically uniformly distributed in each density class. In the overflow port and the upper part of the column, the ash content of −0.25 mm particle size is obviously higher than that of + 0.25 mm particle size, and the −0.125 mm high ash and fine sludge basically accumulate in the upper part of the LSFB, and eventually enter the overflow to seriously pollute the fine coal. This study is of great significance for the development and application of LSFB sorting machine and the optimization of coarse coal slurry sorting and recovery process.