Polymer-infiltrated Ceramic Network Material Research Articles

Intraoral wear of PICN CAD-CAM composite restorations used in severe tooth wear treatment: 5-year results of a prospective clinical study using 3D profilometry

ObjectivesTo evaluate, in a prospective clinical study over 5 years with ex vivo 3D profilometry analyses, the intraoral wear of Polymer-Infiltrated Ceramic Network (PICN) CAD-CAM composite restorations used in severe tooth wear treatment with the One-Step No-Prep technique. Methods192 PICN (Vita Enamic) restorations on molars and premolars were included in a prospective clinical study involving patients treated according to the One-step No-prep protocol (n=7). All patients showed clinical signs of bruxism. Replicas of restorations on molars and premolars were realized at each evaluation time (baseline and then every year up to 5 years) and scanned to perform 3D profilometry. Baseline and recall scans were superimposed with Geomagic Control software. The mean material wear was calculated for the full occlusal area (FOA) and for the occlusal contact area (OCA), respectively. Clinical evaluation of restorations was performed at recall. ResultsAt 5 years, the estimated mean material wear for FOA was inferior to the accuracy threshold of the profilometry measurement chain. For OCA, the estimated mean wear of the material was – 27.97µm. This material wear was shown to be significantly influenced by time (p<0.0001) and patient (p=0.026), while the type of tooth (molar or premolar) had no influence. At 5 years, the survival and the success rates of restorations were 99.48% and 90.62%, respectively. SignificanceThe PICN material exhibits a low wear process in the treatment of severe tooth wear despite the presence of clinical signs of bruxism, and it constitutes a suitable material for the One-step No-prep technique.

Polymer-Infiltrated Ceramic Network Produced by Direct Ink Writing: The Effects of Manufacturing Design on Mechanical Properties

Polymer-infiltrated ceramic network (PICN) materials have gained considerable attention as tooth-restorative materials due to their mechanical compatibility with human teeth, especially with computer-aided design and computer-aided manufacturing (CAD/CAM) technologies. However, the designed geometry affects the mechanical properties of PICN materials. This study aims to study the relationship between manufacturing geometry and mechanical properties. In doing so, zirconia-based PICN materials with different geometries were fabricated using a direct ink-writing process, followed by copolymer infiltration. Comprehensive analyses of the microstructure and structural properties of zirconia scaffolds, as well as PICN materials, were performed. The mechanical properties were assessed through compression testing and digital image correlation analysis. The results revealed that the compression strength of PICN pieces was significantly higher than the respective zirconia scaffolds without polymer infiltration. In addition, two geometries (C-grid 0 and C-grid 45) have the highest mechanical performance.

Development of zirconia-based polymer-infiltrated ceramic network for dental restorative material

Polymer-infiltrated ceramic network (PICN) materials have gained considerable attention as tooth restorative materials owing to their mechanical compatibility with human teeth. However, the mechanical strength of contemporary PICN materials is lower than those of conventional resin composites and ceramics. This study aims to develop novel high-strength PICN for use as a dental restorative material. Zirconia-based PICN (EXP) was fabricated using 3 mol% yttria tetragonal polycrystalline zirconia powder and resin monomers via slip casting, followed by sintering and polymer infiltration. Comprehensive analyses of the microstructure, mechanical properties, and physicochemical properties of EXP were performed using scanning electron microscopy with energy-dispersive X-ray spectroscopy, Fourier transform infrared spectroscopy, inorganic content measurements, three-point bending test, Vickers hardness test, two-body wear test, shear bond strength (SBS) test, surface free energy analysis, and water sorption/solubility test. Commercially available computer-aided design/computer-aided manufacturing (CAD/CAM) materials, including resin composite (CERASMART), silicate-based PICN (ENAMIC), and zirconia ceramic (e.max ZirCAD), were used for comparison. The analyses highlight the dual network structure of EXP, which comprised a zirconia skeleton and an infiltrated resin phase. EXP exhibits a flexural strength of 346.0 ± 46.0 MPa, flexural modulus of 44.0 ± 3.7 GPa, and Vickers hardness of 440.1 ± 51.2 VHN. The mechanical properties of EXP are significantly higher than those of CERASMART and ENAMIC but lower than those of ZirCAD. Notably, the EXP hardness closely mimics that of the human enamel. The wear volume, SBS, and water sorption/solubility of EXP are comparable to those of CERASMART and ENAMIC. Therefore, EXP has potential applications as a tooth restorative material.

Bond strength to dentin of a Polymer-infiltrate ceramic-network material cemented with dual resin cements submitted to different adhesive strategies

The purpose of the present in vitro study is to assess the immediate and long-term bond strength of a self-adhesive and conventional resin luting agents with a new hybrid restorative material to dentin. Blocks of a polymer-infiltrated ceramic-network (PICN) material (VITA Enamic) were cemented to a flat exposed dentin surface through different protocols. The groups were divided considering the combination of resin luting agent and ceramic surface treatment (U200 – Relyx U200 with silane; Ult + Sil – Relyx Ultimate with silane; Ult + SBU – Relyx Ultimate with Scotchbond Universal) and dentin treatment (NT – no dentin treatment; ER – etch-and-rinse with 35 % phosphoric acid) (n = 6). Beam-shaped specimens were obtained by cutting the cemented restorations. Specimens were submitted to microtensile bond strength in a universal testing machine (EMIC). Half of the specimens were tested 24 h after cementation, and the other half were tested after 12 months of water storage. ANOVA revealed one significant interaction between “time” and “dentin treatment” factors, as ER strategy was associated with bond strength decreases after 12 months. All resin luting agents (u200, Ult + Sil, and Ult + SBU) presented higher immediate μTBS with ER adhesive strategy. As the groups Ult + Sil, with both ER and SE adhesive strategies, and (Ult + SBU), with ER adhesive strategy, showed higher μTBS values after 12 months. It was concluded that conventional dual resin cement, combined with ER strategy produced better bond strength to dentin when cementing indirect PICN restoration.

Influence of Ceramic Materials and Preparation Designs on the Marginal Adaptation of Inlays and Onlays after Thermocycling.

The aim of the current study is to evaluate inlay and onlay marginal adaptation of two different ceramic materials using two intra-coronal preparation designs. An examination of the marginal adaption of two materials, lithium disilicate (IPS e.max CAD) (EX) and polymer infiltrated ceramic network material (PICN; Vita Enamic) (EN), and two preparation designs where D1 represents MOD inlay preparation with no cusp reduction and D2 in addition of the basic MOD preparation, the buccal cusps (functional cusps) were reduced by 1.5 mm. 4 sub-groups (EX-D1), (EX-D2), (EN-D1), (EN-D2) were conducted. Forty (n=40) mandibular molars were used. A stereomicroscope was used to assess the marginal gap before, after cementation and after thermocycling. Values were calculated for the mean, median, standard deviation (Sd), minimum, maximum, and 95% confidence interval. Pair-wise comparisons using Tukey's Post-Hoc test were performed following a significant analysis of variance (ANOVA) P ≤ 0.05. The results revealed that lithium disilicate (IPS e.max CAD) showed statistically significantly higher mean gap distance than polymer infiltrated ceramic network material (PICN; Vita Enamic) (61μm to 99μm). Pair-wise comparisons showed that D2 design has statistically significant higher mean gap values than D1. Both lithium disilicate (IPS e.max CAD) or polymer infiltrated ceramic network material (PICN; Vita Enamic) provided marginal adaptation within clinical accepted range. Polymer infiltrated ceramic network material restorations provided better fit than lithium disilicate restorations. Cusp coverage has a greater marginal gap compared to conventional Preparation.

Effects on different full-coverage designs and materials of crack propagation in first mandibular molar: an extended finite element method study.

Objectives: This study aims to investigate the biomechanical properties of fracture resistance in cracked teeth using five different full-coverage restorations made of three different materials. Materials and Methods: A 3D model of a mandibular first molar was created to design five different full-coverage repair models: crown, crown with composite resin filling inside, occlusal veneer, occlusal veneer with composite resin filling inside and onlay. These repair models were fabricated using three different materials, namely, zirconia, lithium disilicate (LDS), and a hybrid polymer-infiltrated ceramic network material (PIC). In total, 15 repair models were tested using the extended finite element method (XFEM), with an occlusal load of 5000N applied slowly to the occlusal surface of the restoration. The analysis of stress distribution in the restoration and dentin crack line was conducted to measure and record the crack initial load on the restoration and dentin. Results: The results showed that restorations on the occlusal surface significantly improved crack resistance, with zirconia exhibiting superior fracture resistance among the materials tested. Restorations of crown with composite resin filling inside demonstrated the highest resistance to fracture, while occlusal veneers showed the lowest. MPS concentration was observed at the interface between the restoration and dentin and at the root bifurcation, with the highest values at the top of crack development. Dentin covered by oxidized restorations had the highest displacement, while PIC restorations exhibited the lowest. Pulp analysis revealed selective MPS concentration and strain patterns in models with zirconia restorations and onlay, with pronounced pulp displacement in zirconia restorations and onlay. Enamel analysis indicated larger MPS values and displacements in zirconia restoration models and onlay, with higher strain in onlay. Restoration played a crucial role in protecting the tooth, with crack propagation initial loads in dentin surpassing restorations in experimental groups. Conclusion: This study confirms that full-coverage restorations significantly increased the fracture resistance of cracked teeth, with zirconia restorations significantly protecting the underlying cracked tooth. Elimination of fracture lines in the restoration design can improve fracture resistance in cracked teeth. The findings have implications for dental prosthetic design and clinical practice.

The effect of water storage on nanoindentation creep of various CAD-CAM composite blocks

BackgroundTo study the effect of water storage (3 months) on the creep deformation of various CAD-CAM composite structures at the nanoscale and compare it to that at the macroscale.MethodsSeven CAD-CAM blocks were investigated: five resin-composite blocks (RCB), one polymer-infiltrated ceramic network (PICN) block, and one ceramic-filled polyetheretherketone (PEEK) block. Specimens of each material (n = 6) were separated into two groups (n = 3) according to their storage conditions (24 h dry storage at 23˚C and 3 months storage in 37˚C distilled water). Nano-indentation creep measurements were undertaken (creep depth measured in µm) using a nanoindenter (Nanovea) equipped with Berkovich three-sided pyramidal diamond tip. The machine was set for the chosen parameters: a load of 20 gf, a pause of 20 s, and the material type. Thirty indentations on 3 samples were made for each material for each test. Data were analysed using two-way ANOVA followed by one-way ANOVA and Bonferroni post hoc tests and independent t-test (< 0.05) for comparisons between the materials.ResultsThe nanoindentation creep depth after 24 h storage ranged from 0.09 to 0.33 μm and increased after 3 months storage in distilled water to between 0.28 and 3.46 μm. There was a statistically significant difference in nanoindentation creep behaviour between the two storage conditions for each investigated material (independent t-test) and between all materials (Bonferroni post hoc). There was a non-significant negative correlation between nanoindentation creep (µm) and filler weight% at 24 h dry storage but a significant correlation at 3 months of water storage. A further non-significant positive correlation between nanoindentation creep (µm) and bulk compressive creep (%) was found.ConclusionThe PICN material showed superior dimensional stability in terms of nanoindentation creep depth in both storage conditions. Other composite blocks showed comparable performance at 24 h dry condition, but an increased nanoindentation creep upon water storage.

Effect of thickness, translucency, and substrates on the masking ability of a polymer-infiltrated ceramic-network material.

The aim of this in vitro study is to evaluate the masking ability of polymer-infiltrated ceramic-network materials (PICN) with different translucencies and thicknesses on multiple types of substrates. Ceramic samples were prepared of VITA ENAMIC blocks in two different translucencies (2M2-T, 2M2-HT) in a thickness range of 0.5-2.5 mm (±0.05 mm). Layered specimens were obtained using composite substrates in nine shades and transparent try-in paste. Spectral reflectance of specimens was measured using a Konica Minolta CM-3720d spectrophotometer and D65 standard illumination. CIEDE2000 color difference (ΔE00 ) between two samples was evaluated using 50%:50% perceptibility and acceptability thresholds. Specular component of the reflection was examined with Specular Component Excluded (SCE) and Included (SCI) settings. Statistical evaluation was performed by linear regression analysis, Kruskal-Wallis test, and multiplicative effect analysis. An increase in thickness of 0.5 mm reduces ΔE00 of HT samples to 73.5%, of T samples to 60.5% (p < 0.0001). Five substrates with HT specimens, and three substrates with T specimens had significantly different results from average (p < 0.05). There is a significant difference between SCE and SCI data depending on the wavelength (p < 0.0001). Masking ability of PICN materials is influenced by the thickness and translucency of the ceramic, and by the substrate. Reflection of the examined PICN material is characterized by both diffuse and specular reflection. Although PICN materials have been available on the market for 10 years now, there is a lack of information regarding their masking ability. Acquiring in-depth data and thereby practical experience of the factors affecting the esthetics of PICN materials is essential for creating perfectly lifelike restorations.

Quality of CAD-CAM inlays placed on aged resin-based composite restorations used as deep margin elevation: a laboratory study

ObjectivesTo assess the impact of the age of resin-based composite (RBC) restorations used for deep margin elevation (DME) on the marginal quality and fracture resistance of inlays.Materials and methodsPermanent human molars with direct RBC restorations, involving the mesial, occlusal, and distal surface (MOD), were allocated to four groups (each n = 12). Half of the teeth underwent thermomechanical loading including 240,000 occlusal load cycles and 534 thermal cycles (TML, 5 °C/55 °C; 49 N, 1.7 Hz). With RBC left in one proximal box as DME, all teeth received MOD inlays, made from lithium disilicate (LDS) or a polymer-infiltrated ceramic network material (PICN). The restored teeth underwent TML including 1.2 million occlusal cyclic loadings and 2673 thermal cycles. The marginal quality was assessed at baseline and after both runs of TML. Load-to-fracture tests were performed. The statistical analysis comprised multiple linear regressions (α = 0.05).ResultsSimulated aging of RBC restorations had no significant effect on the marginal quality at the interface between the RBC and the tooth and the RBC and the inlay (p ≥ 0.247). Across time points, higher percentages of non-continuous margin were observed between the inlay and the tooth than between the tooth and the RBC (p ≤ 0.039). The age of the DME did not significantly affect the fracture resistance (p ≥ 0.052).ConclusionsArtificial aging of RBC restorations used for DME had no detrimental effect on the marginal quality and fracture resistance of LDS and PICN inlays.Clinical relevanceThis laboratory study suggests that—in select cases—intact, direct RBC restorations not placed immediately before the delivery of an indirect restoration may be used for DME.

Fracture resistance of CAD/CAM blocks cemented on dentin using different cementation strategies.

To determine whether the fracture resistance of computer-aided design/computer-aided manufacturing (CAD/CAM) resin-based composites and polymer-infiltrated ceramic network materials cemented on dentin is influenced by the restoration thickness and composite cement application strategy. Disc-shaped specimens (Ø = 7 mm) of 0.8 mm and 1.5 mm thicknesses were milled from two CAD/CAM materials: resin-based composite (RBC, Cerasmart 270) and polymer-infiltrated ceramic network (PICN, Vita Enamic). The discs (n = 8 per group) were cemented on flattened dentin using three different cementation strategies: 1) self-adhesive composite cement (RelyX U200) in light-curing mode (LC-SAC), 2) universal adhesive (Single Bond Universal) with composite cement (RelyX Ultimate) in auto-curing mode (AC cement), and 3) adhesive and composite cement as in 2) but in light-curing mode (LC cement). The restorative surface was indented perpendicularly with a compressive load using a universal testing machine until fracture. The fracture resistance (N) of RBC and PICN was separately analyzed using two-way ANOVA and Tukey's post-hoc test (α = 0.05). The fracture resistance of each material was significantly influenced by the material thickness and cementation strategy (P < 0.05). Irrespective of the material type and cementation strategy, thicker materials exhibit higher fracture resistance. For RBC, the fracture resistance of the LC cement group was significantly higher than that of AC cement only at 0.8 mm thickness. For PICN, the LC-cement cementation strategy produced superior fracture resistance, regardless of the restoration thickness. The fracture resistance of Cerasmart 270 was higher for the thicker material; the fracture resistance of LC cement was higher than that of AC cement at 0.8 mm thickness cemented to dentin. In comparison, LC cement showed the highest fracture resistance for Vita Enamic for both material thicknesses.

Comparative study on the impact-sliding wear behaviour of CAD/CAM resin-ceramic materials and tooth enamel.

To compare the impact-sliding wear of different CAD/CAM resin-ceramic materials and tooth enamel, and explore the corresponding wear damage mechanism. Human tooth enamel (EN), Vita ENAMIC (Vita, VE), Lava Ultimate (3M, LU), and GC CERASMART (GC, CS) were used in this study. The hardness, elastic modulus, and roughness values of the samples were measured. Further, impact-sliding wear tests were performed in a ball-on-flat configuration with spherical zirconia antagonists and the coefficients of friction (CoF) were recorded simultaneously. Additionally, a white light interferometer was used to determine the volume losses and scanning electron microscopy was used to observe the wear morphology of the wear scars and the damage feature in the vertical sections to clarify the damage mechanism during the impact-sliding wear test. EN exhibited the highest elastic modulus and CoF, followed by VE, LU, and CS. The hardness and roughness of EN and VE were similar and were higher than those of LU and CS. Throughout the wear tests, VE exhibited the highest volume loss, whereas CS exhibited the lowest. The wear damage characteristics of VE were similar to those of EN, displaying brittle fractures of inorganic substances and plastic deformation of organic substances in the impact part, exhibiting plough marks in the sliding parts. In the case of LU and CS, the entire wear areas displayed plastic deformation of the resin matrix, exfoliation of the filler particles, and plough marks. Enamel and polymer-infiltrated ceramic network materials exhibit similar wear damage modes. Additionally, the high-density nanocomposite resin material is the most resistant to impact-sliding wear from a tribological perspective.

Three-dimensional assessment of internal adaptation measurement of three cad/cam ceramic systems

This study aimed to evaluate the internal adaptation of three different computer-aided design/computer-aided manufacturing (CAD/CAM) ceramic crowns. The internal adaptation of a polymer-infiltrated ceramic network material (Vita Enamic [VE]) was compared to two machinable glass-ceramics; Zirconia-reinforced lithium silicate (Vita Suprinity [VS]) and a lithium disilicate glass-ceramic (IPS e.max. CAD). Thirty human premolars of average size were prepared (n=10 each group) by computer numerical control to fulfill the criteria of all-ceramic crown design. Optical impressions were taken for each tooth preparation using the CAD/CAM scanner. Thirty crowns were fabricated using CAD/CAM system and divided into three groups (IPS e.max, VE, and VS). To assess the internal fit of tested crowns, the gap between the intaglio of each crown and the corresponding tooth surface was evaluated using a 3D digital scanner using the Triple-scan Protocol. One-way ANOVA followed by Tukey Post Hoc statistical tests were used to statistically analyze results of the internal fit. There was a statistically significant difference for all groups at the four axial walls (p = 0.000002). For total internal fit between groups, comparisons showed a statistically significant difference between all tested groups (p=0.000002). When each pair of groups was statistically compared with each other, all pair comparisons showed a statistically significant difference. IPS e.max CAD had the best internal fit, followed by Vita Enamic, then Vita Suprinity. For all ceramics tested, values of internal fit of all ceramics tested were within the clinically acceptable range.

Surface characterization of indirect restorative materials submitted to different etching protocols

ObjectivesThis in vitro study aimed to evaluate the effect of different times and concentrations of hydrofluoric acid etching on the surface of indirect restorative materials obtained from blocks used in CAD-CAM technology. MethodsSpecimens (4 mm × 4 mm × 0.8 mm) were obtained for each indirect restorative material: zirconia-reinforced lithium monosilicate ceramic (Celtra Duo), nanoceramic resin (Lava Ultimate), and polymer-infiltrated ceramic network material (Vita Enamic). The materials were submitted to etching with 5% or 10% hydrofluoric acid for 20, 40, 60, or 90 s. A control group for each material was evaluated without any surface treatment, totaling nine experimental groups for each material (n = 10). The specimens were evaluated for surface roughness (Ra and Rz), confocal optical microscopy, the contact angle (θ), surface free energy (γs), total free interaction energy (∆G) using a goniometer, and microshear bond strength to resin cement. Specimen images were obtained using scanning electron microscopy, confocal optical microscopy, and atomic force microscopy. Data on the surface roughness, the contact angle, surface free energy, total free interaction energy, and bond strength were subjected to two-way ANOVA and Tukey´s test (α=0.05). ResultsIn general, Celtra Duo showed better results after etching with 10% hydrofluoric acid for 40 or 60 s. Lava Ultimate showed better performance after etching with 10% hydrofluoric acid for 20 or 40 s, whereas Vita Enamic showed better results after etching with 5% hydrofluoric acid for 90 s. ConclusionEach material showed different characteristics after etching with hydrofluoric acid. Knowledge of the proper protocol for each material is essential to ensure improvements in the adhesion process and durability of indirect restorations. In general, Celtra Duo presented mechanical properties superior to those of Lava Ultimate and Vita Enamic. Clinical SignificanceSpecific etching protocols must be recommended for each indirect material because longer exposure to hydrofluoric acid can jeopardize the surface, thus affecting the mechanical and bond strength properties.

Effect of thickness on color and translucency of a multi-color polymer-infiltrated ceramic-network material.

To evaluate the effect of thickness on color and translucency of a multi-color polymer-infiltrated ceramic-network (PICN) material. Specimens of 0.5, 1.0, 1.5 mm thicknesses were obtained by sectioning VITA ENAMIC® multiColor (E-MC) High Translucent CAD-CAM blocks (1M1-HT, 1M2-HT, 2M2-HT, 3M2-HT, and 4M2-HT). Spectral reflectance and color coordinates were measured on white and black backgrounds using a spectroradiometer, CIE D65 illuminant and CIE 45°/0° geometry. CIEDE2000 color and translucency differences (ΔE00 and ΔTP00 ) between thicknesses and adjacent layers were evaluated using their respective 50:50% perceptibility and acceptability thresholds (PT00 and AT00 ). In general, ΔE00 between thicknesses for all shades and layers were above AT00 in general. Chroma decreased from cervical to incisal layers with statistically significant differences (p < 0.05), and ΔE00 between sequential layers were above PT00 , for all shades and thicknesses. TP00 decreased from 0.5 to 1.5 mm and increased from cervical to incisal layers for all shades with statically significant translucency differences (p < 0.05). In general, for all thicknesses, TPT00 < ΔTP00 < TAT00 for sequential layers. The gradient in color and translucency of E-MC PICN material was influenced by the thickness of the CAD-CAM block. In addition, color and TP transition values between the layers depends on the thickness and shade. The effect of thickness must be taken into account by dental technicians and dentists when CAD-CAM multicolor PICN materials are used.

Wear of Polymer-Infiltrated Ceramic Network Materials against Enamel.

Polymer-infiltrated ceramic network materials (PICNs) have high mechanical compatibility with human enamel. However, the wear properties of PICN against natural human enamel have not yet been clarified. We investigated the in vitro two-body wear behaviors of PICNs and an enamel antagonist. Two PICNs were used: Experimental PICN (EXP) prepared via the infiltration of methacrylate-based resin into the porous silica ceramic network and commercial Vita Enamic (ENA). Two commercial dental ceramics, lithium disilicate glass (LDS) and zirconia (ZIR), were also characterized, and their wear performance was compared to PICNs. The samples were subjected to Vickers hardness tests and two-body wear tests that involve the samples being cyclically impacted by enamel antagonists underwater at 37 °C. The results reveal that the Vickers hardness of EXP (301 ± 36) was closest to that of enamel (317 ± 17). The volumetric wear losses of EXP and ENA were similar to those of LDS but higher than that of zirconia. The volumetric wear loss of the enamel antagonist impacted against EXP was moderate among the examined samples. These results suggest that EXP has wear behavior similar to that of enamel. Therefore, PICNs are mechanically comparable to enamel in terms of hardness and wear and are excellent tooth-restoration materials.

Quantitative nano-mechanical mapping AFM-based method for elastic modulus and surface roughness measurements of model polymer infiltrated ceramics

ObjectivesThe aim of this in vitro investigation was to assess and compare surface characteristics and nanomechanics of model polymer infiltrated ceramic network (PICN) materials compared to CAD/CAM resin composite blocks. Material and methodsFour model PICN materials sintered at different temperatures (Exp.125, Exp.130, Exp.135 and Exp.155) were investigated along with three CAD/CAM resin composites; Lava Ultimate (LU), Cerasmart (CS) and Grandio Bloc (GB), and one commercial PICN block - Vita Enamic (VE). Forty samples were prepared with dimensions of 14 × 12 × 2 mm for resin ceramic and VE blocks and 15 × 2 mm discs for model PICN materials. All samples were scanned using atomic force microscopy (AFM) (n = 3) at multiple locations and two different scan sizes (20 ×20 µm and 3 ×3 µm). Surface optical gloss (n = 5) at 60° was also determined for all the groups. Data were analysed using one-way ANOVA, and Tukey’s post hoc test (α = 0.05). ResultsResin composite blocks showed smoother surfaces compared to the PICN materials. The average surface roughness values (Ra) ranged from 7.75 nm to 31.21 nm and the gloss value ranged from 56.43 GU to 91.81 GU. The highest surface roughness value was found for Exp.125 (31.21 nm) while LU showed the lowest roughness value (7.75 nm) (the difference being statistically significant: p = 0.001). Variation was noticed in terms of nanomechanical mapping within and between the groups. Images generated from the elastic modulus map values clearly indicated that all PICN materials had more than one phase and very different components. ConclusionsCAD/CAM resin composite blocks exhibited higher gloss and lower roughness values compared to PICN materials. However, both the commercial and model PICN materials showed more stiffness than resin composite with the presence of at least two different phases. Sintering temperature appears to have a significant effect on material topography and nanomechanical properties. The model PICN sintered at 1550 °C showed a comparable range of elastic modulus values to those of enamel.

Effect of repeated ultrasonic instrumentation on single-unit crowns: a laboratory study.

This laboratory study aimed to assess the effects of ultrasonic instrumentation, simulating 10years of supportive periodontal therapy (SPT), on single-unit crowns. Standardized crowns were fabricated from porcelain-fused-to-metal (PFM) (n = 12), zirconia (ZrO2) (n = 12), lithium disilicate (LDS) (n = 12), feldspar ceramic (FSFC) (n = 6), and polymer-infiltrated ceramic network material (PICN) (n = 6). The crowns, luted on PICN abutments with resin-based luting material (RBLM), and if applicable glass ionomer cement (GILC), underwent thermal cycling and trimonthly ultrasonic instrumentation. After 1 and 10years of simulated SPT, restoration quality assessments were performed, comprising profilometric surface roughness measurements, marginal integrity evaluations, and scores for luting material remnants and visible cracks. The statistical analysis included multiple logistic regressions with nested designs (α = 0.05). During simulated SPT, bulk fractures (n = 2) and a de-cementation failure (n = 1) of LDS and ZrO2 crowns were observed. No significant change in roughness was detected after 10years (p = 0.078). Over time, marginal defects increased (p = 0.010), with PFM crowns showing the highest rate of chippings at sites with a narrow shoulder. Fewer marginal defects were detectable on crowns luted with RBLM compared with GILC (p = 0.005). Luting material remnants decreased during SPT (p < 0.001). Ultrasonic instrumentation caused cracks in most crown materials, in particular at sites with a narrow shoulder and in PFM crowns. Repeated ultrasonic instrumentation may damage single-unit crowns. PFM crowns with a narrow, all-ceramic margin are especially prone to defects. Frequent ultrasonic instrumentation of restoration margins of fixed dental prostheses, PFM crowns in particular, ought to be avoided.

Survival of Hybrid Laminate Veneers using two different tooth preparation techniques: Randomized Clinical Trial.

The aim of this study was to evaluate the survival of laminate veneers constructed using a recent polymer-infiltrated ceramic network material following the aesthetic pre-evaluative temporary (APT) technique of tooth preparation in comparison to traditional technique. Six patients received 54 laminate veneers. They were divided into two equal groups (n=27) according to the technique of tooth preparation: group T: traditional technique and group A: aesthetic pre-evaluative temporary technique. VITA ENAMIC material was used for CAD/CAM construction of laminate veneers. Cementation was performed using a light cured resin cement. The laminate veneers were evaluated at baseline, after 3, 6 and 12 months according to the modified United States Public Health Service (USPHS) criteriea. The data was collected, tabulated and statistically analyzed. Secondary caries, endodontic complications, cracks and loss of retention were not noted in any laminate veneer. Extensive fractures were not detected in both study groups through the study period. There was a statistically significant decrease of color match criteria between the two groups at the 6 and 12 months recalls. Based on this study, both preparation techniques resulted in successful clinical performance. After 12 months, all the veneers in both groups showed no post-operative sensitivity and all patients were highly satisfied regarding their veneers. However, there was a deterioration in color match criteria through the study period in both study groups.

Color Stability and Translucency of Polymer-Infiltrated Ceramic-Network Materials—A Systematic Review of the Literature

This systematic review aimed to compile information and report the color stability and translucency of polymer-infiltrated ceramic-network (PICN) materials for suitable clinical applications in dentistry. Original peer-reviewed articles in electronic databases including PubMed, MEDLINE, Scopus, and Web of Science were searched to identify relevant papers published between January 2013 and August 2020. The published papers were only in the English language and limited to in vitro studies, and experimental reports were considered. The data from nine studies were considered when reviewing the color stability and translucency of PICN in comparison to other commonly used restorative materials. Among the included studies, color stability assessment was performed in five studies, and the other four studies were involved in the combined assessment of both color stability and translucency. PICN materials are a comparatively newer class of restorative materials and are recommended to overcome the drawbacks of ceramics and resin composites. The outcomes of previous laboratory studies still do not provide convincing results regarding the optical properties of PICN materials. However, with existing sources and evidence, PICN materials exhibit less color stability than ceramics do but better color stability compared to that of resin nanoceramics (RNC) and resin composites. The translucency of PICN materials is low compared to that of ceramics, nanoceramics, and resin composites.

Comparison of translucency and opalescence among different dental monolithic ceramics

Statement of problemMonolithic ceramic restorations designed by computer-aided design and computer-aided manufacturing are increasingly being used by clinicians. With the introduction of new materials, their optical characteristics also need to be investigated. PurposeThe purpose of this in vitro study was to compare the translucency and opalescence of lithium disilicate, zirconia-reinforced lithium silicate, presintered zirconia-reinforced lithium silicate, polymer-infiltrated ceramic-network material, and multilayer zirconia. Material and methodsA total of 50 rectangular plates (14×12×1 mm) of 5 monolithic ceramics were prepared in this in vitro study (n=10). Each zirconia specimen was divided into 3 groups of incisal, middle, and gingival thirds. Each group was then evaluated separately. The color parameters of specimens were measured on 3 backgrounds, white, black, and #3 Ivoclar Natural Die Color material, by using a spectrophotometer. The translucency and opalescence of the specimens were determined by the relevant equations, and between-group comparisons were made. One-way ANOVA and Tamhane post hoc tests were used to compare groups (α=.05). ResultsThe difference among the groups was significant in translucency (F=137.346, df=6, P<.001), contrast ratio (F=134.148, df=6, P<.001), and opalescence parameters (F=128.028, df=6, P<.001). The 3 zirconia groups (10.87 ±0.54 to 11.88 ±0.26) had a significantly lower translucency than the other groups, and the zirconia-reinforced lithium silicate group (18.14 ±0.74) showed the highest translucency. Zirconia-reinforced lithium silicate (12.36 ±0.42) had the highest opalescence, and the lowest opalescence was found for polymer-infiltrated ceramic-network (5.43 ±0.28) and the incisal third of zirconia (5.45 ±1.06). ConclusionsThe zirconia-reinforced lithium silicate and presintered zirconia-reinforced lithium silicate specimens had the highest translucency and opalescence. The studied multilayer zirconia, which had different cubic phase values from incisal to gingival blank, showed similar translucency over the entire range, and differences among different regions were related to chromatic variables.