Effect Of Specimen Size Research Articles

Size effect of typical hygrothermal properties test values for building insulation materials

Thermal and moisture properties of building insulation materials are crucial input parameters for analyzing thermal and moisture transfer phenomena in building environments. Accurate determination of these parameters under different conditions is essential for the correct application and assessment of materials and envelope structures. However, numerous factors influence thermal and moisture properties, and while extensive research has been conducted on this topic, the effects of specimen size on typical thermal and moisture property test values remain unclear. To address the issue of unreliable data caused by random specimen sizes in thermal and moisture property testing of building insulation materials, this study selects three materials—expanded polystyrene (EPS), extruded polystyrene (XPS), and foamed cement—as test subjects to explore the size effects on typical thermal and moisture property test values. The results indicate that specimen size significantly affects the test values for typical thermal and moisture properties, with only a few experiments showing negligible size effects for certain materials. For foamed cement, recommended specimen sizes for thermal conductivity testing using the guarded hot plate method and the transient plane source method are 300 × 300 × 30 mm and 50 × 50 × 30 mm, respectively. Except for equilibrium moisture absorption experiments, the weight of other moisture property tests is generally represented by thickness > planar dimensions.

The effect of specimen size on the unconfined compressive strength of cement-stabilized granular mixtures made of natural and recycled aggregates

The cement-stabilization technique is employed on natural and recycled granular materials to improve their mechanical properties. The strength of these materials is assessed by the unconfined compressive strength on laboratory compacted specimens, typically after 7 days of curing. Standards and technical specifications specify different values of specimen height and diameter and different loading modes of testing. This makes the comparison between different materials and with the acceptance limits of technical specifications difficult. The research investigates the effect of specimen size and loading mode on the unconfined compressive strength of both natural and recycled cement-stabilized granular materials. The results revealed significant differences in strength due to variations in specimen size and loading mode. As expected, an increase in specimen slenderness resulted in a decrease in compressive strength. A linear regression model was developed to quantify the effect of the experimental variables on the compressive strength of the two cement-stabilized materials.

Behavior of BFRP-confined geopolymer-based coral aggregate concrete columns under axial compression: Effects of specimen sizes

Behavior of BFRP-confined geopolymer-based coral aggregate concrete columns under axial compression: Effects of specimen sizes

Tensile strength of MgO-graphite based refractories: effect of anisotropy and specimen size

Oxide-graphite refractories represent the new paradigm of materials for extreme environments since 1970´s: materials that resist thanks to "in situ" microstructural changes. The analysis of post-mortem linings necessitates the use of small specimens because main microstructural changes occur within the matrix, exhibiting zonal distributions relatively small compared to maximum aggregate sizes. In this paper the minimized tensile strength of discs (diameter=18 mm, width=8 mm) tested in diametral compression is addressed for commercial materials representative of the typical microstructures. Effects of aggregate and graphite sizes, graphite anisotropy and size of the specimens on the quasi-brittle fracture of these heterogeneous materials are discussed.

Translaminar fracture toughness characterisation for a glass fibre/polyamide 6 laminated composite by a novel approach based on fictitious material concept

This paper proposes a novel approach for the characterisation of the material fracture toughness associated with translaminar tensile failure, consisting in the application of the Fictitious Material Concept (FMC) by using the testing configuration of the Modified Two Parameter Model (MTPM). The main advantage of such an approach is to avoid the use of nonlinear fracture mechanics for material fracture toughness characterisation. The novel approach is applied to compute the translaminar fracture toughness of a unidirectional glass fibre (GF)/polyamide 6 (PA6) laminated composite. Moreover, the experimental campaign carried out is numerically simulated by means of a micromechanical finite element model, and the fracture toughness is computed by employing two different approaches, that is, the novel one and the MTPM. The present study proves, for the first time, that the Fictitious Material Concept can be applied by considering both experimental and numerical structural responses since it provides, in both cases, quite satisfactory accuracy in term of laminated composite fracture toughness. Therefore, the great advantage is that, when a validated numerical model is available, experimental campaigns may be avoided, saving time and money. Moreover, it is proved that the FMC can be used to investigate specimen size effect on fracture toughness.

Specimen size effect on compressive strength of 3D printed concrete containing coarse aggregate with varying water to binder ratios

This study aims to investigate the specimen size effect of compressive strength in 3D printed concrete containing coarse aggregate (3DPCA). Firstly, we compare the specimen size effect of compressive strength in mold-cast concrete (CC) and 3DPCA. Through X-CT scans and image analysis, the underlying mechanisms of this specimen size effect in 3DPCA are revealed. The results indicate that 3DPCA exhibits a less pronounced specimen size effect on compressive strength when loaded along the Z direction compared to CC, due to the presence of interlayer weak zones that mitigate the influence of size variations. Specifically, when the water-binder ratio varies between 0.3 and 0.5, the size coefficient of printed sample is reduced by 0.01–0.07 compared to cast sample. Similarly, variations in coarse aggregate content result in a size coefficient for printed sample that is 0.01–0.05 lower than cast sample. Higher porosity increases the specimen size effect of 3DPCA, but good printing quality can mitigate this influence. A modified Weibull model integrating water-binder ratio and coarse aggregate content was proposed, providing precise predictions of the specimen size effect on 3DPCA's compressive strength, with a correlation coefficient exceeding 93 %.

The use of artificial intelligence to detect parathyroid tissue on ex vivo specimens during thyroidectomy and parathyroidectomy procedures using near-infrared autofluorescence signals

In thyroidectomy and parathyroidectomy procedures, diagnostic dilemmas related to whether an index tissue is of parathyroid or nonparathyroid origin frequently arise. Current options of frozen section and parathyroid aspiration are time-consuming. Parathyroid glands appear brighter than surrounding tissues on near-infrared autofluorescence imaging. The aim of this study was to develop an artificial intelligence model differentiating parathyroid tissue on surgical specimens based on near-infrared autofluorescence. With institutional review board approval, an image library of exvivo specimens obtained in thyroidectomy and parathyroidectomy procedures was created between November 2019 and April 2023 at a single academic center. Exvivo autofluorescence images of surgically removed parathyroid glands, thyroid glands, lymph nodes, and thymic tissue were uploaded into an artificial intelligence platform. Two different models were trained, with the first model using autofluorescence images from all specimens, including thyroid, and the second model excluding thyroid, to prevent the effect of specimen size on the results. Deep-learning models were trained to detect autofluorescence signals specific to parathyroid glands. Randomly chosen 80% of data were used for training, 10% for validation, and 10% for testing. Recall, precision, and area under the curve of models were calculated. Surgical procedures included 377 parathyroidectomies, 239 total thyroidectomies, 97 thyroid lobectomies, and 32 central neck dissections. For the development of the model, 1151 images from a total of 678 procedures were used. The dataset comprised 648 parathyroid, 379 thyroid, 104 lymph node, and 20 thymic tissue images. The overall precision, recall, and area under the curve of the model to detect parathyroid tissue were 96.5%, 96.5%, and 0.985, respectively. False negatives were related to dark and large parathyroid glands. The visual deep-learning model developed to identify parathyroid tissue in exvivo specimens during thyroidectomy and parathyroidectomy demonstrated a high sensitivity and positive predictive value. This suggests potential utility of near-infrared autofluorescence imaging to improve intraoperative efficiency by reducing the need for frozen sections and parathyroid hormone aspirations to confirm parathyroid tissue.

Effects of specimen size and loading rate on the mechanical property of Bentonil-WRK bentonite for engineered barrier system

This study aims to investigate the effects of specimen size and loading rate on the mechanical property of Bentonil-WRK bentonite buffer material for engineered barrier system. Highly instrumented unconfined compressive strength tests were performed on cylindrical specimens prepared using cold isostatic pressing (CIP) technique at varying testing conditions: (a) CIP pressures of 29.43 MPa, 39.24 MPa, and 58.86 MPa, (b) specimen sizes of 30 × 60mm, 40 × 80mm, and 50 × 100mm, and (c) loading rates of 0.5 %/min, 1.0 %/min, and 1.5 %/min. As CIP pressure increases, the unconfined compressive strength (qu), failure strain (εf), and elastic modulus (E) of Bentonil-WRK increase similar to Gyeongju compacted bentonite (KJ-II). Increase in diameter results in a decrease in qu and εf, and increase in E. Minimal effect of loading rate was observed on qu and εf. However, increasing loading rate tends to increase E. In addition, decrease in diameter increases the elastic threshold axial strain (εe,th). Increase in diameter and loading rate slightly increases Poisson's ratio. Prediction models are provided for assessing the effects of specimen diameter on qu and εf. Furthermore, correlation models of qu to ρd and E are proposed for Bentonil-WRK bentonite buffer material.

Effect of specimen size and shape on the compressive performance of high strength engineered cementitious composites at elevated temperatures

This study provides detailed insights into the effect of specimen size on the residual compressive strength of hybrid polyethylene-steel fibre reinforced high strength engineered cementitious composite after exposure to elevated temperatures. A mix design with high residual performance was selected and a total of 120 specimens with different cross-section shape (square and circular), aspect ratio (1 and 2) and sizes (cylinders of 40 mm, 75 mm, 100 mm, 150 mm diameter with height to diameter ratio of 2:1, cubes of 50 mm, 75 mm, 100 mm side and prism of size 75 × 75 × 150 mm) were cast. These specimens were subjected to temperatures ranging from 200 to 800 °C and the residual compressive strength and change in microstructure was then analysed after air cooling. Experimental results indicated that cubic specimens experienced less strength loss compared to prism specimens with the same cross-sectional area and the damage was found to decrease with increase in the volume to surface area ratio of the specimens. Furthermore, no spalling occurred in any of the specimens despite the change in specimen size or cross-section. Unlike previous studies that did not present any clear influence of specimen size, the present work established that the residual strength is dependent on aspect ratio and volume to surface area ratio of the specimen. As a result, these findings are valuable for selecting appropriate specimen size in elevated temperature studies and for the development of suitable guidelines to facilitate meaningful comparisons with the existing data.

Investigating specimen size and shape effects on compressive mechanical behaviors of recycled aggregate concrete using discrete element mesoscale modeling

In comparison to natural aggregate concrete (NAC), recycled aggregate concrete (RAC) typically exhibits a more diverse composition of materials, heightened variability and greater inherent weaknesses. These characteristics may result in varying effects of specimen size and shape on compressive responses. Within this framework, the present study endeavors to comprehensively investigate these influences on RAC's compressive properties and their underlying mechanisms utilizing discrete element simulation technology. At the mesoscale, RAC is depicted by several components, encompassing both new and old aggregates, mortar and interfacial transition zones. Through integrating contacts for each phase, elucidating mesoscale mechanical responses with a parallel bond model and introducing Weibull random fields to delineate variations in phase properties, this study effectively simulates these mechanical responses. Subsequent extensive calculations scrutinize the repercussions of specimen size and shape on the compressive strength, elastic modulus, peak strain and failure modes of RAC across varying water-to-binder ratios. The study concludes that RAC manifests a size effect, albeit less pronounced than in NAC with an equivalent water-to-cement ratio, yet more significant than in mortar. Moreover, owing to end plate constraints, the reduction in RAC's cubic compressive strength is notably less than its prismatic compressive strength. Based on these findings, it is recommended to establish the strength size reduction coefficient and cube-to-cylinder shape coefficient for RAC at 0.86 and 0.72, respectively. Notably, these values diverge significantly from the respective 0.81 and 0.78 coefficients for NAC.

Mechanical mechanism of specimen size effect on impact toughness of Al 6061: Experiment and simulation

Impact toughness has a strong size effect, which restricts the accurate evaluation of material toughness and safety of structural design. However, our understanding of the internal mechanical mechanism that influences the size effect remains incomplete. To fill this gap, this paper adopts the method of combining experiment, theory, and simulation. From the point of view of the dependence of plastic and fracture behavior of material on stress state, the internal mechanical mechanism of the size effect of impact toughness (αk) was studied. Firstly, the Charpy impact tests of different sizes were carried out on Al 6061. αk was divided into cracking initiation toughness (αini) and cracking growth toughness (αgro). The variation of αini and αgro with specimen size was analyzed. Then, through a series of tests, the influence of stress state on the plastic and fracture behavior of Al 6061 was studied. To simulate the whole process of the Charpy impact test, an uncoupled 3D fracture model was proposed. Subsequently, a stress state dependent yield function, modified Voce hardening law, and the proposed fracture model were used to simulate the Charpy impact tests. The predicted results were in good agreement with the tests. Finally, the internal mechanical mechanisms of the size effects of αini and αgro were analyzed. The results show that: (1) The αini and αgro have significant size effects, and there are significant differences between them. (2) The internal mechanical mechanism of the size effect of αini was revealed; that is, the dependence of the plastic behavior of the material on the stress state is the internal root cause of the dependence of αini on the specimen size. (3) The internal mechanical mechanism of the size effect of αgro was revealed; that is, the dependence of the plastic behavior of the material on the stress state and the fracture behavior of the material under ultra-high stress triaxiality is the internal fundamental reason affecting the size effect of αgro. (4) This study reveals the internal complex and intimate relationships between plastic behavior, fracture behavior, toughness behavior, stress state, and the size effect, providing a valuable reference for accurate and comprehensive understanding, evaluation, and selection of metal materials.

A size‐dependent energy‐based strain burst criterion

AbstractThis paper presents a size‐dependent energy‐based strain burst criterion linking strength, elasticity, fracture energies and specimen size effect with stress state due to changes in boundary conditions. It proposes the concept of a ‘Burst Envelope’, a surface in three‐dimensional principal stress space derived based on energy storing and dissipation characteristics of a rock sample, taking into account the size of the specimen and potential localised failure pattern. A scalar burst index is also proposed to quantify the bursting scale. To illustrate and verify its functioning, a numerical modelling framework based on the distinct element method and employing a new cohesive‐frictional contact model is used to perform virtual strain burst experiments under different polyaxial loading‐unloading scenarios, mimicking various underground excavation scenarios. The obtained results are in good agreement with the theoretical prediction of burst occurrence. On that basis, the variation of burst possibility and magnitude are investigated with key factors, including confinement level and the material's elastic, strength and fracture properties. The effect of the specimen's aspect ratio and size on the rock burst potential is elaborated and verified using virtual strain burst experiments, facilitating the linking of the proposed theoretical framework with the evaluation of in‐situ strain bursts in rock masses around underground openings.

Effect of temperature on apparent crack arrest toughness of Eurofer97 measured by a newly developed small specimen test technique

Neutron embrittlement of in-core and out-of-core components made of ferritic steels is one of the key parameters limiting the life of power plants. Owing to the small volume of available irradiation facilities and the limited number of neutron-irradiated specimens, techniques to measure initiation fracture toughness with small specimens have been developed over the years. Although arrest toughness is of equal importance regarding safety assessment, the emphasis has been put on the effect of specimen size on initiation toughness and only a few small specimen test techniques can be found for arrest toughness measurements. The objective of the current work was to develop an experimental technique for measuring the apparent arrest toughness of ferritic steels with miniaturized specimens. Small cantilevers made of the 9Cr Eurofer97 equiaxed ferritic steel were produced with a brittle thin laser-treated layer, which enables crack initiation. The cracks were successfully arrested in the more ductile equiaxed ferritic matrix in a series of tests that were carried out from -123 °C to room temperature with different test configurations. The mechanical tests showed that brittle fracture could be triggered and stopped inside the specimen with a width of 2 mm over a temperature range of more than 100 °C. An apparent arrest toughness was calculated and its temperature dependence was related to the plastic work dissipated by a propagating crack.

Exploring the Effect of Specimen Size on Elastic Properties of Fused-Filament-Fabrication-Printed Polycarbonate and Thermoplastic Polyurethane.

Additive manufacturing (AM) is often used to create designs inspired by topology optimization and biological structures, yielding unique cross-sectional geometries spanning across scales. However, manufacturing defects intrinsic to AM can affect material properties, limiting the applicability of a uniform material model across diverse cross-sections. To examine this phenomenon, this paper explores the influence of specimen size and layer height on the compressive modulus of polycarbonate (PC) and thermoplastic polyurethane (TPU) specimens fabricated using fused filament fabrication (FFF). Micro-computed tomography imaging and compression testing were conducted on the printed samples. The results indicate that while variations in the modulus were statistically significant due to both layer height and size of the specimen in TPU, variations in PC were only statistically significant due to layer height. The highest elastic modulus was observed at a 0.2 mm layer height for both materials across different sizes. These findings offer valuable insights into design components for FFF, emphasizing the importance of considering mechanical property variations due to feature size, especially in TPU. Furthermore, locations with a higher probability of failure are recommended to be printed closer to the print bed, especially for TPU, because of the lower void volume fraction observed near the heated print bed.

Anisotropic Tensile Properties of a 14YWT Nanostructured Ferritic Alloy: On the Role of Cleavage Fracture

Two plates of nanostructured ferritic alloy NFA-1 were processed by ball milling atomized Fe-14Cr-3W-0.4Ti-0.2Y (wt.%) with FeO powders, canning, and hot-extrusion at 850 °C, followed by annealing and multipass cross-rolling at 1000 °C. This produces a severe (001) brittle cleavage texture on planes running parallel to the plate faces. In the first plate (P1), pre-existing microcracks (MCs) formed on the cleavage planes during cross-rolling. The second plate (P2) contained far fewer, if any, MCs. Here, we compare the tensile data for out-of-plane (S) and in-plane (L) tensile axis orientations, at temperatures from −196 °C to 800 °C. We also assess the tensile property differences between P1 and P2, and the effect of specimen size. The L-orientation strength and ductility were excellent; for example, the room temperature (RT) yield stress, σy ≈ 1042 ± 102 MPa, and the total elongation, εt ≈ 12.9 ± 1.5%. In contrast, the S-orientation RT σy ≈ 708 ± 57 MPa, and εt ≤ 0.2%. These differences were due to cleavage on the brittle (001) planes. Cleavage leads to beneficial delamination toughening, but is deleterious to deformation processing and through-wall heat transfer. Therefore, it is important to quantitatively characterize the pronounced NFA-1 strength anisotropy due to severe crystallographic texturing and cleavage fracture.

Analyzing the effects of size and density on the ultimate compressive strength of structural laminated bamboo parallel to the grain

Considering the influence of natural flaws of raw materials and procedures, the size effect is an inherent characteristic that is critical when applying most construction materials. This study focuses primarily on the compressive properties of laminated bamboo, which has become increasingly popular in construction due to its durability and strength. Two specimen sizes (25 × 25 × 100 mm and 50 × 50 × 200 mm) and three densities (0.60, 0.67, and 0.69 g/cm3) were evaluated under uniaxial compression. As a result of this study, the size effect is examined in terms of failure mode, mechanical property, data distribution, and description model, as well as introducing the size effect model with density in an innovative manner. To investigate the effect of specimen size on compressive strength along the grain direction, data analyses were performed. These analyses included failure mechanism analysis, distribution testing, and descriptive model development. According to the results, the compressive strength decreases with increasing dimensions, averaging 62.29 MPa–56.93 MPa, with a decrease rate of 8.60 %, although the failure modes are seldom different. In accordance with the increase in density, the rate of strength reduction also increases, and shows an approximate linear relationship with density. With the change in size, the distribution of the data changes, resulting in a reduction of up to 13.34 % in the standard value. The weakness-link model is better suited for describing data than fracture energy models and fractal theory models, based on which reduction ratios are predicted. By adding density to the size effect model, a more accurate prediction model can be derived between size, density, and compressive strength. As a result of these investigations, we will gain a better understanding of the gap between small clear specimens and large members, as well as those key influences necessary to optimize the use of laminated bamboo in structural applications.

Experimental investigation and numerical modeling of effect of specimen size on microwave-induced fracturing of diorite

The effect of specimen size on microwave-induced fracturing of rocks has not been well understood. In this study, the experimental tests using open-ended microwave and numerical simulations coupling COMSOL Multiphysics and four-dimensional lattice spring model (4D-LSM) were carried out to investigate the evolution process of microwave-induced cracks, and to elucidate the mechanisms responsible for size-dependent microwave-induced fracturing. The experiments show that with the increase of the specimen dimension, the number of microwave-induced cracks is almost constant, and the total crack length first increases and then decreases, while the maximum crack width and maximum crack depth decrease gradually. A comparison of the experimental and numerical temperature characteristics as well as cracking characteristics indicates that the models established in this study are reasonable in the simulation of the rock fracturing behaviours. The numerical results show that the crack initiation time increases logarithmically with the increase of the specimen dimension. For the small-sized specimens, the microwave-induced cracks started from the outer boundary of the specimen and propagated toward to specimen center and into the depth. For the medium-sized and large-sized specimens, the microwave-induced cracks initiated near the outer boundary of the antenna aperture, and then propagated toward to the center of the specimen and the outer boundary of the specimen. The main reason for the size-dependent of fracturing behavior is that the local fracture energy will dramatically decrease when the crack is approaching the specimen boundary.

Effect of Specimen Size on the Dynamic Behavior of Tire-Derived Aggregates (TDA)

Effect of Specimen Size on the Dynamic Behavior of Tire-Derived Aggregates (TDA)

Initiation and growth of fatigue cracks in sheets with U-shaped notches in the first and mixed modes of fracture

Initiation and growth of fatigue cracks in sheets with U-shaped notches in the first and mixed modes of fracture

A new probabilistic control volume scheme to interpret specimen size effect on fatigue life of additively manufactured titanium alloys

The effect of specimen size on the fatigue performance of additively manufactured (AMed) Ti-6Al-4V is investigated in this paper. The fatigue tests of Ti-6Al-4V specimens made by laser powder bed fusion were conducted via ultrasonic axial cycling up to very-high-cycle regime with stress ratio R = –1. The S-N data of five group specimens show an evident size effect, that is, with the increase of specimen size, the fatigue life or fatigue strength decreasing gradually. A new probabilistic control volume scheme is developed to evaluate the fatigue life of large sized specimens by the tested data of small sized specimens. The applicability of the proposed model is validated by the present data and those of our previous investigation. Moreover, a general form of probabilistic control volume model is derived to show the original and present models are the special cases for conventional cast and AMed alloys.