Post-weld Heat Research Articles

Effect of DC Micro-Pulsing on Microstructure and Mechanical Properties of TIG Welded Ti-6Al-4V

This paper deals with the influence of micro-pulsed direct current on microstructure and mechanical properties of gas tungsten arc welding (GTAW) weldments of Ti-6Al-4V (Ti-64). Bead-on-plate GTA welds were made on the samples in the un-pulsed and micro-pulsed (125 Hz and 250 Hz) conditions. Post-weld heat treatment (PWHT) was performed on a few coupons at 700 °C for 3 h in an inert atmosphere, followed by furnace cooling. In the microstructure, the fusion zone (FZ), base metal (BM), and heat-affected zone (HAZ) can be easily distinguished. The top surface of the FZ has large columnar grains because of lower heat loss to the surrounding atmosphere, and the bottom region of the FZ has comparatively smaller equiaxed grains. The micro-pulsed samples’ FZ grain size was lower than that of those made without pulsing. This shows that high-frequency current has substantially refined prior β grains. The microstructure of the FZ is characterized by an acicular morphology composed of α, martensitic α′, and retained β phases. The FZ’s hardness was higher than the BM due to the presence of martensitic α′. Additionally, the hardness in the HAZ was elevated due to the formation of finer martensitic α′. Micro-pulsed DC welding led to improved mechanical properties, including higher hardness, ultimate tensile strength (UTS), and ductility compared to un-pulsed welding. This enhancement is attributed to the grain refinement achieved with micro-pulsed DC. After PWHT, the prior β grain size remained relatively unchanged compared to the as-welded condition. However, the hardness in the FZ decreased due to the decomposition of α′ into α and β phases. The ductility of all samples improved as a result of the widening of the diffusional α phase.

Revealing the embrittlement phenomena after post-weld heat treatment of high-strength weld metal using high-resolution microscopy

High strength combined with sufficient toughness is a fundamental prerequisite for steel in the field of lightweight construction. Joining high-strength steels by means of welding requires the use of highly advanced filler metals and a stress-relief post-weld heat treatment (PWHT) for optimum performance of the joint. However, such a heat treatment can lead to embrittlement in the weld metal. In this context, the present work deals with the influence of different PWHT holding temperatures on the microstructure and mechanical properties of a high-strength multipass all-weld metal to reveal the embrittlement phenomena. The all-weld metal was fabricated via gas metal arc welding using a metal cored wire with a minimum yield strength of 690 MPa. Charpy V-notch impact testing and tensile testing were carried out to characterize the strength and toughness of the all-weld metal in the as-welded condition and after a 2 h stress-relief PWHT at 520 °C, 580 °C, and 620 °C. The microstructure was characterized utilizing high-resolution techniques such as atom probe tomography and high-energy X-ray diffraction. The strength and toughness of the all-weld metal both decrease after PWHT with different holding temperatures. The cause for the observed embrittlement was found to be the formation of Mn-rich cementite precipitates. These carbides increase in size and phase fraction with increasing holding temperature and lead to a brittle transcrystalline cleavage fracture. Consequently, it was concluded that a gas metal arc welded joint with the investigated filler metal should not be exposed to stress-relief PWHT at temperatures higher than 580 °C.

A quasi-in-situ EBSD study on abnormal grain growth in 2219 aluminum alloy friction stir welded joints during post-weld heat treatment

Abnormal grain growth occurs in the friction stir welds of 2219 aluminum alloy during the solution treatment. To further investigate abnormal grain growth, the quasi-in-situ electron backscatter diffraction (EBSD) experiment, including the EBSD testing and heating by thermal simulation testing machine, was proposed to observe the grain growth process in the weld. The results show that the abnormal grain growth behavior in the stir zone and the thermo-mechanically affected zone is different, and different microstructures at different positions in the weld promote the growth of abnormal grains. In the stir zone, the modified Humphreys’ model is used to analyze the abnormal grain growth behavior. The grains with an advantage size and low strain are more likely to grow abnormally. The non-uniform pinning caused by the dissolution of second-phase particles further promotes abnormal grain growth. In the thermo-mechanically affected zone, the abnormal grains are formed by unstrained equiaxed grains near the stir zone or recrystallized sub-grains. The growth of abnormal grains in the thermo-mechanically affected zone is a strain-induced grain boundary migration process. The research is helpful to understand the abnormal grain growth in friction-stir welds during post-weld heat treatment.

Innovative D-process MIG welding for enhanced performance of thick sections of MDN 250 in aerospace applications

Maraging steel, known for its exceptional strength, toughness and ductility, is widely used in aerospace and hypersonic missile manufacturing. The present study investigates the feasibility of joining 12 mm thick sections of maraging steel using advanced D-Process MIG welding technology. The D-Process integrates different welding modes such as MIG, Single Pulse-MIG and Double Pulse-MIG to optimize welding parameters, minimizing heat input. Additionally, the research investigates the influence of various post-weld heat treatments (PWHTs) on the performance of welded joints. The PWHTs included in the study are Ageing Treatment (AT), Solution Treatment + Ageing Treatment (SAT) and Homogenizing Treatment + Solution Treatment + Ageing Treatment (HSAT). Metallographic and mechanical tests were conducted on as-welded (AW) and PWHT conditions. Results showed the HSAT condition yielded superior properties with an average UTS of 1771 MPa, YS of 1734 MPa, and an average fracture toughness (FT) of 88 MPa√m. This underscores the efficacy of D-Process welding in meeting stringent requirements for maraging steel in aerospace and high-performance applications.

Research on the microstructure, mechanical and fatigue performance of 7075/6061 dissimilar aluminum alloy fusion welding joint treated by nanoparticle and post-weld heat treatment

The microstructure and mechanical properties of 7075/6061 high-strength dissimilar aluminum alloy fusion welds, after TiC nanoparticle-assisted welding and heat treatment, were discussed, and their fatigue performance was analyzed. The results indicate that the significant increase in hardness at the weld zone with T6 treatment compared to T5 is due to the solution treatment providing supersaturated solid solution for subsequent aging precipitation. T5 treatment causes the precipitation in the heat affected zones, thereby increasing the hardness of these regions. The joints exhibit excellent yield strength and tensile strength after heat treatment, with the elongation performance being optimal in T6 state. The fatigue performance of dissimilar aluminum alloy joints treated with nanoparticle and heat treatment is superior to the joints with single riveting. Porosity defects and microcracks generated during welding are prone to stress concentration, with interconnected pores and easily propagating cracks forming fatigue sources for pores and cracks. The crack propagation behavior is influenced by the pinning effect of TiC nanoparticles at the grain boundaries, and the second phase particles hinder crack propagation along the grain boundaries, forcing cracks to extend towards the 6061 side or the HAZ of the lower strength 6061 matrix. It demonstrates that the method of combining nanoparticle-assisted melt inert-gas welding and T6 heat treatment improves the fatigue life of 7075/6061 dissimilar aluminum alloy joints.

The effects of tool rotational speed and post-weld heat treatment of friction stir welded AZ31-B magnesium alloy

Abstract This research article examines the effect of increasing the tool rotational speed and post-weld heat treatment behavior of friction stir-welded AZ31-B magnesium alloy. The variable tool rotational speeds of 1000 rpm, 1200 rpm, 1400 rpm, and 1600 rpm with fixed tool traverse speeds of 30 mm min−1 were chosen based on the trial welding method. Results reveal that the as-welded tensile strength values of 133 MPa, 209 MPa, 215 MPa, and 213 MPa for the corresponding tool rotation speeds and post-weld heat-treated tensile strength values of 140 MPa, 213 MPa, 223 MPa, and 227 MPa significantly increased joint strength when compared to the as-welded process. The measured grain size values are reduced when the tool rotational speed increases due to material dynamic recrystallization. Al-Mg brittle intermetallic compounds significantly reduced the mechanical strength during the increase of the tool’s rotational speed. Fractography analysis reveals all welded samples fractured at the center of the stir zone with a ductile fracture angle of 45°.

Microstructure Evolution and Forming Characteristics of Post-Weld Composite Treatment of 6061 Aluminum Alloy Tailor Welded Blanks

The mechanical properties and cross-sectional geometric dimensions of the fusion zone (FZ), heat affected zone (HAZ), and base metal (BM) of 6xxx series aluminum alloys are inconsistent after filler wire welding, which reduces the formability of aluminum alloy tailor welded blanks (TWBs). This paper proposes a post-weld cold rolling-solution heat treatment (PWCR-SHT) composite process, and the effects of weld excess metal, plastic deformation, and SHT on the formability of aluminum alloy TWBs are studied. The results show that the PWCR-SHT composite process eliminates the weld excess metal and internal pores, reduces the stress concentration at the weld toe, eliminates the local strain hardening behavior, and causes recrystallization in the FZ region. The cupping value of aluminum alloy TWBs using SHT is 105% of BM, in comparison, the cupping value of aluminum alloy TWBs using the PWCR-SHT composite process is 119% of BM, which is the result of the combined effect of geometric dimensions consistency and mechanical properties consistency.

Evaluation of corrosion properties of TA2-Q345 explosive composite plate at different heat treatment temperatures

This study investigated the effects of post-weld heat treatment (PWHT) at 500 °C, 600 °C, 700 °C, and 800 °C on the microstructure and corrosion performance of the TA2-Q345 explosive composite plate, with TA2 as the flyer plate and Q345 as the base plate. X-ray diffraction (XRD), optical microscopy (OM), scanning electron microscopy (SEM), and energy dispersive spectroscopy (EDS) analyses were performed, alongside electrochemical experiments. The explosive welding interface of the TA2-Q345 composite plate exhibited a characteristic wavy structure, which indicated high welding quality. The XRD results indicated that the PWHT temperature significantly affects both the phase structure and the intensity of the diffraction peaks of the oxide film. Additionally, the porosity calculations demonstrated that the sample subjected to PWHT at 500 °C exhibited the lowest porosity in the surface oxide film, resulting in a denser oxide film that effectively enhanced corrosion resistance. However, as the temperature continued to rise, defects such as craters, bulges, and delamination between the oxide film and the titanium matrix were observed. The results of the electrochemical analysis indicated that, compared to untreated samples, the PWHT samples demonstrated improved corrosion resistance. Specifically, the sample with PWHT at 500 °C has the lowest corrosion current density (icorr) of 6.1892E-06 A/cm2, while the untreated sample has the highest icorr of 6.3577E-05 A/cm2, indicating that 500 °C is the optimal temperature. The corrosion process involved the hydrolysis of titanium chloride to form a TiO2 film and localized corrosion of the TiO2 protective film. The corrosion products composed of mainly C, O, and Ti were dispersed on the surface of PWHT samples.

Design of explosively welded Fe–Al multilayer laminated composite pipes: A critical microscopy analysis of stand-off distance and post-weld heat treatment effects on interface properties

This study examined the microstructure and mechanical properties of explosively welded (EXW) Fe–Al multilayer laminated composite pipes, specifically SS321/AA1050/AA5083, with varying stand-off distances (SD) and post-weld heat treatments (PWHT). Findings revealed that higher collision forces at higher-SD produced a wavy interface with finer grains at the AA1050/AA5083 interface. In contrast, lower-SD yielded a smooth, flat interface. At the SS321/AA1050 interface, collision energy resulted in the formation of an uneven composite reaction layer comprising multiple intermetallics. Analysis of the SS321/AA1050 interface revealed that an increase in the PWHT temperature results in diffusion toward the reaction layer, transforming the unevenly Al-rich and Fe-rich phases into a uniform Al85(Fe,Cr,Ni)15 solid solution. The increase in the fraction of this phase made the reaction layer more brittle. At the AA1050/AA5083 interface, PWHT at higher temperatures caused a significant hardness decline extending further from the interface in samples with higher-SD. On the SS321 side of the laminated composite, higher SD resulted in higher kernel average misorientation (KAM) and increased hardness. Despite a decrease in hardness after PWHT at 350 °C, the hardness gradient from the matrix to the interface in laminates with higher SD remained relatively unaffected, whereas the lower SD counterparts experienced a noticeable stress relief.

Microstructural and mechanical properties evolution for 9Cr[sbnd]Si heat resistant steel deposited metals under different heat treatment states

To develop the matched filler metal for the structural materials in Generation IV lead-cooled fast reactor (LFR), the microstructural evolution and mechanical property variation of 9CrSi heat resistant steels deposited metals were investigated both for the as-welded and as-aged (at 550 °C) weld metals. The experimental results indicate two precipitates in the as-welded deposited metals: the bigger M23C6 and the smaller MX. Si facilitates the nucleation of M23C6. The chain-like precipitates (consisting of M23C6) form at the boundaries of prior austenite and martensitic laths in high-Si specimens. They deteriorate not only the strength but also the impact energy. Meanwhile, a few δ ferrites form in high-Si deposited metal deteriorating the impact energy. Precipitates tend to nucleate at the interface between the δ ferrite and the martensite after aging. New types of precipitates (Mo-rich M6X and Laves) with rapid coarsening rate form in as-aged high-Si deposited metals as time increases. Coarse precipitates deteriorate the pinning effect, which causes the recovery of laths and dislocations. Subgrain pinned by M23C6 forms in deposited metals with post-weld heat treatment (PWHT) during aging. The structure hinders the formation of M6X and facilitates the formation of nano-sized MX. Therefore, the mechanical properties of deposited metals with PWHT are stable during long-term (up to 10,000 h) aging treatments.

Numerical and experimental studies on the effect of cryogenic treatment on welding residual stress of TIG welded EN8 steel plate

Most of the conventional welding process induces Welding Residual Stress (WRS), hydrogen embrittlement and distortions to welded components. The post-weld mechanical behaviour has an impact on both structural integrity and operational effectiveness of the welded component. Traditional Post Weld Heat Treatment (PWHT) is capable of relieving WRS to some extent. Based on recent research, Heat Treatment (HT) cycles are comprised of conventional HT and Cryogenic Treatment (CT) gives better fatigue life to welded components by redistributing the residual stress field. There is a need for further research to explore the impact of different parameters of CT affects the mechanical behaviour of welded specimens. In this study, numerical and experimental investigations are conducted to understand the impact of HT cycles comprised of austenitizing, quenching, CT and tempering process, over the TIG welded EN8 plates. Numerical model is developed for predicting the variation in WRS with each stage of HT cycles and observed a considerable redistribution of WRS after the completion of proposed HT cycle. Using the proposed HT cycle, the influence of different soaking periods of CT over the welded components are studied experimentally and shows that 36 hours soaking period have higher impact on the welded component’s mechanical behaviour.

Creep relaxation to relieve residual stress in girth-butt welded X80 pipelines: Simulation and experiment

The residual stress in girth-butt weld presents safety risks for large-diameter oil-gas pipelines, necessitating an in-depth investigation into the welding residual stress and the development of effective methods to mitigate these stresses, thereby enhancing structural integrity. In this work, a finite element girth-butt welding model was developed to predict the residual stress of X80 pipelines. The residual stress relief resulting from local post-weld heat treatment (PWHT) was simulated based on the Norton creep model applicable to X80 steel. The simulation results, encompassing the residual stress both before and after PWHT, were validated through blind-hole drilling measurements. The results demonstrate that the welding residual stresses across all orientations were significantly reduced following PWHT, with a maximum stress reduction of approximately 360 MPa. The primary mechanical mechanism for residual stress relief was identified as high-temperature creep, and it was concluded that the PWHT alleviated welding residual stress effectively when the heating temperature exceeded the creep activation temperature. The consistency between the finite element analysis results and the experimentally measured residual stresses affirms the validity and feasibility of the finite-element-based approach for predicting welding residual stresses.

Microstructure-Linked Mechanical Properties of P91-Incoloy 800HT Dissimilar Metal Welds

Dissimilar metal welds (DMWs) between P91 steel and Incoloy 800HT® using shielded metal arc welding (SMAW) with ENiCrCoMo-1 filler electrode were characterized in detail. The impact of multiple weld passes on microstructure in the heat-affected zone (HAZ) and weld fusion zone (WFZ) was thoroughly investigated. Postweld heat treatment (PWHT) impacts on mechanical characteristics and microstructure were also observed. The DMW was observed with heavy C, Cr, and Mo microsegregation in the WFZ, which deteriorated mechanical strength. The microstructural changes directly affected the mechanical behavior of the DMW. The ultimate tensile strength of the weld fusion zone was low at 576 MPa compared to the base metals’ strength. The tensile specimens failed in the IN 800HT base metal and WFZ. The WFZ had significant microsegregation near the solidified grain boundaries (SGBs). The metallurgical heterogeneity in the WFZ caused the formation of localized stress zones, which directly affected the mechanical behavior of the WFZ. The carbide particles influenced the microhardness in the WFZ and P91 HAZ regions. The PWHT successfully homogenized the microhardness in the WFZ and P91 HAZ regions. The impact toughness decreased to 64 J from 82 J after PWHT due to precipitation at SGBs and its coarsening. The SMAW process involves multiple thermal cycles during welding. The deposition of filler metal in multiple welding passes created uncontrolled variations in the solidification behavior of the WFZ. Microsegregation had a detrimental impact on the microstructure and mechanical properties of the P91 and IN 800HT dissimilar metal welds.

Study on low temperature and narrow heating bands of post weld heat treatment for girth welds stress reduction of long-distance pipelines

Residual stress affects the service safety of pipelines, but there are few efficient methods to reduce the residual stress, especially for long-distance pipelines with large diameters. In this paper, a Secondary Post Weld Heat Treatment (S-PWHT) stress reduction method with low temperature and two narrow heating bands is proposed, and this method fully considers the failure of the corrosion resistance layer caused by high temperature. The temperature distribution and stress distribution under different S-PWHT parameters are compared to obtain the optimal S-PWHT parameters using finite element numerical simulation. The thermocouples are conducted to verify the temperature, and the coercivity experiment is used to verify the stress distribution. Results show that two heating bands width of 80 mm and a peak temperature of 120°C are the optimal S-PWHT parameters with the stress reduced by 61%. Besides, the levels of stress reduction on the inner surface and the HAZ are higher than those on the outer surface and the base metal, respectively. The high-stress zone is transferred from the inner surface to the outer surface, and from the HAZ to the base metal. Furthermore, the stress reduction mechanism of S-PWHT has been revealed through constraint theory. Temperature change is the initial force, and the constraint is the driving force for stress reduction.

Evolution of interface voids and columnar grains of the FeCrAl/RAFMs HIP bonding joint

Hot Isostatic Pressing (HIP) diffusion bonding of FeCrAl and reduced-activation ferritic/martensitic steels (RAFMs) is a novel method for preparing the tritium permeation barrier (TPB) in nuclear fusion reactors. This study primarily investigates the formation mechanisms and evolution of interfacial voids and columnar grains under different bonding temperatures and post-welding heat treatment (PWHT) conditions. It is found that increasing bonding temperature facilitates element diffusion, leading to the closure of interfacial voids. Decarbonization of RAFMs and the increase in Cr content facilitates the formation of interfacial columnar grains, with C playing a crucial role in this process due to its lower diffusion activation energy than Cr. Although appropriate PWHT can reduce the size of interfacial columnar grains, it cannot entirely diminish them. The FeCrAl/IPFs joint effectively prevents the formation of brittle (Cr, C) compounds and interfacial AlN defects. After HIP (1050 °C) + PWHT (750 °C), the joint achieves high tensile strength and ductility both at room temperature and 300 °C. The enhancement in ductility is primarily attributed to the high Schmid factor of interfacial columnar grains, which facilitated the activation of the primary slip system under tensile load, resulting in a high elongation of joints.

In situ evaluation of sensitization in the heat affected zone of supermartensitic stainless steel welded with superduplex filler metal

Supermartensitic stainless steels (SMSS) are high strength corrosion resistant alloys used in oil and gas production in deep water. Failures related to sensitization and excessive hardness in the heat affected zone (HAZ) are prone to happen in harsh environments, such as those found in oil production. To avoid dangerous types of failure, post weld heat treatments (PWHT) are necessary. Temperature and duration of PWHTs are fundamental parameters to be adjusted. In the present work, a minicell was developed to perform DL-EPR tests in different regions of a multipass welded joint of SMSS with superduplex stainless steel as filler metal. The welded joint was submitted to PWHT at 650 °C for 5 and 15 min. The effects of these short duration PWHT on the HAZ and base metal were analyzed using a minicell for double loop electrochemical tests (DL-EPR), atomic force microscopy (AFM), and scanning electron microscopy (SEM). The results indicate that both PWHTs (5 and 15 min) caused the increase in the degree of sensitization of HAZ without the reduction of hardness to acceptable values.

THE IMPACT OF POST-WELD HEAT TREATMENT ON RE-WELDING IN SHIELDED METAL ARC WELDING JOINT ST42 STEEL

Re-welding is a technique used to repair welds that are deemed defective and in danger of causing harm. Post-weld heat treatment is a method for improving welding-induced residual stresses, microstructural changes, hardness, and toughness. This work investigated the influence of post-weld heat treatment on the mechanical characteristics of ST 42 steel re-welding utilizing the SMAW technique and E6013 filler. Four samples with varying degrees of rewelding and post-welding treatment were analyzed. Based on the result, re-welding using SMAW to the St42 steel material led to a 20-40% decrease in mechanical properties, with the most significant reduction observed in the modulus of elasticity after two re-welding cycles. Conversely, post-weld heat treatment (PWHT) applied to the St42 steel subjected to two re-welding processes resulted in a 6-20% increase in mechanical properties, notably a 20% increase in the modulus of elasticity. These findings underscore the effectiveness of PWHT in enhancing mechanical properties, particularly microstructure recovery, in materials that have undergone re-welding.

Effect of post weld heat treatment on the springback of dissimilar aluminium and steel tailor welded blanks fabricated using friction stir welding

ABSTRACT Springback is a common geometrical defect that occurs in the sheet metal forming process and depends on material properties. Different methods have been used to compensate or minimise the springback effect to date. One of the methods is post-weld heat treatment. However, not all materials are heat treatable. In this study, post-weld heat treatment effect on the springback of dissimilar materials AA6061 and SAE1020 fabricated by friction stir welding was investigated using free bending. Different artificial ageing times during the heat treatment process were explored to identify the optimum duration to minimise springback via experiment and finite element analysis. Punch stroke and punch offset tests were conducted to evaluate the effect of multiple parameter values on springback. It was found that an artificial ageing time of 6 hours results in the lowest springback. Springback is inversely proportional to punch stroke as higher punch strokes produce lower springback. For punch offset, the springback increases as the punch is offset towards AA6061 and decreases when offset towards SAE 1020. Interestingly, samples that went through post-weld heat treatment recorded lower springback on both sides even for non-treatable material. The experimental results show a similar pattern and acceptable tolerance compared to the simulation results.

Effect of welding method and heat treatment on the fracture toughness of low alloy steel deposited metal

The fracture toughness of the weld deposited metal plays an important role in the safe service of the reactor pressure vessel (RPV). Shielded melting arc welding (SMAW) and submerged arc welding (SAW) are two common welding methods in the construction of RPV. In this paper, the effects of the welding method and post-weld heat treatment (PWHT) on the index T0 of low-temperature fracture toughness of deposited metal were studied respectively. Through the characterization and observation of microstructure and cleavage crack initiation, the effect mechanism of the welding method and PWHT on the low-temperature fracture toughness of deposited metal was determined. The results show that the position in which oxide near the hardening phase is easy to become the cleavage crack initiation of deposited metal. The PWHT dissolves the M-A island to improve the fracture toughness of the deposited metal. The SMAW deposited metal has a smaller oxide inclusion diameter and less cementite than SAW, resulting in higher fracture toughness.

Postweld Heat Treatment of 15Cr-6Ni-2Mo-1Cu Supermartensitic Stainless Steel Welds

Supermartensitic stainless steels with 15Cr-6Ni- 2Mo-1Cu and 135 ksi minimum yield strength (15Cr- 135 SMSS) offer high strength and good toughness through a complex hierarchical microstructure of nanoscale precipitates, tempered martensite, and reverted austenite. Upon welding and postweld heat treatment, substantial changes to heat-affected zone microstructure and hardness may occur. Here, we reveal spatially heterogeneous microstructure and microhardness in the HAZ of 15Cr-135 SMSS; correlate these changes to measured phase transformation temperatures; and demonstrate that HAZ hardness changes depend strongly on postweld heat treatment (PWHT) temperatures. Furthermore, we demonstrate that PWHT may lead to undesired reductions in base metal yield strength and formulate a design guide for PWHT that quantifies the trade-offs in desired reductions of HAZ hardness with undesired changes to base metal yield strength. These findings have important practical implications for welding procedure design and qualification.