Quartz Optically Stimulated Luminescence Ages Research Articles

Dating the Neanderthal environment: Detailed luminescence chronology of a palaeochannel sediment core at the Palaeolithic site of Lichtenberg in the Lower Saxony, northern Germany

Northern Germany is famous for its numerous Neanderthal (Middle Palaeolithic) archaeological sites and well-preserved palaeoclimate records. Nevertheless, our understanding of how hominins responded to climate fluctuations and adapted to changing environments in this region remains limited because there are only a few reliable, highly-resolved chronological frameworks of long stratigraphic successions. Most of the Middle Palaeolithic sites in this region lack a reliable chronostratigraphy beyond the radiocarbon dating range. In this study, we present a high-resolution optically stimulated luminescence (OSL) chronology derived from a ∼21 m long sediment core (Li-BPa) that was drilled in close proximity to the known Neanderthal site of Lichtenberg. Quartz OSL dating was applied to the upper 6.5 m of the core. Subsequently, the obtained quartz OSL ages were compared with feldspar post-infrared (IR) IRSL (pIRIR) measured at 290 °C (pIRIR290), pulsed IR50 (pre-pIRIR225), and pulsed pIRIR225 ages to select a suitable feldspar signal to date older samples. A comparison of the quartz and feldspar ages indicates that only fading-corrected pulsed IR50 (pre-pIRIR225) and pIRIR225 ages agree well with quartz OSL ages. Finally, the age framework of the sediment sequence was established based on the 11 quartz OSL ages and 23 fading-corrected pulsed IR50 (pre-pIRIR225) and pulsed pIRIR225 ages. The resulting Bacon age-depth model agrees with litho- and biostratigraphic designations, indicating that the whole sequence was deposited between ca. 275 ka and ca. 24 ka, corresponding to the Saalian to Weichselian periods.

Chronology of core sediments from the south coastal Bohai Sea of eastern Asia and its implications for sedimentary history

The Shandong Peninsula along the coastal Bohai Sea in China is a vast alluvial plain formed by the Yellow River. It is an ideal place for investigating the evolution of landform in a river–sea interaction area where chronology is key. However, detailed optically stimulated luminescence (OSL) chronology studies of cores are still limited and have mainly concentrated on the Yellow River Delta, while they are scarce on the south coast of the Bohai Sea. In this study 16 OSL samples were collected from the upper 32 m of core DZK01 (192 m in depth) to establish a chronological framework using quartz OSL. Results indicated that the quartz OSL ages ranged from 217 ± 19 ka to 1.63 ± 0.14 ka, and we believe they were the minimum ages when De > ca. 200 Gy owing to OSL signal saturation. Our dating results reveal two sedimentary hiatuses with age gaps of 71–37 ka and 37–9.5 ka. Holocene sediments are located above a depth of 11.8 m with an onset age of approximately 9.5 ± 0.6 ka. Based on the sedimentary facies and dating results, no transgression sediment has been observed during marine isotopic stage (MIS) 3. This sedimentary sequence pattern is consistent with global sea-level change. We also summarized the extents of three transgressions around the Bohai Sea, and found very different patterns for different part of the coasts, e.g., in the north, the west, and the south. This requires further investigation.

High-resolution luminescence-dated sediment record for the last two glacial-interglacial cycles from Rodderberg, Germany

The Rodderberg Volcanic Complex (RVC) is well-known for the long climate record archived in its crater basin, which lasts for several glacial-interglacial cycles. However, a detailed chronological framework is still lacking. Here, we perform high-resolution luminescence dating on a 72.8 m-long sediment core with the optically stimulated luminescence (OSL) signal from fine-grained (4–11 μm) quartz and three kinds of post-infrared infrared (pIRIR) stimulated luminescence signals from fine-grained polymineral fractions. Together with magnetic susceptibility, grain size and quartz OSL sensitivity measurements, a numerical age framework is built for the upper half of the sediment core. Quartz OSL ages align well with pIRIR ages for the last 45 ka, but they underestimate in relation to pIRIR ages for ages beyond 45 ka. The three pIRIR signals, including the pIRIR signal at 225 °C (pIRIR225), the pulsed pIRIR signal at 150 °C (pulsed pIRIR150) and the multi-elevated-temperature pIRIR at 250 °C (MET-pIRIR250), yield consistent ages up to ca. 250 ka at a sediment depth of 37.5 m. Below that depth, dating limits of the protocols are reached. Nevertheless, our results indicate that sediments below 37.5 m predate Marine Isotope Stage (MIS) 7. Altogether, obtained ages reveal continuous dust accumulation during MIS 7 and MIS 6. One erosional event happened at the end of the Eemian (MIS 5e), which eroded the Eemian soil. The sedimentation rate during the Weichselian glacial period is tenfold lower compared to the sedimentation rate observed during MIS 7–6. This low sedimentation rate likely arises from the cessation of slope wash effects and the occurrence of various wind erosional events alternating with dust deposition as the basin is filled by dust. A notably high sedimentation rate is observed at the transition from MIS 6 to the Eemian, marked by the deposition of a 7 m-thick loess layer between 135 and 129 (±5) ka. This high sedimentation rate could be attributed to intensified slope wash and solifluction processes resulting from the thawing of permafrost at the time of deglaciation. Alternatively, it might be a signature of Heinrich event 11, during which strong winds brought large amounts of dust into the basin within a short time.

Underestimated single-aliquot quartz OSL ages of Late-Pleistocene sediments due to the dominance of medium component

Optically stimulated luminescence (OSL) dating technique has increasingly been employed to establish chronologies for coastal deposits since the Late Pleistocene. However, the commonly used single-aliquot quartz OSL dating method may yield inaccurate ages due to factors such as partial bleaching, luminescence characteristics, and the age limit of quartz. In this study, taking the Yangtze River Delta (YRD) as an example, single-aliquot and single-grain OSL dating using varying grain-sized quartz and K-feldspar were cross-checked to establish appropriate dating method for Late-Pleistocene sediments in coastal areas. The quartz OSL signals of the upper 24 m Holocene sediments were dominated by the fast component, and the ages obtained through OSL and AMS 14C ages agree. Conversely, the lower 24–91 m section, representing the last glacial-interglacial cycle, reveals a notable underestimation of quartz OSL ages, with a maximum underestimation of 250%, attributed to the influence of signal components. For samples within the dating limit of quartz (less than 70 ka), the single-grain method effectively mitigates the issue associated with the signal component. Single-grain K-feldspar technique proves valuable for accurately determining the age of those older sediments exceeding 70 ka. Through cross-checking between different OSL dating methods, sediments initially attributed to marine isotope stage (MIS) 3 (36–60 ka) are re-identified as deposited during MIS 5 (80–130 ka). This study highlights the necessity of assessing the variability in luminescence characteristics before applying a single OSL dating protocol to all samples from different sedimentary facies within a single core.

Combined optically stimulated luminescence and radiocarbon dating of aeolian dunes in Arctic Sweden

AbstractMultiple parabolic sand dune fields formed in Arctic Sweden after the last deglaciation, facilitated by an abundance of loose glaciofluvial sediment, limited vegetation cover and strong winds. Following initial stabilisation, these dunes underwent repeated reworking after fire events, as evidenced by the presence of buried soils, charcoal layers and redeposited sands in the dune stratigraphy. These reworking events may be driven by wider climate forcing; however, to date, no chronological framework exists for this activity in Sweden. As such, here, we apply quartz optically stimulated luminescence (OSL) dating of Arctic Swedish sand dunes using two dunes at the sites of Vastakielinen and Jorggástat. Resultant double‐SAR (single aliquot regenerative dose) quartz OSL ages are in good agreement with independent ages provided by 14C dating of charcoal fragments recovered from charcoal layers within the dunes, and we conclude that the chosen protocol is generally well suited for dating aeolian reworking of dune sediments in Arctic Sweden. While feldspar contamination limits precise age assignment for initial dune movement, our results nonetheless suggest repeated and long‐lasting aeolian activity in Arctic Sweden throughout the Holocene and, although there are differences in detail, further suggest some general trends in terms of dune stability and reworking over Arctic Fennoscandia.

Chronology and paleoclimatic context of hominin occupations in the Fenhe River Basin of northern China during the middle to Late Pleistocene

The relationship between climate change and hominin evolution over the Pleistocene in East Asia is still poorly understood, in particular due to the limited number of archaeological finds and fossils with reliable chronologies. Paleolithic sites preserved in loess-paleosol sequences in eastern Chinese Loess Plateau provide prospective evidence for understanding hominin evolution and dispersion across the Middle to Late Pleistocene in northern China. The Fenhe River Basin has been known as a key area for paleolithic sites and fossil hominins. Here, quartz Optically stimulated luminescence (OSL) and K-feldspar post-infrared infrared stimulated luminescence (pIRIR) dating was employed on 61 samples from 13 paleolithic sites in the Fenhe River Basin. The reliability of the ages are checked by analysis of luminescence characteristics and comparison between quartz OSL and K-feldspar pIRIR ages. Paleoclimatic records were established using alternating loess-paleosol sequences, and multi-proxy indices of grain size, magnetic susceptibility, CaCO3 and color from the dated sites. These results provide the reliable chronology for hominin presence in the Fenhe River Basin spanning the past three glacial-interglacial cycles. Our results show that this region experienced predominantly dusty, dry and cold conditions during glacials and comparatively moist and warm interglacial conditions, that are sensitive to variations in East Asian Summer and Winter Monsoon (EASM and EAWM respectively) intensities over glacial-interglacial timescales. The Fenhe River Basin is a key geographic refuge for hominins during glacial-interglacial climatic changes in northern China. It was occupied over glacial and interglacial periods spanning at least the last 370 ky, and the evidence for hominin presence is especially clear from ∼250 to 60 ka and since ∼35 ka. The frequency of hominin activity, as indicated by the number of archaeological sites and density of stone artifacts, increased during warm and humid periods of MIS 7 and MIS 5, in contrast to the cold, windy, and dry period of MIS 6. Site numbers increased in MIS 3 and the Last Glacial Maximum, in association with microblade technology. The dating results indicate that hominins with ‘modern’ features may have occurred in the Fenhe River Basin ∼140 ka ago, however, the exact timing of modern human occupation in the region needs a more combined approach consisting of morphological, ancient DNA and geochronological studies.

Direct dating of a major rockfall at the Ba'ja Neolithic site (Jordan) using rock surface luminescence

In this study, we use luminescence rock surface dating to provide burial ages for buried surfaces of a large boulder now positioned on top of the ruins of the Neolithic Ba'ja village in Southern Jordan. Luminescence depth profiles for quartz optically stimulated luminescence (OSL), and feldspar infrared stimulated luminescence (IR50) signals indicate that the boulder experienced a complex transport history of at least two exposure and two burial events before final emplacement. By comparing the fading-corrected feldspar IR luminescence burial ages derived from these rock surfaces with quartz OSL ages derived from sediment infill from the archaeological structures underneath the boulder, it is concluded that there was a rockfall event around 7–8 ka ago, possibly as the result of an earthquake. Whatever the nature of this event, it resulted in the first recorded movement of the boulder, when the rock was presumably dislodged on the hill slope but did not travel all the way to the settlement at the foot of the slope. About 3–4 ka ago, after the village had been abandoned and the rooms filled with rubble, further movement occurred, possibly initiated by an earthquake. This final transport event moved the boulder further downslope, embedding it in the cultural layers of the derelict settlement on top of the partially collapsed settlement walls.

Mega-lake formation in the eastern Hetao Basin, China, during marine isotope stages 7 and 5: A comparison of quartz and feldspar luminescence dating

Paleo-lacustrine sediments indicate that a mega-lake developed in the Hetao Basin (HTB), suggesting dramatic changes in the geomorphology and surface process of the Yellow River and surrounding regions. However, the formation time of the mega Hetao paleo-lake (HTPL) in the HTB remains unclear. In this study, a set of 7.6-m-thick lacustrine sediments in the middle of the HTB is dated by both quartz optically stimulated luminescence (OSL) and K-feldspar (KF) post-infrared infrared stimulated luminescence (p-IR IRSL, pIRIR). The results are as follows. 1) The quartz OSL ages do not increase with depth as the KF pIRIR ages displayed but are saturated at ca. 80–100 ka with the consequence of age underestimation. The influence of signal saturation may occur below 96 Gy (ca. 32 ka) in this region. Thus, the KF pIRIR ages are chosen for geomorphological evolution reconstruction. 2) These ages suggest the level of the HTPL exceeded 1033 m asl twice—at the early stages of MIS 7 (∼255–245 ka) and MIS 5 (∼130–120 ka). However, the exact scale of the HTPL and its relationship with the Jilantai paleo-lake is unclear. 3) This chronology suggests strong linkage between periodic formation of the HTPL and glacial-scale climatic change. We therefore propose an alternative hypothesis to interpret these processes: the Hobq dunefield expanded eastward to dam the narrow Jin-Shaan Gorge during the glacial periods when the flow of the Yellow River was weak. Then, in the beginning of the interglacial periods, the basin was filled by abruptly resumed runoff in response to increased glacial meltwater and precipitation on the northeastern Tibetan Plateau. Once the lake spilt out, the loose dune dam was quickly breached.

Holocene sedimentary of the Pearl River Delta in South China: OSL and radiocarbon dating of cores from Zhuhai

Deltaic sediments provide a window for investigating delta development processes and the effects of human activities. Despite the fact that numerous studies have been conducted in the Pearl River Delta (PRD), the chronological data are still very limited, which hinder the detailed interpretation of the sedimentary records. The current study aims to establish high-resolution chronology on two cores from Zhuhai using quartz optically stimulated luminescence (OSL) and radiocarbon (14C) dating and, further, to reconstruct the Holocene sedimentary history of the PRD. Core P1-1 has a depth of 79 m and core P3-2 a depth of 60 m. Thirteen quartz OSL samples from P1-1 produced ages between 10.4 and 0.16 ka. Eight OSL and eight 14C ages from P3-2 span from 10.7 to 0.3 ka. The OSL and 14C dates show a good agreement above the depth of 26 m (1.4–0.3 ka), but with discrepancies at depths of 26–54 m. 14C ages (10.7–8.1 ka) are generally older (up to c. 2 ka) than quartz OSL ages, and the discrepancy decreases with depth. The age model shows three phases of the sedimentation process: (1) rapid accumulation rates of 7.48 (P1-1) and 7.52 (P3-2) m/ka between c. 10.7 and 7.5 ka in response to high sea level, (2) followed by a significantly reduced rate of 2.24 m/ka (P1-1) and a depositional hiatus (P3-2) from 7.5 to 2.5 ka as a result of reduced sediment supply and strong scouring by tidal processes, and (3) high sedimentation rates of 8.86 (P1-1) and 9.07 (P3-2) m/ka since 2.5 ka associated with intensive human activities and weakening tidal hydrodynamics. This sedimentary pattern is also evident in many other Asian deltas.

Radiocarbon and OSL dating on cores from the Chaoshan delta in the coastal South China Sea

Accurate chronology plays a crucial role in reconstructing delta evolution. Radiocarbon (14C) and optically stimulated luminescence (OSL) dating are widely used to establish a stratigraphic chronology of the late Quaternary sediments. The Chaoshan plain is located on the southern coast of China and borders the South China Sea. The thickness of Quaternary sediments in this area extends to a depth of 140 m and is considered a valuable archive for studying the evolution of the delta in response to climate and sea-level changes. However, reliable chronological data are still very limited. In this paper, eighteen accelerator mass spectrometry (AMS) 14C and thirteen quartz OSL ages were obtained from two cores from the Rongjiang plain, the middle part of the Chaoshan plain: ZK001 (90.85 m in depth) and ZK002 (100 m in depth). The present study aims to provide a reliable chronology of the Chaoshan plain based on OSL and 14C dating methods and examine the upper limit of the 14C dating on plant remains. Our results show that (1) OSL ages of cores ZK001 and ZK002 range from 56 to 1.7 ka and from 177 to 15 ka, respectively; (2) 14C ages of core ZK002 range from 8.8 to 41 cal ka BP, showing that all 14C ages below ca. 30 m depth are younger than OSL ages and that the upper limit of plant remains is around 35 cal ka BP. OSL ages are consistent with stratigraphic order within uncertainties. The oldest OSL age obtained from core ZK002 is 177 ± 20 ka at a depth of 93 m, and is considered a minimum age. This indicates that the Quaternary deposition in the Rongjiang plain can trace back to at least the marine isotope stage (MIS) 6 during sea-level lowstand, during which the plain is mainly influenced by the fluvial process. The comparison between 14C and OSL ages in the Chaoshan plain suggests that 14C ages older than 35 cal ka BP need to be re-evaluated. However, the OSL dating method proves reliable for establishing a comprehensive chronological framework for the late Quaternary sediments in this area.

Testing the accuracy of OSL and pIR IRSL dating of young geoarchaeological sediments in coastal Peru

Luminescence dating of late Quaternary sediments in Peru is challenging, especially on the Peruvian coast. Earlier studies have shown that quartz grains often exhibit a thermally unstable, medium signal that caused the underestimation of Optically Stimulated Luminescence (OSL) ages. InfraRed Stimulated Luminescence (IRSL) dating has shown to produce more reliable ages, depending, amongst other factors, on the age model (Central or Minimum Age Model), and the IRSL signal. IRSL dating of geoarchaeological sediments has, however, hardly been carried out, let along validated, against an independent age dataset. This dating approach is, nonetheless, the only promising way to date the geological substrate in which many of Peru's archaeological sites are buried. Peru contains some of the oldest and most important archaeological heritage sites, yet not much is known of the environmental context in which many of its early civilizations prospered. A better understanding of which luminescence method works best could therefore help in a better understanding of the geological-stratigraphical context of many of Peru's sites. To investigate this matter more fully, we compared the luminescence dating results of seven sediment samples from the top layer of the Lima alluvial fan and from geoarchaeological layers of the Maranga Complex (San Miguel, Lima), with an independent dataset of sixteen 14 C ages. Our results showed that the quartz OSL ages always underestimated the expected ages due to a signal dominated by medium and slow components, and that the post-IR IRSL 225 (pIR IRSL 225 ) and IRSL 50 ages of K-feldspars, on basis of the Central Age Model (CAM), always overestimated the expected ages. The Minimum Age Model (MAM) on the other hand, correctly predicted the expected ages for the early Holocene, Lima alluvial fan sediments using the pIR IRSL 225 signal of K-feldspars, and the late Holocene, geoarchaeological ages using the IRSL 50 signal.

Rock surface and sand-sized sediment quartz dating using optically stimulated luminescence of a Middle-to-Upper Palaeolithic sequence at the Bordes-Fitte rock shelter (Les Roches d’Abilly, Central France)

In this study, we use optically stimulated luminescence (OSL) to establish a robust absolute chronology for the lower part of the stratigraphic record at “Les Roches d’Abilly”, an important Palaeolithic site in Central France. There, lithic assemblages recording the Middle-to-Upper Palaeolithic transition and the behaviour of Neanderthal and Anatomically Modern Human populations are preserved. At the Bordes-Fitte rock shelter, part of “Les Roches d’Abilly”, the archaeo-stratigraphic record has been sealed and preserved by the collapse of the shelter roof and this site has provided important data on the timing of human occupations and Middle-to-Upper Palaeolithic transition in this region. Here, we first obtain burial ages using standard multi-grain quartz techniques on sand-sized sediment grains and then investigate the information available in blue-stimulated luminescence-depth profiles into the surfaces of four quartz-rich cobbles found in the sedimentary record below the various collapses of the shelter roof. These profiles show qualitative evidence for past daylight exposure and a single burial event, allowing the data to be analysed quantitatively using a multiple-event mathematical model. Based on the results of this modelling, it is concluded that at least part of the cobble surfaces were well-bleached at burial and thus that estimated rock surface burial ages are unlikely to be significantly affected by incomplete bleaching. However, it appears that not all cobble surfaces were well-bleached, demonstrating the importance of only using surface doses derived from those cobble layers that can be shown to have been well-bleached at burial. The rock-surface burial ages of the most recent burial event are consistent with the quartz OSL ages derived from the surrounding sediments, giving burial ages of ∼ 50 ka. The OSL ages are consistent with previously published 14 C age control, although a single 14 C age (uncalibrated age of 41 , 900 ± 1 , 500 yr BP) of a lower unit may underestimate the OSL ages. This study provides a reliable absolute OSL chronology for the Bordes-Fitte rock shelter constraining the Middle-to-Upper Palaeolithic transition to occur between 44±2 ka and 48±3 ka ago (at the 68% confidence level).

Luminescence characteristics of muddy sediments in the turbidity maximum zone of the Yangtze River mouth and implications for the depositional mechanisms

Muddy sediments are the most prominent constituents of sedimentary successions in tide-dominated river deltas and have highly complex depositional mechanisms. In this study, we performed fine-grained (4–11 μm) quartz optically stimulated luminescence (OSL) dating on two sediment cores collected at a shipwreck site in the turbidity maximum zone (TMZ) of the modern Yangtze River mouth, China, which were compared with previously published dating results including 45–63 um quartz OSL dating, radionuclide dating, porcelain artifacts recovered from the wreck, macro-plastics, and the morphological history recorded in marine charts. We investigate the luminescence characteristics of muddy sediments trapped in the TMZ and discuss the implications of OSL ages in understanding depositional mechanisms in tide-dominated river mouths. The results indicate that most OSL ages of muddy sediments in the delta front setting are overestimated compared with other dating methods. We suggest that OSL age overestimation reflects the trapping of sediments from offshore in the TMZ imported by saltwater intrusions and storm events. The offshore inputs contain high percentages of residual luminescence and are also subjected to incomplete bleaching due to turbid water conditions and near-bed dispersal in the salt-wedge river mouth. We thus suggest that the reduced bleaching efficiency of muddy sediments in delta front settings needs to be accounted for in understanding sedimentary processes and distinguishing between different sedimentary facies in tide-dominated river mouths. Furthermore, we propose that differences in quartz OSL ages of fine- and medium-grained fractions may arise in response to extreme events.

The complexity of luminescence dating of tidal sand body revealed by the discrepancy of paired quartz OSL ages

Optically stimulated luminescence (OSL) dating is becoming a useful technique to yield absolute age of organic-poor sandy deposits. The buried tidal sand body (BTSB) in the coastal zone of northern Jiangsu Province, China, has been suggested to have the same origin as the offshore radial sand ridge in the Yellow Sea. However, chronological constrain of the BSTB is still quite limited. In this study, OSL measurements were conducted using silt-sized multi-grain and coarse-grained single-grain quartz to constrain the depositional history of a 25.6 m core from the BTSB. A low luminescence sensitivity of quartz was observed, and only ∼1.04% of the grains passed the standard rejection criterion for single-grain measurement. Analysis of paired OSL ages from two grain-size fractions using different protocols showed that silt-sized quartz ages were underestimated of 0.14–1.35 ka in comparison to coarse-grained quartz in the depth interval of 5.8–22.4 m. We interpret such an age discrepancy as the effects of lateral infiltration of fine-grained sediment into the sand body due to dynamic feature of channel-ridge system on the shelf. As far as we know, it is the first time that such infiltration is demonstrated through OSL dating. Our OSL data indicated that there is a significant hiatus between the Late Pleistocene stiff clay layer (50–18 ka) and the Holocene sequence. Holocene deposits only occurred in the last 2 ka, with rapid accumulation of ∼17 m-thick sediments at ∼2–1 ka, a slower accumulation between ∼1 and 0.1 ka and rapid land emergence through an accretion of ∼4 m-thick sediment over the past ∼0.1 ka. This study highlights the complexity of OSL dating in highly dynamic sedimentary environments. Therefore, examining different grain size fractions and comparing different measurement protocols are highly deserved in carrying out OSL dating in such environments. • We compared multi-grain silt-sized quartz and single-grain coarse-grained quartz ages for a tidal sand body. • Silt-sized quartz underestimated ages due to ‘younger’ sediment infiltration into tidal sand body. • The buried tidal sand body in the northern Jiangsu Province of China was formed in the last 2 ka.

Dunefield expansion and paleoclimate during MIS 3 in the Qaidam Basin, Northeastern Tibetan Plateau: Evidence from Aeolian-Fluvial processes and revised luminescence chronologies

It is proposed that an extremely warm, humid climate existed in the Tibetan Plateau (TP), including the currently hyper-arid Qaidam Basin (QB), during Marine isotope stage 3 (MIS 3). A detailed luminescence study of aeolian, fluvial and aeolian-fluvial records from the Tiekui Dunefield (TKD) and its margins in the eastern QB reveals paleoenvironmental and paleoclimatic changes during the MIS 3 (ca. 60–32 ka). The records, dated by post-Infrared Infrared Stimulated Luminescence (pIRIR), provide the first aeolian MIS 3 ages in the QB thanks to preservation by overlaying fluvial deposition in the dunefield margins and demonstrate the aeolian expansion of the TKD compared to its modern extent. Complemented by aeolian records in nearby regions, these deposits reflect intensified dune activity in an arid and windy climate and with adequate glacier-derived alluvial-dominated sand supply. These results do not support a significant increase in precipitation from the Asian Summer Monsoon (ASM). Comparisons of new ages derived from pIRIR and Optically Stimulated Luminescence (OSL) of quartz in this study suggest that some published quartz OSL ages of the QB may be underestimated, even below 90 Gy (ca. 30 ka, with normal dose rates of 2.8 Gy/ka). The revised chronology questions previously suggested hypotheses of the existence of a mega Qaidam Lake in the upwind reaches of the basin, under an extremely strong ASM during the MIS 3. We propose a conceptual aeolian-fluvial geomorphic model that demonstrates the paleoclimatic value of aeolian-fluvial records and where and how fluvial process can erode or preserve ancient and previously untapped aeolian records.

Application of Optically Stimulated Luminescence Technique in Exploring a Concealed Sandstone‐type Uranium Deposit

AbstractIdentifying ore‐induced geochemical anomalies at the surface that indicate concealed deposits in buried areas remains a significant challenge in geochemical exploration. In this study, in order to trace the source of the geochemical anomalies, systematic luminescence intensity analyses were conducted on quartz grains from the Quaternary regolith at the Hadatu sandstone‐type uranium deposit in the Erenhot Basin. The optically stimulated luminescence (OSL) ages were much older than the depositional ages of the Quaternary regolith. Moreover, quartz OSL ages were closely related to both borehole grades and sampling depths. Thus, the abnormal mineral OSL ages from near‐surface sediments were ultimately controlled by the sandstone‐type uranium deposits. This is identical to the rapid changes of quartz OSL ages (0.063 ka/cm) and equivalent doses (0.19 Gy/cm) with depths in a given sampling site. The instantaneous soil radon concentration was positively correlated with the quartz OSL apparent age, indicating their ore‐induced origin and, as a result, their effectiveness in the exploration of concealed uranium deposits. Other parameters, including mobile‐state uranium and 210Po contents, were poorly correlated with quartz OSL ages and therefore should only be used with caution for geochemical exploration. This is the first time an attempt has been made to discriminate the ore‐induced sources for different surface anomaly parameters, including instantaneous soil radon, mobile‐state uranium and 210Po contents for concealed sandstone‐type uranium deposits.

Luminescence dating of quartz from ironstones of the Xingu River, Eastern Amazonia

This study reports on the first investigation into the potential of quartz luminescence dating to establish formation ages of ferruginous duricrust deposits (ironstones) of the Xingu River in Eastern Amazonia, Brazil. The studied ironstones comprise sand and gravel cemented by goethite (FeO(OH)), occurring as sandstones and conglomerates in the riverbed of the Xingu River, a major tributary of the Amazon River. The Xingu ironstones have a cavernous morphology and give origin to particular habitat for benthic biota in an area that hosts the largest rapids in Amazonia. So far, the Xingu ironstones have uncertain formation ages and their sedimentary origin is still poorly understood. In this way, seven samples of ironstones distributed along the lower Xingu River were collected for optically stimulated luminescence (OSL) dating of their detrital quartz sand grains. Additionally, the organic content of some samples was dated by radiocarbon ( 14 C) for comparison with quartz OSL ages. The luminescence ages of the sand-sized quartz grains extracted from the ironstones were obtained from medium (100–300 grains) and small (10–20 grains) aliquots using the single aliquot regenerative-dose (SAR) protocol. Equivalent doses (D e ) distributions have varied overdispersion (OD) both for medium size aliquots (OD = 19–58 %) and small size aliquots (OD = 29–76 %). No significant trend was observed between D e and aliquot size. The studied ironstones grow over the riverbed, but stay below or above water throughout the year due to the seasonal water level variation of the Xingu River. However, the effect of water saturation in dose rates is reduced due to relatively low porosity of ironstones. Water saturated dose rates (dry sample dose rates) range from 2.70 ± 0.21 (2.79 ± 0.22) Gy/ka to 12.34 ± 0.97 (13.26 ± 1.12) Gy/ka, which are relatively high when compared to values reported for Brazilian sandy sediments elsewhere (∼1 Gy/ka). Samples with high overdispersion (>40 %) are mainly attributed to mixing of grains trapped in different time periods by goethite cementation. The obtained OSL ages for water saturated (dry) samples range from 3.4 ± 0.3 (3.3 ± 0.4) ka to 59.6 ± 6.0 (58.1 ± 6.4) ka, using D e determined from medium size aliquots and dose response curves fitted by an exponential plus linear function. Radiocarbon ages of the bulk organic matter extracted from selected ironstone varied from ca. 4 cal ka BP to ca. 23 cal ka BP. Significant differences were observed between OSL and radiocarbon ages, suggesting asynchronous trapping of organic matter and detrital quartz within the ironstone matrix. These late Pleistocene to Holocene ages indicate that ironstones of the Xingu River result from an active surface geochemical system able to precipitate goethite and cement detrital sediments under transport. The obtained ages and differences between OSL and radiocarbon ages point out that the ironstones have multiphase and spatially heterogeneous growth across the Xingu riverbed. Our results also expand the application of luminescence dating to different sedimentary deposits.

Luminescence dating of a sedimentary sequence in the eastern North Yellow Sea

Sediments from the Yellow Sea (YS) are important archives for investigating the stratigraphic evolution in relation to global and regional sea-level changes. Here, the upper 40-m-thick interval of a 100-m-long drill core (NYS17), retrieved from the eastern North Yellow Sea (NYS), were studied to explore the late Quaternary sedimentary history in this region. To obtain reliable chronological framework of the core, we utilized multiple luminescence signals from sediments for dating. Coarse-grained (CG) and fine-grained (FG) quartz optically stimulated luminescence (OSL), and K-feldspar/polymineral post-infrared (IR) IR stimulated luminescence (pIRIR50/150) signals were analyzed to obtain age estimates for comparison. Primary results show that quartz OSL ages are consistent with the corrected ages of IR50 and pIRIR150 signals. Chronostratigraphy of core NYS17 presents two phases of rapid accumulation. One is at the interval of 35.6–29.8 m deep, as age controls of sedimentary stratigraphy are in the period of 135–130 ka, corresponding to Marine Isotope Stage (MIS) 6/5. Another occurs in the upper section (14.5–0.9 m) as luminescence ages are constrained between 11 and 9 ka. However, the overlying deposits after 9 ka seem to be very thin in the core site. This is likely attributed to the abundant terrestrial sediment supply during the early Holocene and following starvation after further rise of the sea level and transgression. In contrast, the MIS 5–2 interval remains far to be exactly defined in the core as no age constraint is available. Regionally, correlations of chronostratigraphy of our core with other collected cores from the YS and East China Sea, show comparable depositional records for both the late Pleistocene and Holocene sedimentary successions. These findings indicate that the spatiotemporal variations of sedimentary processes in the YS shelf were closely linked to global sea-level changes during the glacial-interglacial cycles.

Chronology of the Huxushan Paleolithic Site in South China: Inferred from Multiple Luminescence Dating Techniques

Abstract The Huxushan archaeological site in northern Hunan Province, China, was recently excavated, from which stone tools including handaxes were unearthed. The deposits of the site are chemically weathered, which makes it difficult to date the site using numerical dating techniques except for optically stimulated luminescence (OSL) method. Here, we used various luminescence procedures including single-aliquot regenerative-dose (SAR), sensitivity-corrected multiple-aliquot regenerative-dose (SMAR) and thermally transferred optically stimulated luminescence (TT-OSL) SAR procedures on fine-grained quartz, and two-step post-infrared infrared stimulated luminescence (pIRIR) and multi-elevated-temperature pIRIR (MET-pIRIR) procedures on fine polymineral fractions. The results show that the fine quartz grains have excellent luminescence properties and the quartz SAR-, SMAR- and TT-OSL ages for the samples agree with each other and in stratigraphical order except for one sample. The fine polymineral fractions exhibited relatively weak pIRIR and MET-pIRIR signals, resulting in difficulty in constructing the dose-response curve for MET-pIRIR signals and the stratigraphically inconsistent pIRIR(100, 275) ages. The seven samples yielded their quartz OSL ages ranging from about 62 ka to 133 ka. The two samples from the cultural layer was dated to 78 to 92 ka using different procedures on fine quartz. However, given the systematically older pIRIR ages obtained with the fine polymineral grains for the two samples, their quartz OSL ages are considered to represent the minimal ages of this layer, and their pIRIR(100, 275) ages of 118 and 110 ka represent the upper age limit, indicating that the site was occupied by hominins during Marine Isotope Stage 5.

Inter-comparison of optically stimulated luminescence (OSL) ages between different fractions of Holocene deposits from the Yangtze delta and its environmental implications

In fluvial and deltaic environments, different grain-size fractions experience varying degrees of bleaching of OSL signals due to variations in hydrodynamics and depositional processes. This has led to ambiguity for selection of grain-size fraction suitable for OSL dating. Comparison of OSL results from multiple grain-size fractions is one approach to ensure the reliability of OSL ages. We determined the quartz OSL ages of four grain-size fractions from fine silt to sand, together with the single grain OSL sensitivity in a Holocene sediment core from the Yangtze delta. For samples from the lower part of the sediment succession (including tidal river, tidal trough fill, estuarine front, tidal sand and delta front facies), OSL ages determined for different grain-size fractions were generally mutually consistent within the age range of ~2–9 ka, implying minor portion of incompletely bleached grains in the sediment at the time of burial. In contrast, significant partial bleaching was observed for three samples from younger delta front facies deposited during 0.4–0.6 ka. In these three samples, fine-silt quartz OSL ages were overestimated by ~0.5–2.0 ka compared with ages of coarser fractions. Based on the investigation of quartz luminescence sensitivity, we suggest that the southward shift of the Yellow River and increasing erosion in the Yangtze River catchment have led to enhanced water turbidity, resulting in partial bleaching of the sediment and substantial overestimation of the quartz OSL ages of fine silt during 0.4–0.6 ka. Alternatively, the erosion of older deposits and their redeposition elsewhere could retain large residual OSL ages. Notably, fine-silt quartz provides reliable ages for the period of 9–2 ka, suggesting that there was a lower degree of water turbidity compared with that since 2 ka. Therefore, the degree of OSL age overestimation may provide an indication of changes in water turbidity and sedimentary environment. Overall, our findings highlight the complexity of OSL dating in delta environments, and that an understanding of sediment transport and depositional processes is critical for reliable OSL dating.