Small Beam Research Articles

GEO 600 beam splitter thermal compensation system: new design and commissioning

Abstract Gravitational waves have revolutionised the field of astronomy by providing scientists with a new way to observe the universe and gain a better understanding of exotic objects like black holes. Several large-scale laser interferometric gravitational wave detectors (GWDs) have been constructed worldwide, with a focus on achieving the best sensitivity possible. However, in order for a detector to operate at its intended sensitivity, its optics must be free from imperfections such as thermal lensing effects. In the GEO 600 gravitational wave detector, the beam splitter (BS) experiences a significant thermal lensing effect due to the high power build-up in the Power Recycling Cavity (PRC) combined with a very small beam waist. This causes the fundamental mode to be converted into higher order modes (HOMs), subsequently impacting the detector's performance. To address this issue, the GEO 600 detector is equipped with a thermal compensation system (TCS) applied to the BS. This involves projecting a spatially tunable heating pattern through an optical system onto the beam splitter. The main objective of the TCS is to counteract the thermal lens at the BS and restore the detector to its ideal operating condition. This paper presents the new beam splitter TCS in GEO 600, its commissioning, and its effect on strain sensitivity. It also outlines the planned upgrade to further enhance the performance of the TCS.

Design and development of bridge erecting machine with small curve radius and bottom feeding beam

As a key equipment in highway and railway construction, bridge erecting machines directly affect the feasibility, progress, and quality of project implementation. In order to solve the problem that traditional bridge building machines are only suitable for application scenarios with large turning radii and large lifting sites, and have low lifting efficiency, which cannot meet the requirements of urban elevated bridge construction, a small radius bottom feeding beam bridge building machine suitable for urban highway and railway construction is proposed. The feasibility and reliability were verified through force analysis and finite element analysis; Design a secondary turning structure and bridge construction process for the front leg, adjusting the turning angle to around 7°, significantly reducing the turning radius of the bridge building machine; Propose a technology for feeding and lifting beams at the bottom of dual-use bridge decks for highways and railways. By vertically lifting beams and slabs, the lifting space is significantly reduced and the lifting efficiency is improved. Finally, a small radius bottom feeding beam bridge erecting machine was developed and tested and applied. The results show that the small radius bottom feeding beam bridge erecting machine designed in this article reduces the turning radius of traditional bridge erecting machines from over 300 m to about 80 m, making it possible to carry out projects that were originally impossible, and solving the problem of elevated bridge construction in limited urban spaces.

Spatially Fractionated Radiotherapy with Very High Energy Electron Pencil Beam Scanning.


To evaluate spatially fractionated radiation therapy (SFRT) for very-high-energy electrons (VHEEs) delivered with pencil beam scanning. Radiochromic film was irradiated at the CERN Linear Electron Accelerator for Research (CLEAR) using 194 MeV electrons with a step-and-shoot technique, moving films within a water tank. Peak-to-valley dose ratios (PVDRs), depths of convergence (PVDR≤1.1), peak doses, and valley doses assessed SFRT dose distribution quality. A Monte Carlo (MI) model of the pencil beams was developed using TOPAS and applied to a five-beam VHEE SFRT treatment for a canine glioma patient, compared to a clinical 6 MV VMAT plan. The plans were evaluated based on dose-volume histograms, mean dose, and maximum dose to the planning target volume (PTV) and organs at risk (OARs).
Main Results:
Experimental PVDR values were maximized at 15.5 ± 0.1 at 12 mm depth for 5 mm spot spacing. A depth of convergence of 76.5 mm, 70.7 mm, and 56.6 mm was found for 5 mm, 4 mm, and 3 mm beamlet spacings, respectively. MC simulations and experiments showed good agreement, with maximum relative dose differences of 2% in percentage depth dose curves and less than 3% in beam profiles. Simulated PVDR values reached 180 ± 4, potentially achievable with reduced leakage dose. VHEE SFRT plans for the canine glioma patient showed a decrease in mean dose (>16%) to OARs while increasing the PTV mean dose by up to 15%. Lowering beam energy enhanced PTV dose homogeneity and reduced OAR maximum doses. The presented work demonstrates that pencil beam scanning SFRT with VHEEs could treat deep-seated tumors such as head and neck cancer or lung lesions, though small beam size and leakage dose may limit the achievable PVDR.&#xD.

Evaluation of a Novel Femtosecond Laser Ablation System for In Situ Analysis Based on Two-Dimensional Galvanometer Scanners.

Uneven energy distribution of femtosecond lasers presents a significant challenge for single-spot analysis, which often leads to concave ablation craters. This study assesses the performance of a femtosecond laser ablation system for in situ analysis using novel galvanometer scanners. A galvanometer rapidly moved the laser beam focus to create craters with a small beam spot. We first examined the inductively coupled plasma mass spectrometry (ICP-MS) signal sensitivity to laser parameters, establishing a strong linear correlation with the laser energy, repetition rate, scanning ablation area, and galvanometer scanning frequency. Elemental fractionation analysis of NIST SRM 610 suggests minimal bias, with fractionation indices of different elements approaching unity. Subsequently, the elemental concentration of six reference material glasses was measured by fsLA-ICP-MS to evaluate the elemental quantification capabilities of the Galvo-femtosecond laser (Galvo-fsLA). The laser's capability for in situ U-Pb dating was demonstrated by concordant U-Pb ages of five zircon reference materials that are highly consistent with the ID-TIMS ages reported previously. Finally, the reliability of the new Galvo-fsLA for isotope analysis was verified by the accurate determination of radiogenic Hf, Pb isotopes, and stable Cu isotopes, all agreeing well with their reference values within uncertainties. These assessments underscore the significant potential of Galvo-fsLA for enhanced accuracy and precision of single-spot in situ analysis.

Localized Laser Heat Treatment on AISI 1045 Steel Using a LPBF Laser

ABSTRACTLaser heat treatment (LHT) can provide local microstructure modification for metallic materials. This study investigates the viability of LHT on AISI 1045 steel using a laser designed for laser powder bed processing (LPBF) with a very small beam diameter compared to existing literature. Energy density models from the literature are analyzed and adapted to improve consistency across varying laser properties, mainly focusing on spot size and laser–material interaction time. Fifteen different laser parameter schematics are evaluated, comparing hardness versus depth relations as well as laser‐affected zone (LAZ) profiles. Through adapting the energy density model, new laser parameters are calculated and demonstrated to produce a valid localized heat treatment.

A Beam Hopping Scheme Based on Adaptive Beam Radius for LEO Satellites.

Toward the vision of seamless global connectivity in the 6G era, the non-terrestrial network (NTN) in space-air-ground integrated networks (SAGINs) network architecture is one of the highly promising solutions. From the perspective of relay nodes, NTN includes satellite nodes and space-based platform nodes. As a resource management technology in satellite communication, beam-hopping has garnered significant attention from researchers due to its effectiveness in ad-dressing the disparity between offered capacities and uneven terrestrial traffic demands. Recognizing that the larger beams offer broader coverage but the smaller ones provide better an-ti-interference capabilities and higher throughput, this paper introduces an adaptive cluster-ing-based approach. It provides large, medium, and small user beams to target ground users. The proposed algorithm aims to minimize total system latency and enhance system throughput. Sim-ulation results show that employing the proposed algorithm in the baseline model results in a 3.44% increase in system throughput and a 35.5% reduction in system latency. Furthermore, simulation results based on alternative models indicate that while the proposed algorithm may lead to a slight decrease in system throughput, it brings significant improvements in system latency.

A simulation study of MR-guided proton therapy system using iron-yoked superconducting open MRI: a conceptual study.

Radiotherapy platforms integrated with magnetic resonance imaging (MRI) have been significantly successful and widely used in X-ray therapy over the previous decade. MRI provides greater soft-tissue contrast than conventional X-ray techniques, which enables more precise radiotherapy with on-couch adaptive treatment planning and direct tracking of moving tumors. The integration of MRI into a proton beam irradiation system (PBS) is still in the research stage. However, this could be beneficial as proton therapy is more sensitive to anatomical changes and organ motion. In this simulation study, we considered the integration of PBS into the 0.3-T superconducting open MRI system. Our proposed design involves proton beams traversing a hole at the center of the iron yoke, which allows for a reduced fringe field in the irradiation nozzle while maintaining a large proton scan field of the current PBS. The shape of the bipolar MRI magnets was derived to achieve a large MRI field-of-view. To monitor the beam position and size accurately while maintaining a small beam size, the beam monitor installation was redesigned from the current system. The feasibility of this system was then demonstrated by the treatment plan quality, which showed that the magnetic field did not deteriorate the plan quality from that without the magnetic field for both a rectangular target and a prostate case. Although numerous challenges remain before the proposed simulation model can be implemented in a clinical setting, the presented conceptual design could assist in the initial design for the realization of the MR-guided proton therapy.

J-PARC linac and RCS – operational status and upgrade plan to 2 MW

The linac and the 3 GeV rapid-cycling synchrotron (RCS) at the Japan Proton Accelerator Research Complex (J-PARC) were designed to provide 1-MW proton beams to the following facilities. Due to the improvement of the accelerator system, we accelerated a 1-MW beam with a small beam loss. The lack of anode current in the radiofrequency (RF) cavity, rather than beam loss, limits the RCS beam power. Recently, we developed a new acceleration cavity that can accelerate a beam with a low anode current. This new cavity enables us to reduce the requirement for the anode power supply and accelerate a beam of more than 1 MW. We considered how to achieve beam acceleration beyond 1 MW. So far, a beam of up to 1.5 MW is expected to be accelerated after replacing the RF cavity. We also studied to achieve an up to 2 MW beam in J-PARC RCS.

Performance evaluation of surface treatment waste glass as aggregate in asphalt mixture

Surface modification is a crucial strategy for enhancing the pavement performance of waste glass hot mix asphalt (HMA) mixtures. This study conducts a comparative analysis of various surface modification techniques to pinpoint the key factors that influence the interfacial interaction between waste glass and asphalt. To assess the performance of asphalt mixtures containing surface-treated waste glass, the study employed methods such as Energy Dispersive X-ray Spectroscopy (EDS), boiling water tests, and contact angle measurements, which helped to quantify surface morphology and the effectiveness of different treatments. The evaluation also included assessments of water stability, dynamic stability, small beam bending, and anti-skid properties. Findings revealed that applying a silane coupling agent to the waste glass significantly enhanced adhesion with asphalt, resulting in markedly improved pavement performance. The study identified that incorporating surface-treated waste glass at an optimal proportion of 6 % within the asphalt mixture led to a 42.3 % increase in dynamic stability and a 38.6 % enhancement in anti-skid performance compared to standard mixtures. This research offers a comprehensive evaluation framework for surface modification techniques of waste glass, underscoring its potential to considerably improve road performance.

Theory of the interference tunability of second harmonic generation for two-dimensional materials in layered structures.

We theoretically study how the intensity of second harmonic generation (SHG) for a sheet of two-dimensional (2D) material is controlled by an underlying layered structure. By utilizing the transfer matrix method with the inclusion of a nonlinear sheet current to describe the response of the 2D material, an explicit expression for the intensity of upward propagating second harmonic (SH) light is obtained, and the effects of the layered structure can be identified by a structure factor β, defined as the ratio of SH intensity from such a structure to that from a freely suspended 2D material. Our results show that the influence of a layered structure on the SHG intensity arises from interference effects of both the fundamental light and the SH light; the value of the structure factor is 0 ≤ β ≤ 64. Furthermore, when the incident light is pulsed, the interference effects are partially canceled due to the existence of many wave vectors and frequencies, and the cancellation becomes severe for thick films, small beam spots, and short pulses. For a specific structure of 2D material/dielectric film/substrate, the thickness of the dielectric film can effectively tune the value of β in an interval [βmin, βmax], and detailed discussions are performed for the thicknesses when these two extreme values can be obtained. When there is optical loss or the substrate is not perfectly reflective, the extreme value of βmax or βmin cannot reach 64 or 0. A large βmax requires two conditions to be fulfilled: (1) the substrate should be highly reflective, and (2) the refractive indices of the dielectric film at the fundamental and the SH frequencies should differ. Our results indicate how practical substrate structures can be used to achieve high SH signals, and the simple expression we give for the SH enhancement will be useful in characterizing the nonlinear susceptibility of 2D materials.

Repairing weld for directly solidified Ni-based superalloy substrates using directed energy deposition of Inconel 625

Although the maintenance, repair, and operation of gas turbine systems are important issues in enhancing the operation of power units, advanced welding repair processes have limitations in depositing directionally solidified Ni-based superalloy components. To overcome this problem, in this study, a directed energy deposition method was applied to repair directionally solidified components using an Inconel 625 alloy. The rapid cooling rate and small laser beam diameter during directed energy deposition minimized the heat-affected zone and duration in the mushy zone, resulting in crack inhibition at the interface. The first laser scan partially melted the substrate and formed a mixing zone with a chemical composition gradient. By combining the chemical compositional gradient and dislocation accumulation due to repetitive solidification, that is, with the melting cycles of directed energy deposition, the thermal stability decreased, resulting in recrystallization and grain growth in the mixing zone. Consequently, the crack-free continuous interface of the partially repaired components did not induce tensile fracture near the interface. Although the mechanical properties of the IN625 deposit layer were degraded by severe heat treatment of the substrate, the results demonstrated that energy deposition with post-heat treatment is an effective approach in repairing Ni-based superalloy components without cracks and inclusion initiation.

Influences of Different Selective Laser Melting Machines on the Microstructures and Mechanical Properties of Co–Cr–Mo Alloys

Dental prostheses have been fabricated using various selective laser melting (SLM) machines; however, the impact of the type of machine on the microstructure and mechanical properties of Co–Cr–Mo alloys remains unclear. In this study, we prepared samples using two SLM machines (the small M100 and mid-sized M290) with different beam spot sizes (40 and 100 µm, respectively). The microstructures and tensile properties of the heated (1150 °C for 60 min) and as-built samples were evaluated. The grain sizes of the M100 samples were smaller than those of the M290 samples due to the small beam spot size of the M100 machine. Both heated samples exhibited recrystallized equiaxed grains; however, the amount of non-recrystallized grains remaining in the M290 sample exceeded that in the M100 sample. This suggests that the M100 samples recrystallized faster than the M290 samples after heating. The elongation of the M100 samples was higher than that of the M290 samples in the as-built and heated states, owing to the smaller grain size of the M100 samples. A comparison of the M100 and M290 SLM machines indicated that the M100 was suitable for producing dental prostheses owing to its good elongation and rapid recrystallization features, which shorten its post-heat-treatment duration.

Design and performance of a low-emittance electron gun for electron beam probe

An Electron Beam Probe (EBP) is preferable to provide a non-interceptive measurement of the transverse distribution of a dense bunched ion beam. During EBP operation, it was observed that the electron beam spot subjects to expansion when scanned across the ion beam due to the strong space charge field of the ion bunch, leading to significant degradation of spatial resolution. To mitigate this effect, a small electron beam spot is beneficial as demonstrated in previous research. This paper presents design details of a low-emittance, small-spot, and long-work-distance electron gun. Geometry optimization of the gun and focus lens is conducted using a multiobjective genetic algorithm (MOGA) interfaced with space charge simulation codes to maintain normalized thermal emittance within an acceptable increase and achieve a small spot at a long work distance. The emittance is measured using a slit-screen technique, resulting in a norm. rms emittance of 0.046(+-0.005) um*rad under low beam current conditions (50 nA). In high-resolution mode, a beam spot size of 0.6 mm (rms) is achieved at a work distance of 1.2 m with the combination of Einzel lens and solenoid. The gun has been successfully operated as part of EBP experiments for accurate and high-resolution measurement of ion beam width, demonstrating excellent agreement with wire scanner measurements with relative deviation not exceeding 1%.

Seismic performance of RC exterior wide beam–column joints

AbstractIn this paper, seven half‐scale specimens are used to investigate the effects of the beam–column width ratio, concrete strength, and axial load on the seismic performance of wide exterior beam–column joints. The test results show that all the specimens undergo bending damage at the beam end. The concrete damage in the core column is not significant, meeting the seismic requirements of strong column–weak beams and strong joint–weak members. For specimens with small beam widths, the increase in axial load can effectively reduce the damage to the concrete in the outer joint and increase the strength of the specimen. Increasing the beam width and concrete strength reduces the ductility of the specimen while increasing the strength of the specimen. The bonding performance of the longitudinal bars anchored outside the core column is poor, as bond–slip with the concrete is observed during the test. In addition, compared with ACI 318‐19, GB 50011‐2010 is more conservative for calculating the shear strength of exterior wide beam–column joints. Finally, a corresponding finite element model is established by MSC Marc and verified based on the experimental results.

Research on the Preparation and Performance of Biomimetic Warm-Mix Regeneration for Asphalt Mixtures

To determine the formula for biomimetic warm-mix regeneration and fulfill the requirements of a “high waste asphalt mixture content, high quality, and high level” for its usage in reclaimed asphalt pavement (RAP), this paper first determined the suitable preparation process and formula for biomimetic warm-mix regeneration based on orthogonal experiments and a gray correlation analysis. Then, the optimum dosage of the warm-mix regenerant was determined by a uniaxial penetration test, low-temperature splitting test, and freeze–thaw penetration test. The rutting test was conducted to characterize the high-temperature performance of the asphalt mixture. The Immersion Marshall Test and the freeze–thaw splitting test were used to characterize the water stability of the recycled asphalt mixture. The low-temperature small beam test was employed to study the low-temperature performance of the recycled asphalt mixture. The asphalt’s short-term and long-term aging processes were simulated using the rotary thin-film oven test (RTFOT) and the pressure aging test (PAV). The action mechanism of biomimetic warm-mix regeneration was revealed by Fourier-transform infrared spectroscopy (FTIR). Finally, a comprehensive thermal performance test was conducted on the aged asphalt after biomimetic warm-mix regeneration. The results showed that the self-made biomimetic warm-mix regeneration agent exhibited an excellent regenerative effect on RAP and significantly reduced the mixing temperature of the styrene–butadiene–styrene (SBS)-modified asphalt mixture. In addition, the self-made biomimetic warm-mix regeneration agent effectively improved the high- and low-temperature performance of the recycled asphalt mixture, but had no noticeable effect on the water stability. The suggested dosage of the biomimetic warm-mix regeneration agent was 6%, and the mixing temperature was 130 °C. The microscopic chemical analysis revealed that biomimetic warm-mix regeneration restored the performance of aged asphalt by supplementing the light component. The change rules of the chemical functional groups and the comprehensive thermal properties of the recycled mixture showed a good correlation with the change rules of its high- and low-temperature performance.

Role of ion-beam current and energy for nano-scale joining of copper nanowires: Experimental and theoretical study

Copper nanowires (Cu NWs) are popular potential building blocks of various interconnecting components, microscale circuits, and nanoelectronics. Making interconnects at the nanoscale is still an open problem, and various methods have been explored during the past decades. While ion beam joining has been known for quite some time, the beam parameter-dependent processes leading to joining is yet to be understood in detail. A low-energy (5 keV) and broad argon ion beam is unable to induce joining among the Cu NW mesh, at the low ion currents (<400 nA). However, when the ion current was elevated to 1 µA at the same energy, a large-scale joining was observed. We developed a 3D finite volume model for heat transfer and Joule heating-based melting, which successfully explains the ion current-induced joining. When the current is increased to a significantly high level, the network fragments into smaller copper nanoparticles due to the heat produced. On the other hand, at higher argon ion energy (200 keV) a large-scale joining is observed even at small (<400 nA) beam current. A state-of-the-art, Monte Carlo-based TRI3DYN simulation predicted the role of recoils, redeposition, and ion beam mixing in such joining process at high ion energy, which is mostly due to elastic collisional consequences. Such ion current-induced nanowelded copper mesh-coated PET substrate shows good transmission in the optical range of wavelengths and a notable decrease in the sheet resistance is observed.

Observation of atmospheric millimeter-wave discharges at 94 GHz and comparison with other microwave and millimeter-wave frequencies

This report describes an investigation by experimentation to elucidate atmospheric discharge plasma induced using a 50 kW millimeter-wave beam at 94 GHz. Millimeter-wave discharge plasma is useful for an ultraviolet light source, radioactive material detection, chemical decomposition, and beamed energy propulsion (BEP). The gyrotron used in this study is the “UT-94” with a frequency of 94 GHz and an output power of 100 kW, which was developed at the University of Tokyo specifically for BEP research. The 94 GHz frequency is promising for atmospheric energy beaming because of its low atmospheric attenuation, small beam divergence, and existing utilization track records in the atmosphere. This study experimentally investigated the relationship between the incident beam power density and propagation velocity of an ionization-wave front, which is particularly critical to thrust performance. In addition, the plasma structures were also clarified at 94 GHz and compared with other microwave and millimeter-wave frequencies, such as 28 GHz and those higher than 100 GHz. As a result, finer microscopic structure in the H–k plane was observed than those reported in earlier studies. Furthermore, we found a clear relation between structures and propagation velocities in terms of the electric field concentration of the incoming electromagnetic-waves.

Pathways to exploit the multi-spot scanning strategy in electron beam additive manufacturing for control of microstructure and defect density

The goal of this study is to investigate the impact of beam deflection pattern characteristics on microstructure and porosity formation during Powder Bed Fusion Electron Beam Melting (PBF-EB/M) processing of Inconel 718. Specifically, the complex interplay between “beam return time” and “beam jump distance” and their influence on heat accumulation, porosity, and grain formation is explored. The findings reveal that beam jump distance plays a critical role in the transition from columnar to equiaxed solidification, while beam return time is essential for achieving optimal heat accumulation and minimizing porosity. By controlling these two universal beam deflection pattern characteristics, a novel multi-spot scanning strategy was developed, enabling the formation of a fine-grained equiaxed microstructure. It is demonstrated that sufficient heat accumulation is essential for a pore-free bulk material and can be achieved by short beam return times or small beam jump distances. However, for equiaxed grain formation, a large beam jump distance, i.e., a wide distribution of melt pools, is required. Therefore, heat accumulation must be controlled by means of the beam return time if equiaxed grains are aimed for. Additionally, it is found that higher beam currents are beneficial for equiaxed grain formation, but the strongest impact on the columnar to equiaxed transition is attributed to the beam movement pattern itself. This approach offers insights into microstructure control and process reliability, regardless of the specific PBF technique employed, and enables application-specific microstructure design of Inconel 718.

The potential of mixed carbon–helium beams for online treatment verification: a simulation and treatment planning study

Objective. Recently, a new and promising approach for range verification was proposed. This method requires the use of two different ion species. Due to their equal magnetic rigidity, fully ionized carbon and helium ions can be simultaneously accelerated in accelerators like synchrotrons. At sufficiently high treatment energies, helium ions can exit the patient distally, reaching approximately three times the range of carbon ions at an equal energy per nucleon. Therefore, the proposal involves adding a small helium fluence to the carbon ion beam and utilizing helium as an online range probe during radiation therapy. This work aims to develop a software framework for treatment planning and motion verification in range-guided radiation therapy using mixed carbon–helium beams. Approach. The developed framework is based on the open-source treatment planning toolkit matRad. Dose distributions and helium radiographs were simulated using the open-source Monte Carlo package TOPAS. Beam delivery system parameters were obtained from the Heidelberg Ion Therapy Center, and imaging detectors along with reconstruction were facilitated by ProtonVDA. Methods for reconstructing the most likely patient positioning error scenarios and the motion phase of 4DCT are presented for prostate and lung cancer sites. Main results. The developed framework provides the capability to calculate and optimize treatment plans for mixed carbon–helium ion therapy. It can simulate the treatment process and generate helium radiographs for simulated patient geometry, including small beam views. Furthermore, motion reconstruction based on these radiographs seems possible with preliminary validation. Significance. The developed framework can be applied for further experimental work with the promising mixed carbon–helium ion implementation of range-guided radiotherapy. It offers opportunities for adaptation in particle therapy, improving dose accumulation, and enabling patient anatomy reconstruction during radiotherapy.

Geochemical analysis of extremely fine-grained cryptotephra: New developments and recommended practices

Tephrochronology is a powerful tool used to synchronise and date stratigraphic records by accurate and precise geochemical analysis of deposited volcanic glass shards. However, in many distal stratigraphic records (e.g., polar ice cores) tephra shards are often extremely fine-grained (<10 μm). Geochemical characterisation of these shards is challenging because conventional preparation and analytical techniques require highly polished glass areas >5 μm for electron probe microanalysis (EPMA) to ensure high analytical totals and minimise alkali element loss. Recent method developments have put forward alternative approaches to accurately measure major oxides of small shards: a smaller 3 μm diameter beam, overlapping large (20 μm) beam areas onto supporting epoxy resin, and using scanning electron microscopy with energy dispersive spectrometry (SEM-EDS). However, there has been no direct intercomparison of these alternative techniques, which to date have only been tested on a limited range of glass compositions and tephras that are much larger than the extremely fine-grained material found in distal archives. These issues complicate decision making about the best analytical approach to take when faced with small shards. Here, we provide a new workflow protocol for the analysis of <10 μm tephra by determining the accuracy and precision of alternative SEM-EPMA methods. By analysing a variety of glass standards including those prepared to replicate fine-grained ice-core cryptotephras, we show that a 3 μm EPMA beam is suitable for use on all glass compositions provided the beam current is reduced to 1 nA. When glass areas are too small for a 3 μm beam we show that overlapping this small beam onto epoxy resin is preferable to SEM-EDS analysis. We also provide evidence confirming that using 3–0.2 μm polishes for <5 min increases analytical precision of the most abundant major oxides by up to three times, whilst, crucially, preserving the smallest shards in a sample. By directly applying these alternative methods to ice-core cryptotephra, we demonstrate the data are of suitable accuracy and precision to make robust geochemical correlations. This workflow can be applied to future tephrochronology studies, significantly increasing the quality and quantity of data that are obtained from cryptotephra horizons in distal records.