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Published in last 50 years
Chemoselective reduction of β-enamino esters with NaBH(OAc)3promoted by MgI2etherate affords the corresponding β-amino esters in excellent yields in a short time under mild conditions.
An improved method for the preparation of both the enantiopure β-amino acids is presented. The diastereomer benzyl β-amino esters, obtained by stereoselective reduction of β-enamino esters, were separated and hydrogenolyzed to the free enantiopure β-amino acids.