Normal Load Research Articles

Exploring the Interplay between Tribocorrosion and Surface Chemistry of the ASTM F139 Surgical Stainless Steel in Phosphate-Buffered Saline Solution

Surgical ASTM F139 stainless steel is used for temporary fixtures in the biomedical field. Tribocorrosion is a major concern in this application. The aim of the present work was to study the interplay between tribocorrosion behavior and the surface chemistry of the ASTM F139 stainless steel in phosphate-buffered saline solution (PBS). Sliding wear tests were conducted against alumina balls at different electrochemical potentials: open circuit potential (OCP), cathodic potential (−100 mV versus the OCP), and anodic potentials (+200 mVAg/AgCl and +700 mVAg/AgCl). The normal load was 20 N. The wear volume was estimated based on micrographs obtained from the wear tracks using confocal laser scanning microscopy. Moreover, the wear tracks were also examined by scanning electron microscopy (SEM). The surface chemistry of the ASTM F139 specimens was analyzed by X-ray photoelectron spectroscopy (XPS). The wear volume was dependent on the electrochemical potential, being maximized at +700 mVAg/AgCl. Delamination areas and grooves were observed in the wear tracks. Detailed assessment of the surface chemistry inside the wear tracks allowed identification of the main chemical species and their relative quantities, thus enabling correlation of the passive film composition with the observed tribocorrosion behavior.

Multi-Objective Optimization of Tribological Characteristics for Aluminum Composite Using Taguchi Grey and TOPSIS Approaches

In this study, a multi-objective optimization regarding the tribological characteristics of the hybrid composite with a base material of aluminum alloy A356 as a constituent, reinforced with a 10 wt.% of silicon carbide (SiC), size 39 µm, and 1, 3, and 5 wt.% graphite (Gr), size 35 µm, was performed using the Taguchi method, gray relational analysis (GRA), and Technique for Order Preference by Similarity to Ideal Solution (TOPSIS) decision-making methods. Tribological tests were carried out on a “block on disc” type tribometer with lubrication. Load, sliding speed, and graphite mass concentration were analyzed as input parameters. As output parameters, wear rate and coefficient of friction were calculated. An analysis of variance (ANOVA) was conducted to identify all parameters that have a significant influence on the output multi-response. It was found that the normal load has the highest influence of 41.86%, followed by sliding speed at 32.48% and graphite addition at 18.47%, on the tribological characteristics of composites. Multi-objective optimization determined that the minimal wear rate and coefficient of friction are obtained when the load is 40 N, the sliding speed is 1 m/s, and the composite contains 3 wt.% Gr. The optimal combination of parameters achieved by GRA was also confirmed by the TOPSIS method, which indicates that both methods can be used with high reliability to optimize the tribological characteristics. The analysis of worn surfaces using scanning electron microscopy revealed adhesive and delamination wear as dominant mechanisms.

Friction and Wear of Hard Yet Tough TiN Coatings Deposited Using High-Power Impulse Magnetron Sputtering

The friction and wear response of hard coatings is complex, which largely depends on a good combination of hardness and toughness, and their service life is difficult to predict. Hence, in this work, hard yet tough TiN coatings were deposited using high-power impulse magnetron sputtering at 5–10 kW. With increasing sputtering power, the coatings showed a transition in crystal texture from (200) to (111), along with a refinement in microstructure, leading to an improvement in hardness (H) of 29.8–31.2 GPa and an effective Young’s modulus (E*) of 310–365 GPa. The hard yet tough TiN coatings deposited at 6.5 kW exhibited the highest H/E* and H3/E*2 ratios of 0.097 and 0.29, respectively, as well as the highest fracture toughness of 2.1 MPa·m1/2 and elastic recovery of 42.5%. Accordingly, the coatings possessed an enhanced adhesion and cohesion, in terms of micro-scratch critical load (LC3 = 19.67 N) and HF Rockwell HF1 level. The friction and wear response of hard yet tough TiN coatings under the normal load of 1–10 N were investigated to explore their durability and predict their critical load up to failure. Wear mechanisms changed from oxidative to severe abrasive wear, with load increasing from 1 to 10 N. At 2–5 N, a combination of oxidative and abrasive wear was observed. The coatings maintained their integrity up to the critical load of 9.4 N before failure event, with a maximum wear track depth of 1.8 μm, indicating their durability under the loading conditions.

Tribology-Based Specifications for Assessing the Production Temperatures of Asphalt Binder

The success of warm mix asphalt (WMA) technology and polymer-modified binders (PMB) depends on the accurate determination of the production temperatures. To date, no standard protocol has been developed to determine the production temperatures of the WMA technology. Recent studies have shown that the production temperature is related to the friction between the aggregate and asphalt binder, which can be explored using tribology. This study attempted to develop a tribology-based approach to evaluate the production temperature of WMA-modified binder and PMB. The ball-on-the-three-plate test was performed using different normal loads (1N, 3N, 5N, and 10N) and sliding speeds (0.05 m/s, 0.1 m/s, and 0.3 m/s). The test results were compared with the equi-viscous (EQ) method. Production temperatures obtained from the EQ method were inappropriate for WMA and PMB. Results of the tribology study showed that the normal load of 1N and 0.3 m/s was found suitable for evaluating the production temperatures. Adding WMA additives resulted in a lower coefficient of friction (CoF), whereas PMB showed higher CoF than viscosity grade binder (V8, which is used for WMA modification). The addition of WMA additive reduced the production temperatures of V8, and reduction was a function of the WMA additive type. Temperature ranges corresponding to the CoF of 0.26 ± 0.021 and 0.33 ± 0.023 were proposed for assessing the mixing and compaction temperatures, respectively.

Experimental Study on Flexural Behavior of RC Piles with Basalt Fiber-Reinforced Polymer Bars and Load Carrying Capacity Calculation

The practical application of BFRPB (Basalt Fiber-Reinforced Polymer Bars) as a support structure in foundation pit and slope engineering is relatively under-researched. The indoor tensile test presented in this paper is carried out on the bond between BFRPB and different labelled concrete. The mechanical characteristics of BFRPB, the failure characteristics, and the load-carrying capacity were analyzed. The results of this study demonstrate that the normal section stress of concrete cylindrical components with BFRP has a good linear relationship and supports the rationality of the flat section assumption. In circular reinforced concrete BFRP structures, the failure of the pile load occurs in four phases, and the cracking load is in the range of 51% to 67% of the normal yield load. The main bars increase in strain with load but become attenuated in the compression zone. The deformation of the main bars increases with the load but becomes muted in the compression zone. Based on the method of calculating the load-carrying capacity of GFRP-reinforced RC piles and the normal limit load-carrying moment obtained from in-door tests, the bending moment correction coefficient in the calculation formula for the load-carrying capacity of BFRP-reinforced RC piles was then obtained.

Developing an initial normal-loading, subsequent passive changes in local normal load/stiffness-allowable direct shear tester of discontinuities and investigating the shear behaviors of discontinuities

A widespread case of discontinuity shearing is among the local shallow rock blocks sliding along non-planer, rough, non-anchored discontinuities, which is characterized by initial normal load in addition to free subsequent change in local normal load/stiffness, provoked by shear dilatancy (INL). The existing direct shear apparatuses of rock discontinuities fitted for those cases are rare, and it is lack of understanding the shear behaviors of discontinuities under such INL boundary conditions. Here, we develop an INL direct shear tester of discontinuities for shear strength. This tester takes advantage of the direct shear test apparatus modified after the YZ-5 model without a servo-controlled system to permit the accomplishment of those boundary conditions. Shear behaviors of unfilled discontinuities and infilled ones under INL boundary conditions are investigated. Moreover, the possible influence of clay content on those shear behavior of infilled discontinuities is clarified. The developed tester made it possible to test the shear performance of the local shallow rock blocks sliding along non-planer, rough, non-anchored discontinuities. This work contributed to a limited body of researches on the shear behaviors of discontinuities under those INL boundary conditions. Limitations of this work are also revealed.

A comprehensive review of experimental studies on shear behavior of bolted rock joints with varying rock joint and bolt parameters and normal stress

AbstractThe shear characteristics of bolted rock joints are crucial for the stability of tunneling and mining, particularly in deep underground engineering, where rock bolt materials are exposed to high stress, water pressure, and engineering disturbance. However, due to the complex interaction between bolted rock joints and various geological contexts, many challenges and unsolved problems arise. Therefore, more investigation is needed to understand the shear performance of bolted joints in the field of deep underground engineering. This study presents a comprehensive review of research findings on the responses of bolted joints subjected to shearing under different conditions. As is revealed, the average shear strength of bolted rock joints increases linearly with the normal stress and increases with the compressive strength of rock until it reaches a stable value. The joint roughness coefficient (JRC) affects the contact area, friction force, shear strength, bending angle, and axial force of bolted rock joints. A mathematical function is proposed to model the relationship between JRC, normal load, and shear strength. The normal stress level also influences the deformation model, load‐carrying capacity, and energy absorption ratio of bolts within bolted rock joints, and can be effectively characterized by a two‐phase exponential equation. Additionally, the angle of the bolts affects the ratio of tensile and shear strength of the bolts, as well as the mechanical behavior of both bolted rock joints and surrounding rock, which favors smaller angles. This comprehensive review of experimental data on the shear behavior of bolted rock joints offers valuable theoretical insights for the development of advanced shear devices and further pertinent investigations.

Anomalous strain dependence of phononic friction between black phosphorus layers

This study reveals unexpected strain-dependent friction, when applied strain to one of two layers of relatively sliding black phosphorus, friction is likely to exhibit characteristic rise and subsequent fall, forming a distinct friction peak. Existence and location of such peak are closely related to magnitude of normal loads. Interfacial pinning is weak at lower normal load, matched dissipation channels are easy to be destroyed, resulting in a monotonic decrease of friction. At higher normal load, tip is also pulled apart once applying a small strain to substrate, stored deformation energy leads to greater energy dissipation than at strain of zero, causing friction to decrease non-monotonically. Moreover, ability of sliding layers to withstand strain decreases with increasing normal loads or temperatures.

Variable cycle fretting conditions meditated wear behavior and mechanism in a self-lubricating composite coating on TC21 titanium alloy substrate

To simulate the variational working conditions of the titanium fastener in the aero-engine, variable cycle fretting wear tests were carried out for normal loading (80/40N), frequency (100/30Hz), displacement amplitude (80/40μm) and operating temperature (500/350°C) in a self-lubricating composite coating on TC21 titanium alloy substrate, and the fretting wear behavior and wear mechanism were thoroughly investigated. The results shows that the coefficient of friction (COF) and the wear volume present a significant difference under variable cycle fretting conditions. The specimen exhibits a relatively stable COF under variable operating temperature. Whereas for the specimen under variable displacement amplitude presents a lowest wear volume. The adhesive wear is mainly found in the specimens under variable normal loading and frequency. Whereas for the specimens under variable displacement amplitude and operating temperature, abrasive wear and oxidation wear is mainly dominated, respectively. The dissipated energy calculation results demonstrate that the variable displacement amplitude and operating temperature have greater impact on the fretting wear behavior. The microstructure analysis in the cross-section of specimens reveals that the sub-surface is composed of amorphous-nano crystalline layer, plastic deformation layer and the origin coating. Additionally, the wear mechanism of the specimens under variable fretting conditions were deeply revealed. This work can provide essential information on fretting behavior and mechanism under the variational working conditions.

Comprehensive assessment of global spinal sagittal alignment and related normal spinal loads in a healthy population

Abnormal postoperative global sagittal alignment (GSA) is associated with an increased risk of mechanical complications after spinal surgery. Typical assessment of sagittal alignment relies on a few selected measures, disregarding global complexity and variability of the sagittal curvature. The normative range of spinal loads associated with GSA has not yet been considered in clinical evaluation. The study objectives were to develop a new GSA assessment method that holistically describes the inherent relationships within GSA and to estimate the related spinal loads.Vertebral endplates were annotated on radiographs of 85 non-pathological subjects. A Principal Component Analysis (PCA) was performed to derive a Statistical Shape Model (SSM). Associations between identified GSA variability modes and conventional alignment measures were assessed. Simulations of respective Shape Modes (SMs) were performed using an established musculoskeletal AnyBody model to estimate normal variation in cervico-thoraco-lumbar loads.The first six principal components explained 97.96 % of GSA variance. The SSM provides the normative range of GSA and a visual representation of the main variability modes. Normal variation relative to the population mean in identified alignment features was found to influence spinal loads, e.g. the lower bound of the second shape mode (SM2-2σ) corresponds to an increase in L4L5-compression by 378.64 N (67.86 %).Six unique alignment features were sufficient to describe GSA almost entirely, demonstrating the value of the proposed method for an objective and comprehensive analysis of GSA. The influence of these features on spinal loads provides a normative biomechanical reference, eventually guiding surgical planning of deformity correction in the future.

Prediction of wear volume and friction coefficients of SS304 alloy using grey taguchi based response surface methodology

Abstract The present investigation is centered on examining the tribological characteristics within a pin-on-disk configuration resembling a cylinder on a flat contact surface. The pin, constructed from Stainless Steel 304 alloy, underwent sliding experiments under varying speeds (1, 2, and 3 m/s) and normal loads (10, 15, and 20 N) across track diameters of 60 and 120 mm. The experiments aimed to mitigate wear and friction in movable components, thus conducted for up to 2000 seconds in the experimental setup without any lubrication. Observations of the coefficients of friction stabilization and wear rate were made by manipulating the input parameters to anticipate the failure range. Higher coefficients of friction and increased wear rates were noted at lower sliding speeds, with wear rates stabilizing at higher speeds. Interestingly, despite a higher coefficient of friction stabilization and wear rate at a 120 mm track diameter, wear decreased. Optical Microscopy studies were carried out to examine surface damage for all normal loads and sliding speeds using both 60 mm and 120 mm track diameters. Additionally, this study employs Grey Taguchi-based Response Surface Methodology (GT-RSM) to forecast and regulate wear and friction. The findings of this study have practical implications for industries such as automotive, aerospace, and others employing SS 304 alloys in their operational components.

Analysis of multilayered two-dimensional decagonal piezoelectric quasicrystal beams with mixed boundary conditions

Piezoelectric quasicrystals have a broad spectrum of promising applications and research value due to their unique atomic arrangement and multi-field coupling effects. This paper presents a mechanical analysis of the static bending and free vibration problems of two-dimensional multilayered decagonal piezoelectric quasicrystal laminated beams. Mechanical models of the beams are established, and the differential quadrature method in conjunction with the state-space method is utilized to obtain the solutions for the beams with mixed boundary conditions. We first investigated the static response and free vibration problem of quasicrystal laminated beams. By degrading them into crystalline materials, we verified the accuracy of the method by comparing the results with the existing ones. Then, the effects of different boundary conditions and slenderness ratios on the stresses, displacements, electric potentials, and electric displacements of quasicrystal laminated beams under normal mechanical loading and free vibration are investigated. Subsequently, the effects of different laying modes on the mechanical properties of the quasicrystal laminated beams when the material principal axis of the beam is changed are also analyzed.

Comparative study between sliding mode and DTC of doubly fed induction machine

Although the great advance in term of AC machine construction, control strategies are also necessary to be developed and improved continuously satisfying output torque/power. Hence the Doubly fed induction motor (DFIM)is widely used in industry, since it can operates in wide range of speed variation around the synchronous speed and the control of flux and torque is independent. In this paper, control of doubly fed induction motor (DFIM) has been investigated, which two control strategies have been studied and compared: the first strategy uses a sliding mode control (SMC); the second employs Direct Torque Control (DTC). Modeling of DFIM and details of both control strategies have been presented. the mathematical description of different basic dynamic models of the DFIM have been carried out The performances in terms of torque tracking, accuracy and robustness of both control techniques under normal and various speed and load conditions have been demonstrated and compared.

Experimental and molecular dynamics simulation based investigation to understand tribological performance of graphene reinforced thermoplastic polyurethane (Gr/TPU) nanocomposites

Ongoing innovative research in tribology aims to develop high-performance polymer nanocomposite (PNC) materials that offer significant improvements in efficiency, reliability, and durability across various engineering systems. Selection of appropriate nanoreinforcements is crucial for maximizing the tribological behavior in PNCs. The primary objective is to investigate how various factors, such as graphene (Gr) loadings, processing techniques, normal loading, and sliding velocity influence the tribological behavior of thermoplastic polyurethane (TPU) and graphene reinforced thermoplastic polyurethane (Gr/TPU) nanocomposites using molecular dynamics (MD) simulation and experiments. Nanocomposite materials fabricated by ultrasonication methods, test specimens are prepared in appropriate dimensions as per ASTM (American Society for Testing and Materials) and DIN (Deutsches Institut für Normung) standard. MD simulations are conducted on the developed plate and rod models under different sliding velocity, pressing and stabbing depth conditions to understand fundamental insights into the friction and wear mechanisms of Gr/TPU nanocomposites at the atomic level. Morphological studies using scanning electron microscopy (SEM) micrographs indicate no case of Gr agglomeration up to 3 wt% Gr/TPU nanocomposite. Energy dispersive spectroscopy (EDS) analysis confirms presence of Carbon (c), Nitrogen (N) and Oxygen (O) in Gr/TPU nanocomposites. Finally the obtained results from MD simulation and experiments show a significant trend of similarity.

A study of fretting fatigue in a contact pair of DZ125/GH4169: its mechanical behavior and life prediction

In this paper, the fretting fatigue test of DZ125/GH4169 contact pair was carried out. Observation and analysis of the wear and fracture were needed to get the fretting damage law. A hardness parameter was introduced to modify the existing life prediction model. The specimen was exposed to both normal and fatigue loads, as indicated by the results, which resulted in the formation of a black oxide layer that stuck to the contact zone's edge. Oxide spalling formed grits and abrasive wear, accelerating the loss of fatigue resistance. At high temperatures, the oxidation was intensified. The life prediction results were all within the double error band. The error range was reduced and the life prediction effect was significantly improved.

Effect of Normal Load on the Nanofriction Behavior of Graphene on Stainless-Steel Substrate: Implication for Nanoscale Lubrication

Effect of Normal Load on the Nanofriction Behavior of Graphene on Stainless-Steel Substrate: Implication for Nanoscale Lubrication

Design of a gradient elastic modulus transition layer based on film-substrate adhesion

The codeformation process of Ti6Al4V (TC4) substrate and chromium nitride (CrN) films with dense/loose CrN and gradient elastic modulus CrN/CrNx/Cr(N) (G-CrN) structures under normal impact load were simulated by changing the thicknesses of the films or the loose CrN and G layers. The dispersed distribution of interfacial tensile stresses and strains of G-CrN films improved the layers’ codeformation, compared with the firm large layer of the dense/loose CrN films. The stress reduced as the loose/G layer thicknesses increased. The 4.7 μm CrN films with various thicknesses of the G-layers, 0.2 µm, 0.6 µm, 0.75 µm and 0.9 µm, were prepared on TC4 to evaluate the film-substrate adhesions and verify the simulated deformation procedure. A G-layer between a ceramic film and its alloy substrate is needed, and the 0.83–1.08 µm thicknesses of the G-layers were suggested for the CrN/TC4 system varied with the films’ thicknesses. The dispersed distribution of the tensile stress and strain within the G-CrN film was the mechanism of the film-substrate adhesion improvement.

Enhancing the Tribological Characteristics of Epoxy Composites by the Use of Three-Dimensional Carbon Fibers and Cobalt Oxide Nanowires

In this paper, the results of our research were presented into the sliding wear behaviors of reinforced epoxy composites made with 3D networked carbon fibers ornamented with nanowires of cobalt oxides (NWRs@CFs). Composites are made using the cast-in-place method. Under different normal loads and sliding velocities, these composites' wear and friction coefficient performances are assessed. Tests were performed at 400 rpm spindle speed, 10, 20, and 30 N normal load, and a duration of 300 seconds. Pure epoxy exhibits wear rates of 0.449, 0.481, and 0.501 * 10-5 mm3/Nm at 10, 20, and 30N. Conversely, 3D CFs/epoxy composites exhibit lower wear rates (0.334, 0.360, and 0.390 * 10-5 mm3/Nm) at the same pressure. The epoxy composites of NWRs@CFs wear less, measuring 2.1, 3.5, and 0.4 * 10-5 mm3/Nm under applied loads. The effects of speed on the tribological characteristics were also studied, the friction coefficients for 400, 800, and 600 rpm at 10 N. Pure Epoxy has fraction coefficients of 0.449, 0.494, and 0.552µ at 400, 800, and 600 rpm. In comparison, three-dimensional carbon fibers and epoxy composites show reduced wear rates (0.334, 0.376, and 0.304 µ) under identical loads. Epoxy composites of NWRs@CFs have friction coefficients of 0.261, 0.304, and 0.332µ. Pure epoxy has high wear, indicating less friction resistance.

Fretting wear behavior on LPBF processed AlSi10Mg alloy for different heat treatment conditions

To widen the industrial application of additively manufactured (AM) parts, the study of fretting wear behavior is essential, as it ensures the safety and reliability that drive innovation in design and materials. This study explores the fretting wear behavior of the as-built and heat-treated state of AlSi10Mg alloy fabricated, viz., laser powder bed fusion (LPBF). Initially, the as-built and T5, T6, and stress-relieved (SR) heat-treated samples were examined using scanning electron microscopy (SEM) to gain insights into the microstructural changes. The as-built samples exhibited a higher hardness level (135 HV) primarily due to the presence of very fine microstructure of the α-Al cellular matrix with embedded Si. The α-Al cellular structure dissolved with various heat treatments, and Si particles coarsened. The hardness decreased to 85, 79, and 67 HV for the T5, T6, and SR conditions, respectively. Subsequently, fretting tests were conducted on the samples, applying various normal loads of 10, 50, and 100 N. Further, the samples were characterized by the coefficient of friction (COF), worn surface morphology, and wear volume loss. The investigation showed that the as-built material showed less wear volume loss under all loading conditions than the heat-treated conditions. Furthermore, the T5 heat treated sample had a lower wear volume when compared to the T6 and SR heat-treated samples. The heat-treated sample exhibits compressive stress, whereas the LPBF processed, the as-built sample shows tensile stress.

Theoretical and experimental investigation of vibration-assisted scratching silicon

Interaction between tip and workpiece plays a crucial role in determining the scratching depth in Vibration-assisted Tip Based Nanofabrication (VTBN), which is more complicated than that of conventional scratching (without vibration-assisted). To establish the relationship between the scratching depth and machining parameters, a cubecorner indenter is employed to conduct VTBN procedure. The indenter is simplified as a cone to calculate the contact model in both 1D groove and 2D surface machining processes. An instantaneous normal load model is established based on the developed tip-workpiece contact model. Due to the variation of instantaneous contact area, effective contact area is put forward for the first time to predict the normal load. Effects of vibration frequency and amplitude on the normal load and surface quality are analyzed based on the proposed model. Experimental results show that higher frequency and larger amplitude will reduce the effective contact area. Vibration can increase the scratching depth and width without enlarging the cutting force. Furthermore, the inconsistency caused by scratching directions in conventional scratching is also overcome during VTBN.