Resin Nanoceramic Research Articles

The Effect of Gastric Acid and Material Type on the Surface Roughness of Additive and Subtractive Manufacturing Resins.

The aim of this study is to examine the effect of gastric acid on the surface roughness of additive and subtractive manufacturing resin. In this study, two subtractive manufacturing CAD-CAM resin nanoceramic (CerasmartTM270 (CS), LavaTM Ultimate (LU)) and two additive manufacturing 3D printing permanent resin (VarseoSmile Crownplus (VSP), Crowntec (CT)) was used. CS and LU samples were turned into 10 mm diameter cylinders with a scraper and cut into 2 mm slices on the cutting device. CT and VSP samples were produced on a 3D printer (2mm thickness-10mm diameter) (n:15). All samples were exposed to a cycle of 60 seconds of gastric acid, 5 seconds of distilled water, and 30 minutes of artificial saliva, 6 times a day for 10 days. Surface roughness mean (Ra) and depth (Rz) was measured with a contact profilometer at baseline and after gastric acid cycling. Data were analyzed using SPSS (22.0), One way ANOVA, post-hoc Tukey's and Independent-t test (p <.05). Ra-Rz values of CT and VSP were significantly higher than CS and LU at baseline and after the gastric acid cycle (p <.05). After the gastric acid cycle, the Ra-Rz values of all materials increased significantly compared to the baseline (p <.05) but the Ra values of all materials were at a clinically acceptable level (<0.2µm). Although additive manufacturing 3D printing permanent resins offered higher roughness values, they weren't at a clinically unacceptable level. Therefore, they can be an alternative to subtractive manufacturing CAD-CAM resin nanoceramics.

Effect of Hydrogen Peroxide-Based Bleaching Agents on the Color Dimensions and Surface Roughness of Different Milled Restorative Dental Materials.

To compare the color dimensions, color discrepancies (ΔE00), and surface roughness of milled materials before and after application of a bleaching agent. A total of 10 extracted molars were obtained. Each tooth was cut in transverse sections to create disks (3-mm thick, 10-mm diameter; control group). Disk specimens of eight materials (n &#61; 10 per group) were fabricated: polymethyl methacrylate (PMMA) interim material (PMMA-Telio group), two resin nanoceramics (RNC-Ultimate group and RNC-Cerasmart group), two hybrid ceramics (HC-Shofu group and HC-Enamic group), lithium disilicate (LD-Emax group), zirconia-reinforced glass ceramic (ZGC-Suprinity group), and zirconia (Zr-InCeram group). Color measurements were obtained using a spectrophotometer before and after applying 35% hydrogen peroxide-based bleaching agent. Pre- and postbleaching surface roughness (Sa) analyses were completed using a profilometer. Significant L*, a*, b*, and ΔE00 value differences were found (P < .05). Color discrepancies (ΔE00) ranged from 0.30 ± 0.14 to 4.82 ± 0.10. The highest color discrepancies were measured on the PMMA-Telio group, while the lowest color discrepancies were computed for ZGC-Suprinity, RNCUltimate, and RNC-Cerasmart. Significant surface roughness differences were found (P < .05). The largest increase of surface roughness values between the pre- and postbleaching measurements was obtained in the PMMA-Telio group with a mean ΔSa value of 4.73 ± 3.02, while the largest decrease of surface roughness values between the pre- and postbleaching measurements was obtained in the Zr-InCeram group with a mean ΔSa value of -1.58 ± 0.10. The milled materials showed significant pre- and postbleaching color and surface roughness discrepancies.

Effects of Er,Cr:YSGG Laser Surface Treatments and Composites with Different Viscosities on the Repair Bond Strength of CAD/CAM Resin Nanoceramic.

This study aims to evaluate the repair micro-shear bond strength of the CAD/CAM resin nanoceramic block treated using four different surface treatments and composite resins of different viscosities. For the current study, 96 samples with dimensions of 14 × 12 × 2 mm were obtained from a CAD/CAM resin nanoceramic block (Cerasmart) with a low-speed precision cutting saw under water cooling. The relevant samples were randomly divided into four groups according to the surface treatment processes: grinding with diamond bur, aluminum oxide airborne-particle abrasion, long-pulse laser, and short-pulse laser. Following silane application, universal adhesive was applied to all surface-treated samples and cured with an LED for 10 s. The samples prepared for the repair procedure were divided into two subgroups (microhybrid composite and injectable composite) according to the viscosity of the repair material to be used (n = 12). After the repair procedure, care was taken to keep the samples in distilled water in an incubator at 37 °C for 24 h. The repair micro-shear bond strength values (μSBSs) of CAD/CAM resin nanoceramic-composite resin complexes were tested. In addition, randomly selected samples from each group were examined with a scanning electron microscope to evaluate the surface topography after both surface treatments and the micro-shear bond strength test. Data were analyzed by two-way ANOVA and Bonferroni test. It was determined that the surface treatment preferred in the repair protocol significantly affected the μSBS value (p < 0.001). While the highest μSBS value was obtained with the short-pulse laser airradiation group, the lowest μSBS values were found in samples with long pulse laser irradiation. However, samples grinded with a bur and airborne-particle abrasion showed similar μSBS values (p > 0.05). The preferred composite viscosity in the repair procedure has a significant effect on the μSBS value (p < 0.001). However, the interaction between the surface treatment and the viscosity of the repair composite does not affect the μSBS values in a statistically significant way (p = 0.193). It may be recommended to clinicians to repair CAD/CAM resin nanoceramic restoration surfaces with injectable composites or after treatment with short-pulse lasers.

Clinical Performance of Computer-Aided Design (CAD)/Computer-Aided Manufacturing (CAM) Resin Nanoceramic Endocrowns in Restoring Molars: An In Vivo Study.

Background It is difficult to determine the optimal method for restoring endodontically treated teeth, as several factors affect this decision. Functional requirements and the amount of remaining coronal tissue are considered the most important factors in choosing the best restoration for those teeth. Endocrown was introduced as a conservative alternative for endodontically treated and coronally damaged teeth. Aim The aim of this study is to assess the clinical performance of the nanoceramic system for molar endocrowns by evaluating color change, gingival condition, prosthesis integrity, and the presence of secondary caries. Materials and methods The sample consisted of 20 endocrowns. The teeth were prepared with at least 2 mm of wall thickness and a cavity depth of 4 mm from the occlusal surface. The final impression was taken, and the prostheses were adhered using dual-cure resin cement. It was clinically evaluated according to clinical success criteria (United States Public Health Service) in terms of color stability, gingival indexes, integrity of the restoration, and the presence of secondary caries after a week, three months, six months, and a year. The statistical study was conducted using IBM SPSS Statistics for Windows, Version 23.0 (Released 2015; IBM Corp., Armonk, NY, USA), and the results were considered statistically significant at the 95% level of significance. The Friedman test was used to study the significance of the differences in the average values of color change, plaque index, and the integrity of the prostheses during follow-up periods. Results The study showed a gradual increase in the degree of color change with follow-up periods. Furthermore, there was no significant difference in the incidence of gingival changes, the integrity of the prosthetic margins, or the occurrence of secondary caries during the follow-up periods. Conclusions Within the limitations of this study, an endocrown made of CeraSmart nanoceramic is an acceptable option for crowning decayed and endodontic-treated molars with acceptable clinical performance.

In Vitro Evaluation of Color and Surface Roughness Changes of Polyetheretherketone, Monolithic Zirconia, and Resin Nanoceramics Exposed to Staining Liquids.

This study aims to investigate color stability and surface roughness of polyetheretherketone (PEEK), zirconia, and hybrid ceramics while stored in different liquids. A total of 240 specimens were prepared from monolithic zirconia, PEEK, and hybrid ceramics. All specimens were polished using rubber sets with different grain sizes. Color parameters (L*, a*, b*) were measured three times using a dental spectrophotometer in standard D65 lightning. Each group was divided into eight different groups to be kept in eight different solutions as distilled water, cola, red wine, tea, coffee, heptane, citric acid, and 50% ethanol. Specimens were held in solutions at 37°C for 12 days. Color measurements were repeated, and color change (ΔE) was calculated using the CIE Lab formula. The color difference of PEEK specimens was found above the clinically acceptable limit; however, color differences for monolithic zirconia produced by coffee were found within the clinically acceptable limits. ZR and HC specimens' color change values were found between threshold values (1<ΔE < 3.3). The differences observed in surface roughness levels amongst the ZR specimens could be caused by the polishing instrument and procedure. The color change of the materials was within acceptable limits, whereas the surface roughness increased more than 0.2 µm. Especially cola, heptane, and red wine significantly increased the mean surface roughness.

Effect of coffee staining and simulated oral hygiene methods on the color and translucency of a nanoceramic resin.

Evaluate the color and translucency of a nanoceramic resin subjected to hygiene practices and immersion in coffee over time. Specimens (n = 80, HT and LT, 0.5-mm thick) of a nanoceramic resin were obtained and were divided in groups according to the simulated oral hygiene: no intervention (NT), brushing with an electric brush and water (BN), brushing with an electric brush and toothpaste for 10 s (BT), and immersion in mouthwash for 30 s (MW). Oral hygiene practices were repeated after staining in coffee solution for 15, 48, 336, 1440, 8640, and 35,040 min. Spectral wavelengths were recorded with a spectrophotometer at each time. ∆E00, ∆L', ∆C', ∆H', and TP00 were calculated by CIEDE2000 and were evaluated by 2-way ANOVA, repeated measures ANOVA, and Tukey's HSD test (α = 0.05). ANOVA showed significance among factors for ΔE00 (p < 0.05), with higher ΔE00 for NT-HT (11.7) and NT-LT (11.2). After T6 (2-year simulation), the lowest values were found for BT-HT (5.3) and BT-LT (4.9). All groups showed a reduction in lightness and translucency and increased chroma and hue. However, the smallest variations were found in the BT groups (p < 0.05). Brushing with toothpaste effectively minimized the color change of NCRs caused by coffee staining. Oral hygiene practices, such as brushing with toothpaste, might be important to minimize staining of nanoceramic resin restorations, especially in patients who frequently consume coffee.

Comparison of volumetric loss and surface roughness of composite dental restorations obtained by additive and subtractive manufacturing methods

Statement of problemPermanent crown materials produced with new generation additive manufacturing and traditional subtractive manufacturing materials have not been compared in terms of wear resistance. PurposeThis study aims to compare the volumetric loss related to wear and resulting surface roughness after aging in a chewing simulator between resin nano ceramics produced with milling technique and permanent crown materials produced with three dimensional (3D) printing. Materials and methodsThree different hybrid composite-ceramic (HCC) (The three materials are GC: Cerasmart, VE: Vita Enamic, and GV: Grandio Voco.) and one 3D printed definitive crown resin (FormLabs Permanent Crown Resin) were investigated before aging (n:8), the surface roughness of all samples was measured with a profilometer, and 1 randomly selected sample from each subgroup was imaged with scanning electron microscope (SEM). 3D scans of each sample were obtained with a desktop scanner. Thermomechanical aging was performed using a chewing simulator. Four hundred thousand cycles were completed under a vertical occlusal force of 49 ± 0.7 N with a thermal cycle of 1.7 Hz 5–55° and with a dwell time of 120 s, mimicking 2 years of aging. The imaging procedures were repeated, and the change in surface roughness was evaluated. 3D images were also overlapped, and the volumetric loss was calculated with the relevant inspector software. The data obtained were analyzed by two-way ANOVA (p < 0.05). ResultThe results showed significant statistical differences for both parameters (p > 0.05). The highest volumetric loss was found in the GV group while the lowest volumetric loss was in the VE group. The highest surface roughness values were observed in the GV group, while the lowest values belonged to the VE one. ConclusionOf the restorative materials evaluated, the VE group is suitable for long-term restorations, whereas the GV one is suitable for medium-term restorations. It is promising in terms of 3D printing technologies that the 3D material gives comparable results with the GV group. Clinical i̇mplicationAdditive manufacturing techniques are a successful method that accelerates the manufacturing process. Permanent crown resins are promising alternatives to conventional production.

Tensile bond strength of CAD-CAM all ceramic crowns before and after thermomechanical aging.

The purpose of this in vitro study was to compare the tensile bond strength (TBS) of resin nanoceramics (RNC), zirconia, and lithium disilicate (LS2) restorations cemented to titanium abutments before and after thermomechanical aging. Twelve specimens per group were fabricated to determine the TBS between a titanium abutment and four types of crown materials (2 RNCs, LS2, and translucent zirconia crowns for the maxillary molar). After milling, the abutments and crowns were cemented with resin cement after air-particle abrasion. In addition, thermomechanical aging (200,000 cycles, 50 N, 2Hz) was applied to half of the specimens by using a mastication simulator. TBS was measured by using a universal testing machine. The interface between the crown and the cement was observed by using scanning electron microscopy (SEM). Two-way ANOVA was performed to analyze the effects of crown materials and thermomechanical aging. Failure-mode and interface analyses were also conducted. After thermomechanical aging, the TBS decreased in the LS2 specimens and increased in RNCs (p < 0.001). The ratio of mixed failure and debonding with the hole-sealing resin increased in the RNC group. SEM images showed the reduced gap between the crown and the resin cement after thermomechanical aging in the RNC group. Differences in TBS were affected by the crown materials after thermomechanical aging. After thermomechanical aging, the RNC crowns showed increased TBS, whereas LS2 and zirconia crowns exhibited decreased or similar TBS.

The fracture strength and the failure mode of lithium disilicate or resin nano ceramics as a crown, overlay, or endocrown restoration on endodontically treated teeth.

Different materials and restorative concepts have been proposed over the years to restore endodontically treated teeth (ETT). Monolithic ceramic and composite restoration can be lute to the tooh, without the use of a post. However, little is known how the material stiffness and presence of a composite core will affect the survival and failure mode. The objective of this in-vitro study was to evaluate the fracture strength and failure mode of endodontically treated molars, restored with ceramic or hybrid composite monolithic restoration, in the presence of absence of a composite core. Sixty depulped molars were restored with a lithium-disilicate (e.max CAD) or hybrid composite (Cerasmart) restoration. Both materials were used in a monolithic approach, but with 3 different designs: (a) monolithic endocrown, (b) crown with a separate composite core, and (c) overlay without core buildup or pulpal extension. Ten sound teeth were used as control group. All groups were thermocycled (10,000 cycles), subsequently loaded in a chewing simulator (100,000 cycles) and finally loaded until fracture. Peak fracture loads and failure modes were registered. No significant differences were seen between the groups in terms of fracture load. Failure modes were statistically significantly different among groups with significant correlation between restoration type and material. (p < 0.001 and p = 0.033, respectively). No group presented significantly higher fracture resistance. Although ceramic crowns and overlays presented the highest repairability, all restored ETT were within the range of the intact tooth' fracture strength. No restoration presented significant different fracture loads. However, the type of restoration and material choice were correlated to the fracture mode.

Adhesive Performance of Resin Cement to Glass-Ceramic and Polymer-Based Ceramic CAD/CAM Materials after Applying Self-Etching Ceramic Primer or Different Surface Treatments.

Ensuring optimum bond strength during cementation is vital for restoration success, with the practicality of the process being crucial in clinical practice. This study analyzed the effect of a single-step self-etching ceramic primer (MEP) and various surface treatments on the microshear bond strength (µSBS) between resin cement and glass-ceramic or polymer-based ceramic CAD/CAM materials. Specimens were fabricated from leucite-based glass-ceramic (LEU), lithium disilicate glass-ceramic (LDC), resin nanoceramic (RNC), and polymer infiltrated ceramic network (PICN) (n = 160). They were then classified based on the surface treatments (n = 10): control (no treatment); sandblasting with Al2O3 (AL); etching with hydrofluoric acid (HF); and MEP application. Scanning electron microscopy was used to evaluate the surface topography. µSBS was measured after cementation and thermocycling procedures. Failure modes were examined with a stereomicroscope. Statistical analysis involved two-way analysis of variance and Tukey HSD tests with a significance level of 0.05. µSBS was significantly influenced by both surface treatment and CAD/CAM material type. The most enhanced µSBS values for each material, regarding the surface treatment, were: LEU and LDC, HF; RNC, AL; PICN, AL or HF. MEP significantly increased the µSBS values of CAD/CAM materials except RNC, yet it did not yield the highest µSBS values for any of them.

The optimal design and three-dimensional finite element analysis of CAD/CAM integrated roach attachment

ObjectivesTo investigate the effect of different designs of movable parts and prosthetic materials on the stress distribution of supporting tissues in mandibular free end dentition defects using three-dimensional finite element analysis of digital Roach attachments. Material and methodsA 3D model of a patient with Kennedy class I mandibular edentulous conditions was generated, and twelve prosthesis models were applied, combining two designs of removable parts and six types of CAD/CAM restorative materials with different elastic modulus (conventional zirconia, ultra-translucent zirconia, Polyetheretherketone (PEEK), Lithium disilicate, Nanoceramic resin, and resin composite (Paradigm MZ100, 3 M ESPE)). The stress distribution of abutment periodontal ligament, edentulousmucosa, and junction of attachment were analyzed using finite element analysis. ResultsThe stress value of the buccal neck of the periodontal ligament and the maximum compressive stress of the distal periodontal ligament of the design with clasp arms were higher than those without clasp arms, while the stress on the junction of attachment and the displacement of the mucosa in the edentulous area were smaller. Restorative materials with high elastic modulus, such as conventional zirconia and ultra-translucent zirconia, are recommended to be used as the fixed part of Roach attachment. ConclusionCAD/CAM Roach attachments with clasp arms are recommended for the protection of mucosal soft tissue. Restorative materials with high elastic modulus, such as conventional zirconia and ultra-translucent zirconia, are recommended as the fixed part of Roach attachment for patients with free end defect of mandibular dentition. Clinical significanceThis study provides references for the design with clasp arms and the selection of clinical fixed-movable prosthetic materials. Clinicians should consider the design of attachments and selection of appropriate manufacturing materials carefully to avoid negative impacts on patients' periodontal support tissues.

Zirconia-Reinforced Lithium Silicate Ceramic in Digital Dentistry: A Comprehensive Literature Review of Our Current Understanding.

Zirconia-reinforced lithium silicate (ZLS) ceramic is a new innovative dental material with unique a chemical composition that is designed to combine harmoniously with the appropriate optical properties of lithium disilicate and the enhanced mechanical strength of zirconia. A thorough understanding of ZLS materials is essential for both clinicians and dental technicians. At present, the mechanical behavior and optical properties of the ZLS ceramic system have not been extensively researched, and there is still a lack of consensus regarding the fabrication process and clinical behavior of ZLS all-ceramic restorations. The aim of the present study was to present a selection of comprehensive information concerning zirconia-reinforced lithium silicate ceramics and their optical and mechanical properties, as well as to assess data regarding cementation procedures and clinical outcomes for ZLS all-ceramic restorations. Three electronic databases (PubMed, Web of Science, and the Cochrane Library) were used for the research by two independent reviewers. The search was limited to articles published in the English language, as well as clinical and in vitro studies of color and studies on mechanical behavior and the cementation procedures of ZLS restorations. The exclusion criteria comprised abstracts, questionnaire-based studies, case reports, literature reviews, and studies that were not available in English. Zirconia-reinforced lithium-silicate-based ceramic presents a unique and complex microstructure that increases mechanical resistance but decreases aesthetic appearance, especially its translucency, due to tetragonal zirconia content. A material's thickness, the color of the underlying tooth structure, and the resin cement shade are important factors that influence the final shade and aesthetic appearance of ZLS restorations. Mechanical properties, which are defined by the fracture toughness, flexural strength, elastic modulus, and hardness of ZLS ceramic are higher compared to feldspathic, lithium disilicate, and hybrid ceramics, as well as resin nanoceramics; however, they are lower than translucent or high-translucency zirconia. Acid etching, sandblasting, and laser etching represent the most used methods to prepare the ZLS restoration surfaces for proper bonding procedures.

Biomechanical behavior and Weibull survival of CAD-CAM endocrowns with different marginal designs: A 3D finite element analysis

ObjectivesTo evaluate and compare the effect of tooth preparation designs and different CADCAM. materials on stress distribution and Weibull survival probability of endocrowns. applied to root canal-treated lower first permanent molar using the 3D finite element. analysis method. MethodsA root canal-treated lower first permanent molar was prepared for endocrowns with a. butt joint or with a ferrule design by placing, circumferentially, a 1-mm wide shoulder. finish line. The prepared molar was scanned for the two designs and modeled on a 3D. Finite element model. Monolithic zirconia (IPS e.max ZirCAD MT, FCZ), lithium. disilicate (IPS e.max CAD, EX), and nano-ceramic resin composite (Lava Ultimate, LU). CAD-CAM materials were used for each preparation to design the virtual endocrown. A. total of six models were built according to the different tooth preparation designs and. endocrown materials. An occlusal load of 600 N and a transverse load of 20 N in. magnitude that simulates the average occlusal load was directed toward the occlusal. surfaces. von Mises and maximum principle values were evaluated Weibull risk-ofrupture. analysis was used to analyze the survival probability of the restorations and. tooth in the different models. ResultsThe highest von Mises were found in the butt joint design for FCZ, EX, and LU (45.3. MPa, 35.2 MPa, and 24.2 MPa, respectively) compared to the ferrule design for the. same materials (42.6 MPa, 31.2 MPa, and 23.6 MPa, respectively). For von Mises. stress distribution in the remaining part of tooth structure (dentin), the highest stresses. were found in LUFerrule which was closely similar to LUButt joint (135.4 MPa and. 134.7 MPa, respectively), followed by EXFerrule and FCZFerrule (132.2 MPa and. 131.7 MPa, respectively), while the lowest stresses were found in EXButt joint and. FCZButt joint (129.0 MPa and 128.4 MPa, respectively). Shear stresses within the. resin cement were the highest in FCZ and EX compared to LU. EX was found to be the. most reliable material with the highest survival probability, while FCZ showed the. lowest survival probability according to the Weibull risk-of-fracture results. SignificanceMaterials with high elastic modulus transfer more stresses to the endocrown and less. to the remaining tooth structure. Endocrown tooth preparation with ferrule design has. better stress distribution and magnitude compared to the butt joint design.

Fatigue resistance of 3D printed anatomic post-and-core after mastication simulation

Rigid post-and-core systems have traditionally been used in the restoration of endodontically treated teeth and are regarded by many as the standard treatment. Flexible materials, including nanoceramic resins, are being increasingly implemented as post-and-core systems, but data supporting their use are lacking. The purpose of this in vitro study was to compare the fatigue resistance of conventional cast metal and nanoceramic 3-dimensionally (3D) printed resin post-and-core systems with teeth without posts. Thirty freshly extracted human maxillary premolars were endodontically treated and divided into 3 subgroups (n=10) according to the restorative procedure: cast metal post-and-core (CM), nanoceramic 3D printed resin post-and-core (3DR), and without a post (0P). The CM post-and-core group was fabricated conventionally, while the 3DR group was printed using a 3D resin printing material. For the 0P group, the teeth were restored with a composite resin foundation after root canal obturation. Complete coverage 3-mol% monolithic zirconia restorations were cemented on all specimens. The specimens were exposed to simultaneous mastication simulation (1.2 million cycles) and thermocycling (10 000 cycles at 5 ºC to 55 ºC) and analyzed based on the failure of specimens. Data were analyzed using the Kruskal-Wallis survival analysis and the Wilcoxon rank sum test (α=.05). The Kruskal-Wallis test indicated statistically significant differences among the cycles needed to reach failure for each of the 3 groups (P<.001). At 1.2 million cycles, there were no CM failures. The 3DR group failed at a median value of 950 000 cycles, while the 0P group failed at a median value of 222 500 cycles (P<.001). All the endodontically treated teeth that received CM survived the 1 200 000 simulated mastication cycles. Both 3DR and 0P specimens fractured at the crown cervical third during mastication simulation.

Flexural strength and translucency of barium-silicate-filled resin nanoceramics for additive manufacturing.

This in vitro study aimed to evaluate the flexural strength (FS) and translucency parameter (TP) of resin nanoceramics (RNCs) with barium silicate for additive manufacturing. An RNC slurry was prepared by mixing a barium silicate filler and resin monomer. For the FS tests, specimens with three filler contents (0, 50, and 63 wt%) were designed according to ISO6872 for dental ceramics and ISO10477 for dental polymers. These specimens were then formed into discs with thicknesses of 1 and 2 mm for TP measurement. In the specimens prepared according to ISO6872, the FS increased significantly depending on the filler content. However, in the case of ISO10477, there was no significant difference between the FSs of the specimens with 0 and 50 wt% filler contents. The increase in thickness affected translucency, and the lowest translucency was obtained at a filler content of 63 wt%. The filler distribution was dense in the specimen with 63 wt% filler and uniform but relatively sparse in the specimen with 50 wt% filler. More voids were observed in the specimen with 63 wt% filler. The thickness and filler content of the specimen affected its TP. The TP of the specimen with 63 wt% filler was similar to that of human enamel. The FS was significantly higher at a filler content of 63 wt%. The lowest translucency was obtained at a filler content of 63 wt% for all tested thicknesses. Increasing the filler content was advantageous for the mechanical properties of the RNCs. A high filler content led to low translucency in the RNCs. Therefore, the esthetics of human teeth can be reproduced if layering according to the filler content is performed in areas where esthetic characteristics are required.

Microtensile Bond Strength of CAD-CAM Restorative Dental Material Blocks to Resin Cement: An In Vitro Study

Introduction: Today’s dentistry frequently employs bonded partial restorations, which are usually fabricated in ceramic materials. In the last decade, hybrid materials have emerged that attempt to combine the properties of composites and ceramics. Objectives: To evaluate in vitro, by means of a microtensile test, the bond strength between CAD-CAM restorative materials and the cement recommended by their manufacturer. Material and Method: From blocks of CAD-CAM restorative material bonded to composite blocks (Filtek 500®), beams with a bonding area of approximately 1 mm2 were made and divided into four groups: EMAX (IPS e.max CAD® lithium disilicate), VE (VITA Enamic® polymer-infiltrated ceramic matrix), LUA (Lava Ultimate® nano-ceramic resin with sandblasting protocol) and LUS (Lava Ultimate® nano-ceramic resin with silica coating protocol). In each group, perimeter (external) or central (internal) beams were differentiated according to the position in the block. The samples were tested on the LMT 100® microtensile machine. Using optical microscopy, the fractures were categorized as adhesive or cohesive (of the restorative material or composite), and the data were analysed with parametric tests (ANOVA). Results: The LUS group had the highest results (42 ± 20 MPa), followed by the LUA group (38 ± 18 MPa). EMAX had a mean of 34 ± 16 MPa, and VE was the lowest in this study (30 ± 17 MPa). In all groups, the central beams performed better than the perimeter beams. Both EMAX and VE had the most adhesive fractures, while LUA and LUS had a predominance of cohesive fractures. Conclusions: Lava Ultimate® nanoceramic resin with the silica coating protocol obtains the best bond strength values.

Effect of the application of a hydrogen peroxide home bleaching agent on the cytotoxicity of different CAD-CAM restorative materials.

The information regarding the cytotoxicity of ceramic and resin-matrix ceramic materials subjected to over-the-counter bleaching agents is limited in the literature. The aim of the present study was to investigate the cytotoxic effects of lithium disilicate ceramic (LDC), resin nano-ceramic (RNC) and nano-hybrid composite (NHC) computer-aided design/ computer-aided manufacturing (CAD-CAM) block materials subjected to a home bleaching agent and artificial saliva. A total of 432 specimens were prepared from 3 different CAD-CAM materials. Each material group was divided into 4 groups according to the storage medium (phosphate-buffered saline (PBS) or artificial saliva), and whether the specimens were subjected to a bleaching agent or not. For the bleached groups, hydrogen peroxide (10%) was applied to the specimens for 30 min/day for 15 days, and the specimens were immersed in PBS or saliva after bleaching. The viability of epithelial cells was detected using the 3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide (MTT) assay at the end of the 5th, 10th and 15th day of the study. The data was statistically analyzed. Regardless of the storage medium and the time period, all restorative materials decreased the viability of cells. The highest cytotoxicity levels were determined on the 15th day of the study. The application of a bleaching agent increased the cytotoxicity of the LDC specimens stored in artificial saliva. The RNC material stored in PBS demonstrated significantly higher cell viability than the LDC and NHC groups. The LDC and RNC specimens stored in artificial saliva did not show any significant difference in cytotoxicity. When the materials were subjected to bleaching, NHC demonstrated the highest cytotoxicity during all periods. No significant difference was found between the LDC and RNC specimens subjected to both artificial saliva and bleaching in terms of cytotoxicity. The type of restorative material, the immersion medium, the application of a bleaching agent, and the application period affected the cytotoxicity of the materials. Over-the-counter home bleaching agents may induce cellular cytotoxicity due to the existing restorations, and patients should be informed about this potential biological response.

Effect of hydrogen peroxide-based bleaching agents on the color dimensions and surface roughness of different milled restorative dental materials.

To compare the color dimensions, color discrepancies (ΔE00), and surface roughness of milled materials before and after the application of a bleaching agent. A total of 10 extracted molars were obtained. Each tooth was cut in transversal sections, to create discs (3 mm thick, 10 mm diameter) (control group). Disk specimens of 8 materials were fabricated: polymethyl methacrylate (PMMA) interim material (PMMA-Telio group), 2 resin nanoceramics: (RNC-Ultimate group) and (RNC-Cerasmart group), 2 hybrid ceramics: (HC-Shofu group) and (HC-Enamic group), lithium disilicate (LD-Emax group), zirconia reinforced glass ceramic (ZGC-Suprinity group), and zirconia (Zr group) (n=10). Color measurements were obtained using a spectrophotometer before and after applying 35% hydrogen peroxide-based bleaching agent. Pre- and post-bleaching surface roughness analysis were completed using a profilometer. Significant L*, a*, b*, and ΔE00 values differences were found (P < .05). Color discrepancies (ΔE00) ranged from 0.30 ± 0.14 to 4.82 ± 0.10. The highest color discrepancies were measured on the PMMA-Telio group, while the lowest color discrepancies were computed on the ZGC-Suprinity, RNC-Ultimate, and RNC-Cerasmart. Significant surface roughness differences were found (P <.05). The largest increase of surface roughness values between the pre- and post-bleaching measurements was obtained in the PMMA-Telio group with a mean ΔSa value of 4.73 ± 3.02, while the largest decrease of surface roughness values between the pre- and post-bleaching measurements was obtained in the Zr-InCeram group with a mean ΔSa value of -1.58 ± 0.10. The milled materials tested showed significant pre- and post-bleaching color and surface roughness discrepancies. Int J Prosthodont. doi: 10.11607/ijp.8359.

Predictable esthetics in hybrid and resin-based CAD/CAM restorative materials: Translucency as a function of material thickness.

The CAM of esthetically pleasing monolithic dental restorations presents with specific challenges. One vital parameter to consider is the translucency of the materials. Previous studies have proven a correlation between translucency and material thickness for various all-ceramic materials. The aim of the present study was to assess and define the relationship between thickness and translucency in modern resin-based restorative materials. Specimens fabricated from two resin nano-ceramics (Cerasmart, Lava Ultimate), a polymer-infiltrated ceramic network (Vita Enamic), and a polymethyl methacrylate (Telio CAD) were examined, representing these different material classes. For each material, 12 specimens (n = 12) were fabricated in five thicknesses (0.4, 0.7, 1.0, 1.3, and 1.6 mm; N = 240). The translucency was measured with a spectrophotometer. The total light transmittance for each specimen was calculated applying specialized software. Regression curves were fitted to the results and their coefficient of determination (R2) fit was determined. Logarithmic regression curves showed the best R2 approximation (Cerasmart: R2 = 0.994; Vita Enamic: R2 = 0.978; Lava Ultimate: R2 = 0.997; Telio CAD: R2 = 0.997) to the light transmission values. The results of the present study indicate that the translucency of resin-based materials can be calculated using a mathematic approach to estimate their optical behavior. Cerasmart, Lava Ultimate, Vita Enamic, and Telio CAD exhibit a logarithmic relationship between material thickness and translucency. By determining material-specific coefficients for this logarithmic function, the resulting translucency can be computed for any given material thickness.

Influence of type of restorative materials and surface wetness conditions on intraoral scanning accuracy

ObjectivesTo assess the influence of different restorative materials and surface wetness on intraoral scanning accuracy. MethodsReference casts with an extracted second premolar and first and second molar were digitized (L2). Four groups were established according to the material of the first molar: natural tooth (control), zirconia (Z), lithium disilicate (LD), and nanoceramic resin crown (NC). Four subgroups were developed: dry, low-, mild-, and high-wetness subgroups (n = 15). All the scans were completed by using an intraoral scanner (TRIOS 3). In the control-dry subgroup, the reference cast was dry. In the control-low subgroup, artificial saliva was sprayed with a 1 mL/min volumetric flow for 4 s. In the control-mild and control-high subgroups, the same procedures as in the control-low subgroup were performed, but with a volumetric flow of 4 and of 8 mL/min, respectively. In the Z, LD and NC groups, each crown was fabricated with its respective material. Trueness was analyzed using 2-way ANOVA and Bonferroni tests. The Levene and Bonferroni tests were used to assess precision (α = 0.05). ResultsMaterial (P < .001) and wetness (P < .001) significantly influenced trueness and precision. The mild and high subgroups revealed lower trueness and precision compared with the dry and low subgroups. The control, Z, and LD groups under dry and low wetness conditions showed better trueness compared with the NC group, but the materials tested had no significant precision discrepancies. Under mild wetness conditions, all the materials showed no significant trueness discrepancies. Under high wetness conditions, the LD group demonstrated the best trueness and precision. ConclusionsThe restorative materials and surface wetness tested influenced scanning trueness and precision of the IOS assessed. Clinical significanceDried surfaces are recommended to maximize the scanning accuracy values of the IOS tested. Overall, the presence of saliva and dental restorations can reduce the performance of the IOS tested.