The sedimentation of spherical-particle aggregations is the common phenomenon in natural world. However, the related research is quite limited. In this study, the spherical particles with four different densities and three diameters were first used for preparing aggregations with two, three and four particles, respectively. And then the final settling velocity of the aggregations was measured using a visual vertical pipe column. It was found that the final settling velocity would increase with the density and the diameter of the unit particle, which is well in agreement with the Stokes’ theory. Furthermore, the geometry arrangement of the particles can also affect the settling velocity significantly, but no model available to consider its influence. With the increase of particle number, the final velocity presents increase tendency.