Evolution Of Physical Properties Research Articles

Testing dynamic correlations and nonlinearity in bivariate time series through information measures and surrogate data analysis.

The increasing availability of time series data depicting the evolution of physical system properties has prompted the development of methods focused on extracting insights into the system behavior over time, discerning whether it stems from deterministic or stochastic dynamical systems. Surrogate data testing plays a crucial role in this process by facilitating robust statistical assessments. This ensures that the observed results are not mere occurrences by chance, but genuinely reflect the inherent characteristics of the underlying system. The initial process involves formulating a null hypothesis, which is tested using surrogate data in cases where assumptions about the underlying distributions are absent. A discriminating statistic is then computed for both the original data and each surrogate data set. Significantly deviating values between the original data and the surrogate data ensemble lead to the rejection of the null hypothesis. In this work, we present various surrogate methods designed to assess specific statistical properties in random processes. Specifically, we introduce methods for evaluating the presence of autodependencies and nonlinear dynamics within individual processes, using Information Storage as a discriminating statistic. Additionally, methods are introduced for detecting coupling and nonlinearities in bivariate processes, employing the Mutual Information Rate for this purpose. The surrogate methods introduced are first tested through simulations involving univariate and bivariate processes exhibiting both linear and nonlinear dynamics. Then, they are applied to physiological time series of Heart Period (RR intervals) and respiratory flow (RESP) variability measured during spontaneous and paced breathing. Simulations demonstrated that the proposed methods effectively identify essential dynamical features of stochastic systems. The real data application showed that paced breathing, at low breathing rate, increases the predictability of the individual dynamics of RR and RESP and dampens nonlinearity in their coupled dynamics.

Low temperature sputtering deposition of Al1−xScxN thin films: Physical, chemical, and piezoelectric properties evolution by tuning the nitrogen flux in (Ar + N2) reactive atmosphere

This work investigates the physical properties of Al1−xScxN thin films sputtered at low temperatures by varying the process conditions. Specifically, the films were deposited at room temperature by applying a radio frequency power equal to 150 W to an AlSc alloy (60:40) target, varying the nitrogen flux percentage in the (Ar + N2) sputtering atmosphere (30%, 40%, 50%, and 60%) and keeping constant the working pressure at 5 × 10−3 mbar. The structural and chemical properties of the Al1−xScxN films were studied by x-ray diffraction and Rutherford backscattering spectrometry techniques, respectively. The piezoelectric response was investigated by piezoresponse force microscopy. In addition, the surface potential was evaluated for the first time for Sc-doped AlN thin films by Kelvin probe force microscopy, providing piezoelectric coefficients free from the no-piezoelectric additional effect to the mechanical deformation, i.e., the electrostatic force. By alloying AlN with scandium, the piezoelectric response was strongly enhanced (up to 200% compared to undoped AlN), despite the low deposition temperature and the absence of any other additional energy source supplied to the adatoms during thin film growth, which generally promotes a better structural arrangement of polycrystalline film. This is a strategic result in the field of microelectromechanical systems completely fabricated at low temperatures.

Evolution of physical properties of a cultivated organic soil drained by drainage trench

Evolution of physical properties of a cultivated organic soil drained by drainage trench

Fabrication of a packaging film based on PLA blends: The evolution of physical, mechanical, and rheological properties

AbstractToday, the use of biodegradable polymers has become widespread in a wide range of industries. This research scrutinized the physical, mechanical, and rheological properties of poly (lactic acid)/poly (ethylene oxide)/carbon nanotube (PLA/PEO/CNTs) blend nanocomposites, as a good candidate for usage in the packaging industry. PEO and CNTs were added at various concentrations to improve the flexibility, toughness, gas permeability, thermal stability, and mechanical properties of PLA via solution blending. Differential scanning calorimetry (DSC), thermogravimetric analysis (TGA), Field Emission Scanning Electron Microscope (FESEM), water contact angle (WCA), rheometric mechanical spectrometer (RMS) test, gas permeability, and tensile characterization were performed to characterize the properties of the prepared blends and nanocomposites. The experimental results revealed that the addition of 25 wt% PEO to the PLA matrix made a partially miscible blend with a droplet‐matrix morphology. PEO at this concentration increased the elongation at break (from 2.2% to 18%) while reducing the modulus (from 25 to 6 MPa). Also, the experimental results indicated that the miscibility of PLA and PEO was enhanced by the addition of 1 wt% CNTs to the prepared blend, associated with diminished entropy of mixing in the LCST phase diagram. Theoretical calculations predicted that the CNTs would be localized in the PLA phase which increased the total crystallinity of the sample by 28%, considerably reducing the amount of gas permeation into the nanocomposite. In addition, the introduction of the CNTs to the blend increased the elongation at break and tensile strength by 13% compared to pure PLA and lowered the rate of thermal degradation effectively. Also, the final results showed that the COOH‐CNTs located in the PEO phase caused a decline in the crystallinity and an increase in the gas permeability of the prepared nanocomposite.Highlights Improvement of physical properties of PLA by blending with PEO and CNTs. A deep investigation on rheological behavior of the prepared nanocomposite. Increasing the crystallinity degree of PLA/PEO blend by adding CNTs. Improvement of the miscibility between PLA and PEO in the presence of CNTs. Controlling the CNTs localization by surface modification.

Incommensurately Modulated Cu0.9Pb1.2Sb2.9Se6 in the Lillianite Structure Type.

Samples with the nominal composition Cu0.9Pb1.2Sb2.9Se6 mainly contain a phase with incommensurately modulated lillianite-type structure with the respective composition. Single crystal diffraction with synchrotron radiation enabled a detailed refinement using the superspace group Cmcm(α00)00s with lattice parameters a = 4.16537(5), b = 14.0821(2), c = 19.8234(3) Å, and a modulation vector q = 0.6890(2)a* at room temperature. The structure is built up from tilted and distorted NaCl-type slabs that are interconnected by bicapped trigonal prisms, which mainly host Pb atoms, according to a 4L arrangement. Satellites up to the second order reveal positional and occupational modulation that mainly involves a sequence of Sb and Cu atoms and allows the Se substructure to adapt in a way that Sb and Cu feature predominantly octahedral and tetrahedral coordination, respectively. Above 523 K, satellite reflections disappear, and the crystal structure becomes more disordered with average coordination spheres of both Sb and Cu atoms corresponding to distorted octahedra. This phase transition leads to discontinuities in the evolution of lattice parameters and physical properties as functions of temperature. HRTEM investigations corroborate centrosymmetry and highlight atoms that are strongly affected by the modulation. Measurements of transport properties reveal a p-type semiconductor with a thermoelectric figure of merit up to 0.1 at 623 K. In accordance with B factor analysis, a small amount of substitution could increase zT significantly by optimizing the carrier concentration.

Microstructure evolution of porous calcium hexaluminate compacts during first heating

Porous calcium hexaluminate (CaAl12O19 or CA6) structures show long-term stability at high temperatures, high refractoriness, low thermal conductivity, and excellent chemical resistance, thus being Taylor-made for thermal insulation. Previous works attained porous structures from in situ formation of CA6 combining CaO and Al2O3 sources in solid-state reactive sintering. Although the approach is time-and-energy-saving regarding the production of large parts of complex shapes, it faces considerable difficulties related to the expansive formation of calcium aluminates. To overcome such drawbacks, pre-formed porous CA6 aggregates improve the system's dimensional stability before sintering. Despite the straightforward processing, few studies have investigated such materials systemically. This article addresses the combination of pre-formed porous CA6 aggregates and organic and inorganic binders for the production of porous structures by two shaping processes, namely, uniaxial pressing and direct casting of aqueous suspensions. After drying, the samples' microstructure and physical properties evolution were investigated up to sintering (1100-1500 °C) through total porosity, Young's modulus, compression strength, pore diameter, and thermal conductivity measurements, dilatometric analyses, and scanning electron microscopy. Reference samples of coarse calcined alumina were tested under the same conditions to highlight the impacts of CA6 particles' morphology. Compared to them, the CA6-containing samples showed almost no variation in total porosity and average pore size levels during thermal treatments, although their strength and rigidity increased significantly after sintering. Their microstructure remained practically unchanged after drying, showing clusters of large asymmetrical CA6 crystals bonded to each other by their edges, and surrounding a large fraction of 1.8–2.2 μm pores. According to the results, although water content, processing method, and compacting levels are important parameters, particles' microstructure, ratio of intra-particle pores, and asymmetrical shape are key variables for the development of physical properties. Such characteristics strongly contributed to their densification resistance and lower thermal conductivity after exposure to high temperatures.

Effects of temperature and charged vacancies on electronic and optical properties of β-Ga2O3 after radiation damage.

β-Ga2O3 as an ultra-wide bandgap material is widely used in space missions and nuclear reactor environments. It is well established that the physical properties of β-Ga2O3 would be affected by radiation damage and temperature in such application scenarios. Defects are inevitably created in β-Ga2O3 upon irradiation and their dynamic evolution is positively correlated with the thermal motion of atoms as temperature increases. This work utilizes first-principles calculations to investigate how temperature influences the electronic and optical properties of β-Ga2O3 after radiation damage. It finds that the effect of p-type defects caused by Ga vacancies on optical absorption diminishes as temperature increases. The high temperature amplifies the effect of oxygen vacancies to β-Ga2O3, however, making n-type defects more pronounced and accompanied by an increase in the absorption peak in the visible band. The self-compensation effect varies when β-Ga2O3 contains both Ga vacancies and O vacancies at different temperatures. Moreover, in the case of Ga3- (O2+) vacancies, the main characters of p(n)-type defects caused by uncharged Ga0 (O0) vacancies disappear. This work aims to understand the evolution of physical properties of β-Ga2O3 under irradiation especially at high temperatures, and help analyze the damage mechanism in β-Ga2O3-based devices.

Diesel soot combustion in air-NO environment: Evolution of soot physical properties and fragmentation characteristics

Since the oxidation activity of nitrogen oxides on soot is obviously higher than that of O2, it is one of the most effective means to improve soot combustion in diesel particulate filter (DPF) by fully utilizing the oxidation activity of nitrogen oxides in diesel exhaust. This paper investigated the physical properties (i.e. morphology, primary particle diameter, fractal dimension and nanostructure) and oxidation-induced fragmentation characteristics of diesel exhaust soot particles during oxidation degrees (0 %, 20 %, 50 % and 80 %) in different atmospheres (air, air-1000 ppm NO and air-2000 ppm NO). The results showed that during the oxidation process the variation trends of soot morphology in air and air-NO environments were similar, while the number and size of primary particles in an aggregate decreased and the fractal dimension of the aggregate increased with the presence of NO in air atmosphere. With the progress of oxidation, the nanostructure of soot particles became more ordered, while this variation trend was slowed down when NO was added to the air atmosphere. This is because soot particles oxidized in air-NO atmospheres showed less probability of internal oxidation but more external oxidation than those in air atmosphere. Over the oxidation process, the soot aggregate fragmentation rate presented a decreasing variation trend under each oxidizing atmosphere, with a higher aggregate fragmentation rate and more apparent variations in air-NO atmospheres. Moreover, in the air atmosphere, the probability of primary soot particle fragmentation showed a consistent upward trend, while the addition of NO slowed down this trend and showed an upward trend in stages 1(0 % ∼ 20 %) and 2(20 % ∼ 50 %), but a downward trend in stage 3(50 % ∼ 80 %). This suggests that the addition of NO reduces the probability of oxidants (especially O2) entering the particles, which would lead to a decrease in the probability of primary soot fragmentation caused by internal oxidation.

Evolution of Physical and Mechanical Properties of Granite after Thermal Treatment under Cyclic Uniaxial Compression

The combined effects of thermal and cyclic loading result in complex mechanical behavior in engineering rock masses. The study of the physical and mechanical properties of these rock masses is of great importance for improving the stability and sustainability of structures built on thermally treated rock masses. In order to understand the failure mechanism, uniaxial compression tests and cyclic loading and unloading tests were conducted on granite specimens that had undergone thermal treatment at various temperatures. The test results indicate that the density and P-wave velocity of the specimens decrease while the degree of damage increases after thermal treatment. The compressive strength and elastic modulus of the specimens generally decrease as a result of thermal treatment, although thermal hardening does occur within the temperature range of 200–400 °C. The dilatancy characteristics of the specimens change with the treatment temperature, and they are more prone to shear dilation under external loading. Furthermore, the failure mode of the specimens transitions from brittle to ductile failure as the treatment temperature increases. The combination of thermal treatment and cyclic loading causes the rock fragments to become looser and finer following specimen failure.

Evolution of Meteosat Solar and Infrared Spectra (2004–2022) and Related Atmospheric and Earth Surface Physical Properties

The evolution of atmospheric and Earth surface physical properties over a period of 15 years (based on data from the longer period from 2004 to 2022) is analyzed through the radiance fluxes measured by the Meteosat second generation (MSG) satellite series. The results show significant changes in the solar (−2.6% to −1.2%) and infrared (+0.4% to +1.0%) domains, with −3.9% for the CO2 absorption band (near 13.4 µm), all variations consistent with results from similar studies of radiation fluxes. Whereas the variation at 13.4 μm radiation is explained by the increase in the CO2 concentration in the atmosphere, the flux increase towards the satellite in the remainder of the infrared spectra measured by MSG corresponds to surface warming (as documented in external sources like the IPCC, the Intergovernmental Panel on Climate Change). The solar outgoing flux decrease exposes a recent reduction in the Earth’s cloud cover under the nominal field of view of Meteosat at 0 degrees longitude (MFOV). Radiance evolution at 6.2 µm and 7.3 µm, a spectral region of intense absorption by water vapor, is interpreted in terms of sensitivity to the humidity content in the middle and upper troposphere by means of a simple radiation transfer model.

Interfacial Interactions of a Myoglobin/DOPC Hybrid System at the Air-Water Interface and Its Physicochemical Properties.

In the present study, the intermolecular interactions between a water-insoluble phospholipid (DOPC) and water-soluble protein (myoglobin) and the interaction among themselves were investigated at the air-water interface using the Langmuir and Langmuir-Blodgett techniques. The effects of changes in physicochemical factors, like pH and temperature, on these interactions were also examined. Surface pressure-molecular area (π-A) isotherms of the DOPC monolayer at the air-water interface, with and without myoglobin (Myo) revealed the evolution of various physical properties, such as elastic, thermodynamic, and hysteric properties, in response to changes in subphase pH and temperature. With the increment of subphase pH from 5 to 7 at a fixed temperature (20 °C), the DOPC isotherm expanded, and the in-plane elasticity (CS-1) decreased, but no significant presence of hysteresis was encountered in either of the pH values. On the other hand, a diminution of temperature (from 20 to 5 °C) leads to an expansion of monolayers yielding low elasticity and significant hysteresis. The incorporation of Myo molecules within the DOPC monolayer decreased the CS-1 value of the DOPC monolayer. Such a decrement in CS-1 was also encountered while increasing the pH and decreasing the temperature (T) of the subphase in the absence of Myo. Systematic expansion of DOPC isotherm and increased hysteric area with the increase in Myo proportion were observed and the atomic force microscopy (AFM) observations suggested a strong conjugation between Myo and DOPC in the mixed monolayer. The denaturation effect of Myo molecules was studied using AFM at different temperatures. Furthermore, the Myo molecules were found to be most surface active at pH = 7, which is very close to its isoelectric point. These observations come up with the interaction mechanism between biomolecules under dynamically varied conditions.

Geomechanical risk and mechanism analysis of CO2 sequestration in unconventional coal seams and shale gas reservoirs

With global greenhouse gas emissions hitting record highs in 2021, CO2 geological sequestration (CGS) is the most realistic and feasible technology to ensure large-scale carbon reduction to achieve global carbon capping and carbon neutrality goals. Both coalbed methane and shale gas have the characteristics of self-generation and self-storage, which is considered to be a valuable target reservoir for geological sequestration of CO2. After a high volume of CO2 is injected into unconventional coal seams and shale gas reservoirs, many geomechanical issues may be induced, resulting in leakage. Therefore, it is crucial to evaluate the geomechanical risks of CO2 geological sequestration. In this article, global CO2 emissions and geological resources available for sequestration are teased out. The effects of coupled CO2-water-rock-driven geomechanical, geophysical, and geochemical interactions on the evolution of rock physical properties and pore characteristics, as well as caprock sealing, are discussed. The caprock failure and its inducing mechanism are analyzed, and the criteria for predicting the occurrence of risk are summarized, which is necessary for pressure management and risk prevention. To serve as a benchmark for CO2 sequestration in unconventional coal seams and shale gas reservoirs.

Crystal Growth and Physical Properties Evolution in Co‐Doped NiTe2 System

Transition metal tellurides have been widely studied for their diverse crystal structures and exotic physical properties such as large magnetoresistance, charge density waves, superconductivity, ferromagnetic and topological properties. NiTe2 has recently been found to be a Dirac semimetal, allowing it to achieve exotic properties by pressure and doping. A series of Ni1−xCoxTe2−δ single crystals are synthesized by the standard solid‐state reaction method. The energy‐dispersive X‐ray spectroscopy and X‐ray diffraction tests confirm Co is successfully doped into the crystal structure. The electrical transport measurements show typical metallic behaviors for all the samples. Magnetization measurements reveal that, in the doping range of x = 0.12–0.62, the samples exhibit a coexistence of antiferromagnetic and paramagnetic phases above the characteristic temperature Tt. By using the combined Curie–Weiss and spin‐wave model, the antiferromagnetic to ferromagnetic transition is found to occur as the temperature drops below Tt. The magnetic transition is attributed to the Te vacancies, which can be explained using the bound magnetic polaritons model. A magnetic phase diagram for Ni1−xCoxTe2−δ system is constructed.

Do Optically Denser Trade‐Wind Cumuli Live Longer?

AbstractThis study investigates the lifetime and temporal evolution of physical properties of trade‐wind cumuli based on tracking individual clouds in observations with the Advanced Baseline Imager aboard the geostationary GOES‐16 satellite during the “ElUcidating the RolE of Cloud–Circulation Coupling in ClimAte” (EUREC4A) campaign east of Barbados in winter 2020. A first application of our upgraded cloud‐tracking toolbox to measurements with high spatio‐temporal resolution (2 × 2 km2 and 1 min) provides probability density functions of lifetime and area of clouds that develop as a consequence of meso‐to‐synoptic scale motions. By separately considering clouds that exist during daytime and live in distinct lifetime intervals, we find that shallow marine cumuli live longer when they cover a larger surface area and show higher cloud optical thickness (COT). Besides the effect of COT, the scale of the atmospheric motions with which the clouds interact is also critical to their lifetime.

Evolution of physical and mechanical properties of fused silica after subsurface damage layer removal by RIE treatment

The subsurface damage of polished fused silica can be removed by various post-treatments to improve the strength of fused silica in high energy laser systems, but the evolution of physical and mechanical properties of fused silica after the removal of subsurface damage remains unclear. In this study, the physical and mechanical properties of fused silica are studied after various depths of subsurface damage removal by reactive ion etching process. The results show that as the etching depth increases, the concentration of metal ions contamination in the subsurface of fused silica decreases significantly, the water contact angle of fused silica decreased, while homogeneity of adsorbed water molecules on fused silica surface increases, especially at higher humidity conditions. Furthermore, the nanohardness and reduced modulus of fused silica increases with the etching depth. These results will be helpful for optimizing the manufacturing and lifetime of fused silica in high energy laser systems.

Pore-scale analysis of hydrate saturation on the physical parameters of hydrate-bearing sediment with different particle shapes

Methane hydrate is the most potential novel energy source with huge reserves to be developed, and is the priority of countries' future energy development strategies. Evaluating the basic physical characteristics of hydrate reservoirs, especially permeability, thermal, and electrical conductivity, is essential for clarifying the main controlling factors of physical characteristics and formulating a reasonable development strategy. Accordingly, 16 cementing hydrate-bearing models with different particle shapes were constructed account of a new three dimensions morphologic modeling algorithm for hydrate in this study. Based on the above models, the evolution of pore space distribution and basic physical properties of hydrate-bearing sediments (HBS) have been analyzed via pore network modeling (PNM) and finite volume method (FVM). The results show that (1) the quantity of pores and throats of HBS with round particles is higher, and the average radius is smaller than those of HBS with irregular particles, (2) increasing hydrate saturation leads to a decrease in absolute permeability, with a more rapid decrease in permeability for HBS with irregular particles, (3) the thermal conductivity of HBS with round particles exceeds those of HBS with irregular particles, and the their curves remain parallel with increasing hydrate saturation, (4) the resistivity index of HBS with round particles increases faster as hydrate forms, and the conductivity is always smaller than those of HBS with irregular particles.

The Evolution of Pore Pressure, Stress, and Physical Properties During Sediment Accretion at Subduction Zones

AbstractWe study stress, pressure, and rock properties in evolving accretionary wedges using analytical formulations and geomechanical models. The evolution of the stress state from that imposed by uniaxial burial seaward of the trench to Coulomb failure within the wedge generates overpressure and drives compaction above the décollement. Changes in both mean and shear stress generate overpressure and shear‐induced pressures play a particularly important role in the trench area. In the transition zone between uniaxial burial and Coulomb failure, shear‐induced overpressures increase more than overburden and are higher than footwall pressures. This rapid increase in overpressure reduces the effective normal stress and weakens the plate interface along a zone that onsets ahead of the trench and persists well into the subduction zone. It also drives dewatering at the trench, which enables compaction of the hanging‐wall sediments and a porosity offset at the décollement. Within the accretionary wedge, sediments are at Coulomb failure and the pore pressure response is proportional to changes in mean stress. Low permeability and high convergence rates promote overpressure generation in the wedge, which limits sediment strength. Our results may provide a hydromechanical explanation for a wide range of observed behaviors, including the development of protothrust zones, widespread occurrence of shallow slow earthquake phenomena, and the propagation of large shallow coseismic slip.

Hydration of Transitional Shale and Evolution of Physical Properties Constrained by Concurrent NMR and Acoustic Observations

Hydration state is a key factor affecting the pore structure and mechanical properties of shale that directly impacts the migration and then production of geofluids. We quantify the impact of the hydration state on physical properties through spontaneous imbibition experiments constrained by concurrent nuclear magnetic resonance (NMR) and acoustic observations as diagnostics of response. The long-duration experiments (24 days) are on samples from the Permian Shanxi Formation of the Ordos Basin, complemented by measurements of composition and physical properties. These shales primarily comprise quartz and clay minerals with intraparticle pores present within the clay minerals. The NMR T2 spectra indicate that mesopores (2–50 nm) comprise ∼80% of the total pore space. The imbibition rate decreases by a factor of 3 from 0.08 g/h to a stable rate of 0.03 g/h from the 1st to the 24th hour. This is accompanied by a 10% decrease in the deformation modulus from 44 to 40.3 GPa over 24 days. The reduction in the modulus is consistent with observations of the shedding and spalling of hydrophilic quartz particles from the unconstrained surface and the generation of fractures. Reduction in the imbibition rate is consistent with the swelling followed by squeezing of clay minerals and the corresponding reduction in pore diameters in the confined core of the sample, together with the reduction in saturation gradients with the progress of imbibition. Understanding the mechanisms and effects of hydration on the pore structure and mechanical properties is important in understanding the shale hydration process and defining diagnostic (acoustic and NMR) signatures that may be used in reservoir surveillance.

Acoustic Emission Characterization Analysis of Quasi-Static and Fatigue Compression Properties of Aluminum Foam

In order to explore the evolution of physical and mechanical properties and acoustic emission (AE) characteristics of aluminum foam under fatigue and quasi-static compression from a microscopic point of view, the AE monitoring technology was used to analyze the deformation, hardening, and energy absorption characteristics of open-cell aluminum foam under quasi-static compression at different rates (2, 10 and 50 mm/min) and fatigue loading tests with different peak stress ratios k (k = maximum stress/yield stress) by means of MTS fatigue testing machine and CCD camera. The results indicated that under different compression rates, the AE ring down count had the same trend as the engineering stress–strain response of the specimens, the AE ring down count rate at the plastic deformation stage showed the same performance as the work hardening rate, and the AE energy absorption efficiency corresponded well to the experimental results. The specimen entered the densification stage with the stability of AE count and the decrease in energy absorption efficiency. During the fatigue tests of different k values, the change trend of strain was consistent with the response of acoustic emission characteristic parameters, and the fatigue compression damage caused by the deformation process of the specimen can be monitored by the change in AE characteristics. The AE characteristics can dynamically monitor the compression process and provide a new research method and idea for the study of mechanical properties of aluminum foam.

Research on floc structure and physical properties based on pipeline flocculation

The flocculation effect of tailings has an important influence on the turbidity of thickener overflow and the solid-liquid separation effect of tailings slurry. However, pipeline flocculation has not been applied to the tailings dewatering in the thickening process of mines. Moreover, previous studies are limited by the size of the experimental device, and the variation of floc structure with settling height during the free settling process in the thickener was insufficient. Therefore, based on a plot thickener with sufficient height (113 cm) and the pipeline flocculation device, the evolution of the structure and physical properties of flocs with settling height can be clearly explored. And the effects of flocculant dosage, tailings slurry concentration, flocculant slurry concentration, and fluid shear gradient on floc structure, physical properties, and supernatant turbidity in pipeline flocculation were studied. The evolution of floc size and physical properties with settling height in thickener with or without shear was also analyzed. The results show that when the flocculant dosage is 90 g·t−1–105 g·t−1, the concentration of tailings slurry is 20 wt% ~ 25 wt%, the concentration of flocculant solution is 0.005 wt% ~ 0.01 wt%, and the fluid shear gradient is 29.2 s−1–48.7 s−1, the tailings particles are fully mixed with the flocculant solution. Which effectively reduces the turbidity of the overflow. The flocs were broken during the settling process. Accordingly, the floc size and settling velocity decreased with the decrease in settling height, and the density and strength of flocs increased with the decrease in settling height. The reasonable control of the shearing speed of the rake can improve the settling velocity of flocs, which is beneficial to the solid-liquid separation of thickening. Through the research of this study, a method of thickening and dewatering mine tailings slurry through pipeline flocculation was proposed. The variation law of floc structure in the process of free settling in thickener was explored, which provided a reference for the rapid solid-liquid separation of tailings slurry in the thickener.