Percentage Of Content Research Articles

Is It True That More Than Half of Web Contents Are in English? Not If Multilingualism Is Paid Due Attention!

The belief that English is and will remain largely dominant as the first language of the Internet in terms of content and is the natural lingua franca in cyberspace plays against the mobilization of human and funding resources to incorporate minority languages. We sustain that this belief stands on biased data and that multilingualism is more and more the nature of the Internet and translation its lingua franca. We challenge the validity of a source widely used, since 2011, to state that English represents a steady percentage of web contents over 50%. This business source, W3Techs, is well-famed and considered reliable for its surveys on web technologies, exploring a large sample of the Web. However, languages differ from other web technologies, in the fact than more than one language could be used on a website. Not taking into account the multilingual nature of the Web is a serious bias that leads to major errors. The study of the rate of multilingualism of the sample of websites used by W3Techs concludes that the percentage of English contents on the Web is within a 20%–30% range, a value coherent with the results from three referenced alternative methods. We plan for 2025 to create a tool for measurement of languages and rate of multilingualism in a series of websites, with thorough attention to list all the languages used within a website, a complex matter. This tool will be applied to the same sampling and should close definitively this matter.

Spatial Variability in the Speciation of Lead (Pb) and Other Metals Across Urban Lawns Is Linked to Post-Deposition Weathering Reactions

The historical use of lead (Pb) poses ongoing health risks via exposure to contaminated urban soils. However, there is limited information about heterogeneity in Pb speciation and distribution at the house lot scale. This study determined highly spatially resolved Pb and other metal speciation along horizontal transects and vertical soil cores from three homes in the Akron, Ohio (USA) municipal. Solid phase characterization was coupled with a sequential extraction protocol to determine operationally defined speciation (exchangeable (MEX), reducible (MRED), oxidizable (MOX), and residual (MRES)). Lead and Zn were strongly correlated across all fractions (R2 = 0.92). Total extractable Pb and Zn were found in low weight percent concentrations nearest to the homes, and speciation was dominated by MEX and MRED. High Pb in the MEX fraction was correlated with the presence of Pb-bearing paint chips in the soil. Lead in the MEX fraction in soils near the homes decreased with increasing time due to exterior renovations coupled with increases in Pb and Zn in the MRED fraction. These results suggest that homes are the dominant source of Pb and Zn due to the weathering of exterior surfaces and highlight the acute risk of exposure to more labile Pb immediately following exterior renovations and damage to home exteriors in areas of older housing stock.

Foliar Application of Methyl Jasmonate and Chitosan Improve Growth, Yield, and Quality of Guar (Cyamopsis tetragonoloba L.) Under Water-Deficit Stress

Guar (Cyamopsis tetragonoloba L.), a summer legume, is becoming increasingly important as an industrial crop due to its high gum and viscosity content. This study investigated the effects of methyl jasmonate (MeJA), chitosan (CH), and their combination on the growth, yield, and quality of guar under irrigation regimes. A greenhouse experiment was conducted using a factorial design to evaluate the effect of foliar spraying with MeJA (5, 25, and 50 µM), CH (100, 150, and 200 mg/L), their combination (25 µM MeJA + 150 mg/L CH), and control on two commercial guar varieties (RGC-986 and BR-2017) under different irrigation regimes (100%, 70%, and 40% field capacity). The results showed that the exogenous application of MeJA and CH, individually and in combination, significantly enhanced various morphological traits and yield components in guar, including plant height, pod characteristics, seed yield, and root development. Additionally, the combination treatments improved seed quality parameters, such as gum percentage and viscosity content. Leaf analysis revealed increased levels of total phenolic content, total flavonoid, and anthocyanin contents. The BR-2017 variety showed superior performance in most morphological and qualitative traits, demonstrating greater resistance to irrigation regimes. It maintained yield and quality characteristics under water-deficit conditions, particularly when treated with 25 µM MeJA and 150 mg/L CH. The highest gum percentage (33.67%) and viscosity (4768.5 cP) were observed in the RGC-986 variety, along with enhanced levels of secondary metabolites. This study provides new insights into how MeJA, CH, and their combination can improve the yield and quality of guar under water deficit stress conditions. The results suggest that the use of these elicitors, especially in combination, represents an innovative strategy for improving guar production and quality, with potential variety-specific responses to water-deficit stress.

Glutamate increases the lean percentage and intramuscular fat content and alters gut microbiota in Shaziling pigs

This study aimed to explore the effects of glutamate (Glu) supplementation on the growth performance, carcass traits, meat quality, composition of amino acids and fatty acids in the longissimus dorsi muscle, and the colonic microbial community of Shaziling pigs. A total of 48 healthy male Shaziling pigs (150 d, 31.56 ± 0.95 kg) were randomly assigned to two groups, and fed a basal diet with no supplement (control group) or supplemented with 1% Glu (Glu group) for 51 d, and 6 pigs per group were finally slaughtered. Glu significantly increased the average daily gain (P = 0.039), lean percentage (P = 0.023), and intramuscular fat (IMF) content (P = 0.015), and decreased the fat percentage (P = 0.021) of Shaziling pigs. In the muscle, Glu increased the concentrations of inosine-5’-monophosphate (P = 0.094), Fe (P = 0.002), Cu (P = 0.052), and monounsaturated fatty acids (MUFAs) (P = 0.024), and decreased the content of C18:2n6 (P = 0.011), n6 polyunsaturated fatty acids (n6 PUFAs) (P = 0.014), and PUFAs (P = 0.014). Moreover, Glu significantly upregulated the mRNA expression of adipogenesis-related genes (FAS, SREBP-1C) (P = 0.032, P = 0.026) and muscle growth-related genes (MyHCⅡb, MyHCⅡx) (P = 0.038, P = 0.019) in the muscle, and increased the relative abundance of Spirochaetota (P < 0.001) and the acetic acid content in the colon (P = 0.039). Correlation analysis indicated that the acetic acid content was positively correlated with the relative Spirochaetota abundance and the IMF content, and a negative trend with the fat percentage of Shaziling pigs. In conclusion, these results indicated that Glu could simultaneously increase the lean percentage and IMF content and decrease the fat percentage of Shaziling pigs, and these beneficial effects may be related to increased colonic Spirochaetota abundance and acetic acid concentrations.

The addition of humic acid into soil contaminated with microplastics enhanced the growth of black gram (Vigna mungo L. Hepper) and modified the rhizosphere microbial community.

Microplastics have polluted agricultural soils, posing a substantial risk to crop productivity. Moreover, the presence of microplastic pollution has caused a disturbance in the composition of the microbial community in the soil surrounding plant roots, therefore impacting the growth of beneficial bacteria. A study was conducted to examine if humic acid (HA) can counteract the harmful effects of microplastics (MPs) on the growth of black gram crops and the composition of the rhizosphere soil microbial community, to reduce the negative impacts of microplastics on these microorganisms and crops. The research was carried out using mud pots and the plastic utilized for the experiment consisted of 60% high-density polyethylene (HDPE) and 40% polypropylene (PP). The soil was enriched with lignite-based potassium humate, which had a pH range of 8.0-9.5 and with 65% humic acid. The experiment consisted of six treatments: T1, which served as the control without HA and MP; T2, which involved the use of HA at a concentration of 0.15% w/w; T3, which involved the use of MP at a concentration of 0.2% w/w; T4, which involved the use of MP at a concentration of 0.4% w/w; T5, which involved the combination of HA at a concentration of 0.15% w/w and MP at a concentration of 0.2% w/w; and T6, which involved the combination of HA at a concentration of 0.15% w/w and MP at a concentration of 0.4% w/w. The plant growth characteristics, including germination percentage, nodule number, and chlorophyll content, were measured. In addition, the DNA obtained from the rhizosphere soil was analyzed using metagenomics techniques to investigate the organization of the microbial population. Seedlings in soil polluted with MP exhibited delayed germination compared to seedlings in uncontaminated soil. Following 60days of growth, the soil samples treated with T5 (0.2% MP and 0.15% HA w/w) had the highest population of bacteria and rhizobium, with counts 5.58 ± 0.02 and 4.90 ± 0.02CFUg-1 soil. The plants cultivated in T5 had the most elevated chlorophyll-a concentration (1.340 ± 0.06mgg-1), and chlorophyll-b concentration (0.62 ± 0.02mgg-1) while those cultivated in T3 displayed the lowest concentration of chlorophyll-a (0.59 ± 0.02mgg-1) and chlorophyll-b (0.21 ± 0.04mgg-1). Within the phylum, Proteobacteria had the highest prevalence in all treatments. However, when the soil was polluted with MPs, its relative abundance was reduced by 8.4% compared to the control treatment (T1). Conversely, treatment T5 had a 3.76% rise in relative abundance when compared to treatment T3. The predominant taxa found in soil polluted with MP were Sphingomonas and Bacillus, accounting for 19.3% of the total. Sphingomonas was the predominant genus (21.2%) in soil polluted with MP and supplemented with humic acid. Humic acid can be used as a soil amendment to mitigate the negative effects of MPs and enhance their positive advantages. Research has demonstrated that incorporating humic acid into soil is a viable method for maintaining the long-term integrity of soil's physical, chemical, and biological characteristics.

The Flexural Behavior of Reinforced Ultra-High Performance Engineering Cementitious Composite (UHP-ECC) Beams Fabricated with Polyethylene Fiber (Numerical and Analytical Study)

Ultra-high performance engineered cementitious composite (UHP-ECC), which is a new and ductile version of concrete, has attracted researchers recently due to its exceptional mechanical properties: its very high compressive strength (from 100 to 200 MPa) and very high tensile strain capacity (not less than 3% and up to 8%). However, the available experimental literature is small due to its very high cost. To overcome the high cost of the experiments of UHP-ECC, the finite element modeling package ANSYS was used to create a new modeling technique using the Menetrey–Willam constitutive model, recently added to ANSYS. This technique was validated using previous experimental results for UHP-ECC beams and found to be accurate and effective. The previous FE model was used to conduct a parametric study and the variables—the compressive strength of the concrete, the percentage of the volume content of polyethylene fibers, the tensile reinforcement ratio, and the span-to-depth ratio—were found to be effective upon the flexure behavior of the reinforced UHP-ECC beams. As the analysis and design of UHP-ECC beams fabricated with polyethylene fiber are not available yet through design codes, an analytical model including some equations was deduced to calculate the flexure capacity of such beams. The results of the parametric study were used to investigate the validity and accuracy of the analytical model. The proposed equations demonstrated a good estimation compared with the numerical analysis results.

Mechanical strength analysis of bio composite made by using micro powder made of Prosopis cineraria wood

The Present study examines the mechanical strength of bio-composites fabricated from wood powder of Prosopis cineraria (Khejri) and jute fiber as reinforcement inside an epoxy resin matrix. The mechanical performance of these bio-composites was assessed by altering filler content percentages (0%, 4%, 8%, 12%, 16%, and 20%) and filler particle sizes (250 microns and 500 microns) under standard and carbonate conditions. Tensile strength and impact energy assessments were performed to evaluate the effects of filler content, particle size, and filler type on the mechanical characteristics of the composites. The tensile strength tests reveal that composites with 12% filler and a particle size of 250 microns had the maximum tensile strength, measuring 33.4 MPa under normal settings and 34.8 MPa under carbonate conditions. An increase in filler content over 12% resulted in a reduction in mechanical strength due to filler agglomeration, which decreased stress transfer efficiency. The composites with 250-micron particles consistently demonstrated superior tensile and impact strengths compared to those with 500-micron particles, due to the increased surface area of the smaller particles. Comparative analysis of normal and carbonate conditions demonstrated that carbonate fillers offered superior reinforcement owing to their increased density and enhanced matrix-filler interaction, leading to augmented tensile and impact strength. These findings provide significant insights into the development of bio-composites for structural applications, namely in improving their mechanical strength and durability.

Fabrication of Zinc(II) Mediated Poly(Acrylamide Co Acrylic Acid) Hydrogel with Thixotropic and Tribological Properties.

Hydrogels have emerged as promising candidates for biomedical applications, such as replacing natural articular cartilage, owing to their unique viscoelastic properties. However, sufficient mechanical properties, self-healing ability, and adhesive nature are some issues limiting its application window. Here, a facile one-pot synthesis of dual cross-linked zinc-coordinated copolymer hydrogels is presented. The network structure of the copolymer hydrogels is strategically developed via dynamic and reversible physical cross-linking by Zn2+ ions and simultaneous covalent cross-linking through a covalent cross-linker viz methylene bisacrylamide. Fourier-transform infrared (FTIR), X-ray diffraction (XRD) scanning electron microscopy (SEM), and Brunauer-Emmett-Teller (BET) analysis have thoroughly characterized the structure of the synthesized hydrogels. The introduction of Zn2+ offers dynamic and reversible complexation, leading to excellent mechanical properties and self-healing features. Moreover, the percentage of the equilibrium water content of zinc-coordinated copolymer hydrogel samples is comparable with that of natural articular cartilage. The Shear sliding study shows the dominant adhesive behavior of HGel-Zn(NO3)2 sample compared to the parent HGel sample. This facile dual cross-linked hydrogel, HGel-Zn(NO3)2, with a combination of good mechanical properties, efficient self-recovery, adequate water content, and favorable adhesive nature, seems very promising to mimic the articular cartilage.

Enhancing burning rate of ammonium nitrate by ammonia borane: Mechanism from reactive molecular dynamics simulation.

The development of ammonium nitrate (AN)/ammonia borane (AB) as a green propellant is crucial for their applicability in different engines. This study investigates the release patterns of small products, particularly nitrogen-containing molecules, during the initial pyrolysis of AN/AB at low and high pressures using ReaxFF MD simulations. Compared with pure AN, the addition of AB gives the hybrid system enhanced reactivity, leading to faster decomposition and higher energy release. The results show that the consumption of AN in the S13 system (AB with a mass ratio of 12.6 %) is accelerated at 1.47 MPa. NO2 and NO are produced through HNO3 and NO3. At 6.89 MPa, AN exhibits the fastest decomposition rate in the S15 system. The high pressure enhances more reactions of NO with free radicals such as NH and accelerates the release of N2. As the percentage content of AB increases to 15.3%, more H2O while more NO2 is generated. The effect of AB on the generation of radicals such as H2 and H, is analyzed. AB not only promotes the initial pyrolysis of AN but also accelerates the conversion of intermediates.

Influence of Al2O3 and h-BN on Wear and Corrosion Performance of IN625 Nickel-Based Coating

IN625 offers high-temperature oxidation resistance, wear resistance, and stable chemical properties. To improve the corrosion and wear resistance of the Q345B steel surface, two types of metal matrix composites (IN625 + 1% Al2O3 and IN625 + 1% h-BN) were applied to the substrate surface using the laser cladding process. This study analyzed the hardness, electrochemical corrosion, friction, and wear properties of both the laser-clad specimens and the substrates. The results show that (1) the hardness and wear resistance of the fusion-coated coating were significantly improved compared with the base material. Notably, the hardness increased by 19%, and the coefficient of friction decreased by 41% compared with the IN625 + 1% h-BN coating. Furthermore, the hardness and wear resistance of the IN625 + 1% h-BN coating were superior to those of the IN625 + 1% Al2O3 coating, attributed to the formation of eutectic compounds such as NiB and Ni2B in the dendritic region. (2) The corrosion resistance of the IN625 + 1% Al2O3 coating exceeds that of the IN625 + 1% h-BN coating and is also superior to that of the substrate. This improvement is primarily attributed to the addition of Al2O3, which enhances solid solution strengthening within the dendritic crystals of the fused-coating layer, reduces the percentage content of inclusions, and elevates the corrosion resistance of the coatings.

Studies on Dry Sliding Wear Mechanisms of Al7075/Si3N4 Composites

Abstract In this investigation, Al7075 aluminum alloy reinforced with Si3N4 particles (3, 6, 9, and 12 wt%) was used as reinforcements to manufacture composites through a stir-casting approach. The microstructural characteristics have shown significant grain refinement owing to the presence of Si3N4 particle distribution during the solidification. SEM micrographs confirm the uniform distribution of Si3N4 particles with considerably fewer particle agglomerations throughout the matrix alloy. The reinforcement particle cluster formation is relatively increased for increasing the Si3N4 content. The SEM and EDS analyses showed good integrity at the matrix–refinement interface with no interfacial compound formation. The mechanical properties, such as hardness (up to 118 BHN), tensile strength (up to 281 MPa), and yield strength (up to 178 MPa), were enhanced by 30.69% and 20.27%, respectively. The wear-rate and coefficient of friction of the composites were evaluated with increasing percentages of Si3N4 content. The average wear-rate of the composites is 0.019, 0.0085, 0.0075, and 0.0065 mm3/m, respectively, for the increased Si3N4 ceramic particulate content from 3 to 12 wt%, while the average COF of the composites is 0.45, 0.37, 0.32 and 0.28 respectively. With the addition of Si3N4 particulate content, the wear resistance performance of the composites at 30 N has shown up to 46% enhancement and increased from 0.0052 to 0.0103 mm3/m with the increasing sliding velocity from 1.5 to 3.5 m/s for varying Si3N4 particulate content from 3 to 12 wt%, while reducing the COF up to 65%, and from 0.43 to 0.27. Different wear mechanisms are characterized by identifying the typical features of wear on the SEM micrographs of the worn surfaces. The dominant wear mechanisms of the composites are typically observed as abrasion, oxidation, delamination and melt wear. The mechanism and behavior of composites under dry sliding conditions are analyzed through the construction of wear maps. The windows of wear mechanisms and progression in terms of load and sliding velocity for the composites with various wt% of Si3N4 content were identified, analyzed, and presented.

The effect of multi-step cycles on the surface properties of Ni-TiO2 coatings produced by pulse current electrodeposition

ABSTRACT In this study, the Ni-TiO2 coatings were deposited on copper substrates by pulse plating. The effect of multi-step current cycles on the metallurgical properties of produced coatings was investigated. The results showed that the values of applied currents within the periods significantly affect the surface properties of all coatings. Using the negative current cycles, the surface morphologies completely changed from regular and compact to irregular, compared to the deposits that did not have a negative cycle in the coating process. Also, the surface roughness increased by 1.5 times in the best case. Applying the 8-step cycle increased the percentage of TiO2 content inside the Ni-TiO2 layer from 13.13 vol.% to 31.58%. The corrosion and wear analysis results showed that the coating applied by a 4-step cycle with a 90-second off time has the best properties. Therefore, the corrosion and wear properties were not necessarily directly related to the participation percentage of TiO2 particles. Compact morphology with high current efficiency, wide distribution of TiO2 particles (6.31 vol.%) with minimal agglomeration, low coating roughness (Ra = 0.32 µm), high hardness value (436 Vickers), and the participation of (111) plane in the preferred texture improved the corrosion and wear behaviour of the optimal coating.

Effect of pullulan and pullulan-chitosan composite coating on the antioxidant activity, texture, color and shelf-life of a local cultivar of sweet cherry

This study explored the effects of pullulan and pullulan-chitosan composite edible coatings on the post-harvest quality of sweet cherries over 20 days of storage. We evaluated weight loss, total soluble solids (TSS), decay percentage, color value, texture and biochemical content, including ascorbic acid, total phenolic content (TPC), flavonoids, anthocyanins, antioxidant activity and enzyme activity. The results revealed that cherries with 3 % pullulan coating presented the lowest weight loss (25 % vs 26.33 % in the control) and decay percentage (25 % vs 47 % in the control) and maintained superior texture and stability compared with those of the control and other coatings. TSS increased less in the coated cherries than in the control cherries, with 3 % pullulan-treated cherries showing the least increase, indicating slower ripening. Pullulan coatings effectively reduced color changes, with the 3 % coating delaying darkening in cherries more than the other treatments did. Additionally, the pullulan coating preserved higher levels of ascorbic acid, phenolic compounds (TPC) and flavonoids and delayed the decrease in antioxidant activity. Notably, the 3 % pullulan-treated cherries maintained the highest antioxidant activity (88.97 %) and had the greatest TPC (2.79 mg GAE/g FW) at the end of storage. The activity of enzymes, particularly peroxidase (POD), increased less in coated cherries, highlighting the role of coatings in delaying oxidative stress. Overall, the pullulan coatings, especially at a 3 % concentration, were the most effective at extending the shelf-life and maintaining the quality of the sweet cherries. These findings suggest that the use of a pullulan-based coating is a promising approach for preserving fruit quality during storage, thereby extending shelf-life. These coatings can contribute to a reduction in food waste, improved consumer acceptability and improved economic gains by reducing postharvest losses and maintaining quality. To optimize pullulan-based coatings for commercial application, future research can focus on optimizing the formulation, consumer acceptability and scalability. Moreover, field trials to assess the effectiveness of these coatings in preserving the quality of cherry can be performed. By addressing these areas, future research can contribute to the development of sustainable options for preserving the quality and extending the shelf life of sweet cherries and other fruits.

Nutrient content of tamarind seed hydroponic fodder due to different watering frequencies

Limited feed for pigs encourages using alternative feed such as tamarind seeds using hydroponic fodder technology. The research aimed to examine the nutrient content of tamarind seed hydroponic fodder due to different watering frequencies. The research was conducted in Kolhua Village, Kupang City from April-September 2023. The research used tamarind seeds originating from the Lembata city. The research used a Completely Randomized Design, with 3 watering frequency treatments, namely R0 = 1 watering (07.00 WIT), R1 = 2 times (07.00 and 19.00), R2 = 3 times (07.00, 15.00 and 23.00 Wita) and 8 repetitions. There were 100 seeds per container. Variables include tamarind seed fodder's nutrient content (organic matter, crude protein, crude fiber, crude fat, and ash). Analysis used Analysis of Variance and Duncan's advanced test. The research results showed that watering frequency had a very significant effect (P&lt;0.01) on the nutrient levels of tamarind seed hydroponic fodder except for ash content and the watering frequency that produced the best nutrient levels was twice/day. In conclusion, the germination percentage and nutrient content of tamarind seed hydroponic fodder are influenced by watering frequency twice/day with 30 ml being the best frequency.

Effect of a Bacillus subtilis-based direct-fed microbial, on milk yield, milk components, feed intake and plasma hormones and metabolites in lactating Holstein cows

To investigate the effects of a Bacillus-based direct-fed microbial on milk production and related factors, a study was conducted on Holstein cows (n = 28) starting at 90 ± 11 DIM. The cows were divided into two dietary groups: a control group (CON) that received a total mixed ration (TMR), and a Bacillus-fed group (DFM) that received the same TMR along with a Bacillus subtilis product containing two strains (747 and 1781) in equal amounts. The study lasted for 25 wk and included both primiparous and multiparous cows. The cows were housed in a free-stall barn and were provided with ad libitum TMR, which was fed twice a day. Their daily meals and dry matter intake (DMI) were recorded during wk 1–4 and wk 19–25 using electronic feeders. Milk samples were collected weekly during morning and evening milkings and analyzed for milk fat, protein, lactose, and milk urea nitrogen (MUN). Blood samples were also collected weekly and analyzed for plasma glucose, insulin, cholesterol, insulin-like growth factor 1 (IGF1), and progesterone concentrations. Additionally, rumen fluid samples were collected and evaluated for various species of bacteria. One of the key findings was that daily 4 % fat-corrected milk production (FCM) was influenced by the interaction between treatment (DFM vs. CON) and parity (primiparous vs. multiparous), with multiparous DFM cows producing 11 % more FCM compared to CON. The DFM cows also had a higher milk fat percentage (4.41 % vs. 4.02 %) and MUN concentrations were 1.0 mg/dL higher in the DFM group. In terms of blood metabolites and hormones, multiparous DFM cows had lower plasma cholesterol, glucose, and insulin concentrations compared to CON multiparous cows. However, there were no significant differences between the groups in terms of plasma IGF1 concentrations, insulin-to-glucose ratios, and luteal phase plasma progesterone concentrations. The analysis of rumen fluid samples revealed that the abundance of Ruminococcus albus and Fibrobacter succinogenes group I was greater in the DFM cows compared to CON cows. Furthermore, during the periods when feed intake was measured, the DFM cows had a 9 % reduction in feed intake and a 14 % improvement in feed efficiency (FCM per DMI) compared to CON cows. In conclusion, the two-strain Bacillus product used in this study (Certillus) showed potential as an effective direct-fed microbial. It was found to increase feed efficiency and milk production by altering the composition of ruminal microbiota and metabolism in the cows.

Impact of Mid-season Moisture Stress on Yield Attributes and Seed Quality in Groundnut Genotypes

A field experiment was conducted at Regional Agricultural Research Station, Tirupati, Acharya N.G. Ranga Agricultural University during rabi, 2022 and 2023 to study the impact of mid-season moisture stress (40-80 DAS) on yield attributes and quality traits of groundnut genotypes. The experiment was carried out in randomized block design with factorial concept with two main treatments i.e., control and mid-season moisture stress (40-80 DAS) and 12 sub treatments i.e., two check varieties and ten contrasting groundnut genotypes in three replications. Among the groundnut genotypes and check varieties tested for their tolerance to moisture stress the genotypes, TCGS 2326, TCGS 1792, K9 and TCGS 2333 were found to withstand mid-season moisture stress and maintained highest 100 kernel weight, shelling percentage, protein and oil content indicating tolerance to moisture stress.

AQbD-guided stability indicating HPLC method for azelnidipine and chlorthalidone fixed-dose combination tablet: a green approach

This study developed a stability-indicating RP-HPLC method for quantifying azelnidipine and chlorthalidone in fixed-dose formulations using Analytical Quality by Design (AQbD) principles. A Plackett-Burman design was used for factor screening, followed by risk assessment and optimization using a central composite design to evaluate the effects of the organic phase percentage, flow rate, and modifier concentration. Acetonitrile percentage was identified as the most critical factor. The optimized method employed a Reliant™ C18 Waters column with a mobile phase of 0.1% formic acid and acetonitrile (62:38% v/v), with chlorthalidone and azelnidipine eluting at 4.1 and 13.7 minutes, respectively. Validation showed the method's robustness, accuracy, and precision. Forced degradation studies confirmed its reliability for tablet formulation analysis, and an Analytical Greenness score of 0.55 highlighted its environmental sustainability. This method is efficient, simple, and well-suited for routine quality control in the pharmaceutical industry.

Dynamic Constitutive Model of Tungsten‐Whisker‐Reinforced Aluminum/Polytetrafluoroethylene Composite Material and Quantitative Determination of Impact Reaction Release Energy in Vacuum Environment

To meet the strength requirements of aluminum/polytetrafluoroethylene (Al/PTFE) in practical applications, tungsten (W) whisker is added into the traditional formula Al/PTFE (26.5%/73.5%) to improve the dynamic compressive strength of the reactive material. Mechanical properties of reactive material specimens prepared by sintering are tested. In the results, it is shown that the dynamic compressive strength of Al/PTFE‐reactive material reinforced by tungsten whisker with volume fraction of 13.1% can reach 141 MPa at strain rate of 1800 s−1. The constitutive model of dynamic compression for tungsten‐whisker‐enhanced Al/PTFE‐reactive material is constructed, and the results are basically consistent with the experimental results. The quantitative impact energy release of reactive material specimens under vacuum environment are performed by using the two‐stage light gas gun loading system, and the quantitative impact release energies of Al/PTFE‐reactive material reinforced by tungsten whisker under different whisker percentage content and diameter are obtained.

Organoleptic Evaluation of Aonla (Emblica officinalis G.) Nectar during Storage

A research experiment was conducted during the year 2019-20 and 2020-21 in the Fruit and Vegetable Processing Unit Laboratory, Department of Horticulture, College of Agriculture, Gwalior with seven different varieties of aonla viz., NA-4, NA-5, NA-6,NA-7, NA-10, Laxmi and Chakaiya. This study was carried out in a completely randomized design with three replications. It was studied about the preparation of various value added products such as aonla nectar. From the finding it was observed that, the increase in the percentage of acidity, moisture, phenols and fiber content of aonla nectar while total soluble solids and total sugar content was decreased. There was gradual increase in moisture content of aonla nectar prepared with different pulp combination of aonla fruits during storage period. However, total soluble solids, ascorbic acid content decreased with advancement of storage period. Observations were recorded up to storage period of six months at ambient conditions. Laxmi and Chakaiya varieties were found superior with respect to colour, appearance, taste and aroma as well as flavour. As per the organoleptic evaluation the overall acceptability of anola nectar was found significant with the storage intervals of 30, 60, 90 and 120 days.

Volatile, glycerides, tocopherol, phytosterols, and triterpene alcohol in 31 commercial walnut oils from three countries

Walnut oil, well-known for its nutritional value, is a promising source of healthy lipids. This study assessed the physicochemical properties and levels of volatile compounds, glycerides, tocopherol, phytosterols, and triterpene alcohol in 31 commercial walnut oil samples from different countries: China (with 27 samples), France (with 3 samples), and Germany (with 1 sample). The percentage content of unsaturated fatty acids in walnut oils exceeded 90 %. A total of 93 volatile compounds were identified, and the corresponding concentrations ranged from 28.02 to 528.37 mg/L, including 22 aldehydes, 14 acids, 22 alcohols, 10 alkanes, 13 ketones, 4 alkenes, 6 esters, and 2 pyrazines. 58 glycerides were identified, with concentrations of 568.59–2056.53 mg/kg. TG (54:2), TG (54:3), and TG (54:7) were the top three glycerides. Five types of phytosterols were identified, with levels of 568.48 mg/kg - 2364.68 mg/kg. γ-tocopherol was the most abundant tocopherol, ranging from 51.18 mg/kg to 1832.55 mg/kg. Total triterpene alcohol ranged from 106.73 to 717.64 mg/kg, including taraxerol, cycloartenol, and parkeol, etc. The results indicated that there were slight differences in the chemical composition of walnut oils among different regions or countries. Notably, walnut oil was a good source of unsaturated fatty acids, phytosterols, and tocopherols.