Multiple Stress Creep And Recovery Research Articles

Assessing pavement characteristics: An in-depth evaluation of waste engine oil and Buton rock asphalt composite modified asphalt and its mixture

To investigate the cooperative influence of waste engine oil (WEO) and Buton rock asphalt (BRA) on asphalt characteristics, the WEO/BRA composite modified asphalt and its mixture with varied dosages were prepared. The high-, moderate-, and low-temperature assessments of WEO/BRA composite modified asphalt were conducted through temperature sweep tests, multiple stress creep and recovery (MSCR), and bending beam rheometer (BBR) tests. The softening point difference was used to analyze the storage stability of composite modified asphalt. Based on the Fourier transform infrared spectroscopy (FTIR) and fluorescence microscope (FM) test, the microscopic feature and chemical constitution of WEO/BRA composite modified asphalt were analyzed. Rutting test, low-temperature bending test, immersed Marshall test, freeze-thaw splitting test, and four-point fatigue bending test were carried out to verify the pavement properties of the WEO/BRA composite modified asphalt mixture. The results indicated that WEO improved the capability in low-temperature conditions and fatigue properties of asphalt modified with BRA. BRA enhanced the high-temperature property of asphalt modified with WEO. The synergistic effect of WEO, BRA, and neat asphalt was a physical reaction, and these modifiers were uniformly distributed in the asphalt. Meanwhile, WEO/BRA composite modified asphalt had excellent storage stability for the single modified asphalt. The test results of the asphalt mixture verified the results, indicating that WEO/BRA composite modified asphalt can be considered a new green and durable asphalt pavement material.

Waste coffee biochar and bi-oil composite modified rejuvenated asphalt: Preparation, characterization, and performance evaluation

In the realm of sustainable road construction, bio-oil has emerged as a promising and eco-friendly alternative for rejuvenating aged asphalt. Nevertheless, challenges arise due to poor stability, diminished performance at elevated temperatures, and limited anti-aging properties. This study introduces an innovative approach by blending biochar, obtained from the pyrolysis of waste coffee grounds, into bio-oil to create a composite modified regenerator. Initially, the study conducts a microscopic characterization of the biochar using X-ray diffraction (XRD), scanning electron microscopy (SEM), and energy-dispersive X-ray spectroscopy (EDS). Subsequently, the rheological properties of this composite rejuvenated asphalt are evaluated across low, moderate, and high-temperature ranges using bending beam rheometer (BBR), linear amplitude sweep (LAS), and multiple stress creep and recovery (MSCR) tests. Departing from the traditional emphasis on initial property restoration, it further delves into performance alterations after re-aging of rejuvenated asphalt through temperature sweep (TS) and Fourier transform infrared spectroscopy (FTIR) tests, providing a comprehensive assessment of the anti-aging characteristics of rejuvenated asphalt. Additionally, gel permeation chromatography (GPC) is employed to quantitatively analyze the changes in asphalt molecular weight distribution. The microscopic characterization reveals the development of a rough and porous structure within the biochar, facilitating enhanced adhesion and interaction between the rejuvenator and the asphalt binder. Moreover, bio-oil rejuvenated asphalt exhibits excellent low-temperature crack resistance and moderate-temperature fatigue resistance. Following the incorporation of biochar, notable enhancements in high-temperature rutting resistance and anti-aging properties are observed, validating the efficacy of the biochar with bio-oil composite modified regenerator. To achieve optimal performance outcomes, a biochar content of 6 % (as a proportion of aged asphalt), corresponding to a 1:1 ratio of biochar to bio-oil, is recommended. Under this condition, the properties of the composite modified rejuvenated asphalt demonstrate comparability to those of the original asphalt. In summary, this research underscores the potential for integrating waste coffee biochar material into infrastructure development, thereby promoting circular economy principles and advancing more sustainable construction practices.

Rheological and mechanical evaluation of a novel fast curing cold asphalt concrete made with asphalt emulsion, by-products and magnetic induction

This work studies the feasibility of a new cold asphalt concrete with 5 % voids with fast curing, developed with asphalt emulsion and magnetic induction. Until now, it was impossible to produce fast curing cold asphalt concretes due to the impossibility of compacting and evaporating the water in the asphalt emulsion quickly. Therefore, the aim of this work is to solve the impossibility of compacting the cold asphalt concrete and thus reduce the long curing times. For this purpose, at laboratory level, an experimental cold asphalt concrete was designed with magnetic induction and compared with two reference hot asphalt concretes manufactured according to Spanish standards without magnetic induction (one with 50–70 grade bitumen and another with a PMB45/80–65 type polymer-modified bitumen). The research was carried out in two stages. First, the new cold asphalt concrete was rheologically characterized, the binder recovered from the asphalt concrete was analyzed according to the tests of ring and ball, penetration, dynamic shear rheometer (DSR) and multiple stress creep and recovery (MSCR). Secondly, the new cold concrete asphalt was mechanically characterized, the mechanical performance of the cold asphalt concrete was analyzed by evaluating stability and deformation, dry and wet indirect tensile strengths (ITS), wheel tracking test, stiffness modulus and resistance to raveling dry and wet conditions. Based on the rheological analysis results, the asphalt emulsion recovered from the cold asphalt concrete is extremely soft with a low softening point and a high penetration rate. On the other hand, the values of viscosity, phase angle, stiffness and non-recoverable creep compliance are between those of the bitumen 50/70 and the PMB45/80–65, but closer to bitumen 50/70. As for their mechanical performance, the novel cold asphalt concrete studied presents better resistance to water damage and particle loss, both in dry and wet conditions, but also high permanent deformations and low ITS, probably due to the fact that the residual binder of the emulsion used is softer than the others.

A comparative study into the effect of spent coffee powder and ash on improving the mechanical properties of bitumen

Nowadays, waste and renewable materials are used to modify bitumen and asphalt, reduce costs, decrease the use of natural resources, and maintain ecological balance, and have thus received much attention. This study aimed to improve the rheological properties of bitumen and reduce spent coffee grounds' (SCG) waste by partially replacing it with SCG powder and ash. SCG powder and ash were added in percentages of 0, 1, 3, 5, and 8 wt percent of bitumen to check the properties of control and modified bitumens. Microstructural properties were evaluated by Fourier transform infrared spectroscopy, thermal gravimetric analysis, X-ray fluorescence spectroscopy (XRF), and scanning electron microscopy (SEM). Penetration, softening point, and ductility tests were performed to check the physical properties of bitumens, along with the storage stability test. Rheological tests (viscosity, bending beam rheometer (BBR), dynamic shear rheometer (DSR), multiple stress creep and recovery (MSCR), and linear amplitude sweep (LAS) were also carried out. According to the BBR results, adding SCG powder up to −12 °C and adding SCG ash up to −6 °C increased the resistance to low temperatures. Based on DSR and MSCR results, SCG, either in the form of ash or powder, increased the resistance to rutting, and adding SCG ash improved the high temperature performance of bitumen by 1 grade. At 64 °C, adding 8 % of SCG powder increased the rutting resistance by 43 %, and adding SCG ash raised the rutting resistance by about 113 %. LAS results also showed that SCG ash outperforms SCG powder in fatigue. Although both SCG powder and ash performed well in high, moderate, and low temperatures, SCG powder performed better in cold regions, and SCG ash performed better in regions with temperate and tropical climates.

Investigating the efficacy of bio-rejuvenators in restoring aged asphalt binder properties

The asphalt binder used in pavements oxidizes quickly owing to the elevated temperatures, solar radiation, and exposure to atmospheric oxygen. In this study, epoxidized castor oil (ECO) and acrylated cashew nut shell liquid (ACNSL) were investigated as potential rejuvenators for use as aged binders. The binders were aged in the laboratory using short- and long-term aging methods. The additives and rejuvenated binders were characterized by Fourier transform infrared spectroscopy (FTIR). The properties of the rejuvenated binders were evaluated by frequency sweep, multiple stress creep and recovery (MSCR), and linear amplitude sweep (LAS) tests. The additives improved binder performance, particularly for the sample modified with 15 % cashew nut shell liquid (CNSL). The rheological parameters indicated that both the bio-rejuvenators increased the elasticity of the binder. Regarding the rutting resistance as measured by MSCR test, the results indicated that the sample with the 7 % ACNSL rejuvenated binder exhibited the best rutting resistance at both intermediate and elevated temperatures. Additionally, the fatigue resistance of the sample with 10 % ACNSL was higher than those of the other samples. This study indicates that the bio-oils used are potentially useful as rejuvenating agents for aged binders, thus enabling the recycling of aged asphalt binders.

Mechanistic Fatigue Performance Evaluation of Stone Mastic Asphalt Mixtures: Effect of Asphalt Performance Grade and Elastic Recovery.

This study evaluates the crack performance of stone mastic asphalt (SMA) mixtures according to the performance of a modified asphalt binder, evaluated based on the asphalt performance grade (PG) and the elastic recovery of multiple stress creep and recovery (MSCR) according to AASHTO M 320 and T 350. The cracking performance of the mixture was evaluated using the asphalt mixture performance tester (AMPT) according to AASHTO T 378 and T 400 through dynamic modulus and direct tension cyclic fatigue tests. Furthermore, the recently developed viscoelastic continuum damage (VECD) theory was utilized to evaluate the cyclic fatigue index parameter (apparent damage capacity, Sapp) and the permissible heavy vehicle class. For performance evaluation, six modified asphalt mixtures were prepared and tested using SMA aggregate gradation with a nominal maximum aggregate size (NMAS) of 10 mm. The MSCR test results revealed that, of the six asphalt mixtures, the rubber-based PG76-28 exhibited the least initial strain and the highest elastic recovery. The dynamic modulus test results demonstrated that using a rubber-based modifier increased the elastic modulus at high temperatures and decreased it at low temperatures, thereby enhancing resistance to plastic deformation in the summer and reducing low-temperature cracking in the winter. Finally, the correlation between the Sapp performance index and the elastic recovery of modified asphalt and the number of direct tension cyclic loads until failure of the mixture was evaluated as 0.87 and 0.76, respectively.

Investigation of Rutting and Low Temperature Cracking Behavior of Reactive Ethylene Terpolymer and Waste Cooking Oil Modified Bitumen

With sustainability being the most crucial issue of recent years, the use of waste materials in bitumen modification is increasing and becoming widespread. In this experimental study, it was aimed to investigate the high- and low-temperature behavior of bitumen samples modified with waste cooking oil (WCO), reactive ethylene terpolymer (RET), and polyphosphoric acid (PPA). Accordingly, the multiple stress creep and recovery (MSCR) test and the bending beam rheometer (BBR) test were conducted. Depending on the increasing WCO ratio, the Jnr,R%,∆T_c,and λ parameters of modified bitumens were examined in detail. It was observed that with increasing WCO ratio,the Jnr value increased, and elastic recovery and stiffness decreased. In addition, it has been determined that this composite-modified bitumen is resistant to heavy traffic loads and has sufficient flexibility at low temperatures.

Recovering the properties of aged bitumen using bio-rejuvenators derived from municipal wastes

Ageing of bitumen leads to significant performance deterioration of asphalt pavements and leads to material properties that are not conducive to recycling. Aiming to maximise the reusability of bitumen, this study investigated the feasibility of rejuvenating aged bitumen using bio-based rejuvenators synthesised from municipal wastes. Two bio-rejuvenators were used in this study, namely Rej-A which was a crude polymer with bio-waste pyrolysis dense fractions and Rej-B which was a filtered pyrolysis wax further derived from Rej-A. The bio-rejuvenators, virgin, aged, and rejuvenated bitumen were characterised using a comprehensive testing programme of gas chromatography and mass spectrometry (GC-MS), Fourier-transform infrared spectroscopy (FTIR), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), multiple stress creep and recovery (MSCR), linear amplitude sweep (LAS), and frequency sweep tests. It was observed that both bio-rejuvenators produced in this study can effectively recover the rheological properties of aged bitumen, improving its fatigue performance, e.g. the fatigue lives (at 15 % strain level) of Rej-A and Rej-B rejuvenated bitumen were 5.4 times and 3.0 times of that for aged bitumen when the dosage was 14 %. The rejuvenated bitumen was more sensitive to strain while less sensitive to temperature compared with virgin bitumen. Overall, Rej-A outperformed Rej-B in recovering the properties of aged bitumen. However, Rej-A was thermally unstable, undergoing 15.6 % mass loss when heated to 160 °C.

Effect of Salt Solution Environment on the Aging of Styrene-Butadiene-Styrene (SBS)-Modified Asphalt.

The aim of this paper is to investigate the aging mechanism of asphalt in the sea salt erosion environment from a rheological point of view. In order to simulate the real pavement aging process in the sea salt erosion environment, base asphalt and Styrene-Butadiene-Styrene (SBS)-modified asphalt were selected for salt environment aging tests. The asphalt samples were aged via a thin film oven test (TFOT) and a pressure aging vessel (PAV) test. Then, thermo-oxidizing conditions were created after the samples were immersed in salt solution, mixed with four different concentrations of sodium chloride (NaCl) and sodium sulphate (Na2SO4), to investigate the aging state of asphalt. Temperature scan (TS), frequency scan (FS), and multiple stress creep and recovery (MSCR) tests performed using a Dynamic Shear Rheometer (DSR) were used to investigate the effects on the rheological properties of aged asphalt in a salt environment. The results showed that both base asphalt and SBS-modified asphalt were aged to different degrees under mixed salt solutions. The two asphalt samples aged in a salt environment showed increased hardness. SBS-modified asphalt exhibited higher aging resistance compared with base asphalt in the sea salt environment. However, due to the degradation of the SBS modifier and the aging of base asphalt, the properties of the SBS-modified asphalt showed more obvious complexity with changes in salt solution concentrations.

Anti-ageing and rheological performance of bitumen modified with polyaniline nanofibres

Asphalt pavements represent the great majority of roads worldwide. However, the bitumen physico-chemical properties change due to ageing processes during both the production and service life of the asphalt mixes. In recent years, a completely new trend has been observed in the road engineering industry oriented to extending the service life of roads, bringing direct economic, ecological and social benefits. This work presents the possibility of inhibiting ageing of road bitumen by using polyaniline nanofibers (PANI_NFs) as well as enhancing its rheological properties examined with Linear Amplitude Sweep (LAS) as well as Multiple Stress Creep and Recovery (MSCR) tests. These results show that the application of PANI_NFs maintains the primary penetration value of bitumen short-term and long-term aged road bitumen at 88 % and 52 %, respectively. Moreover, bitumen modification with PANI_NFs reduces the softening temperature increase by 33 % and 24 %, respectively, and the viscosity increase of road asphalt by 50 % and 25 %, respectively. PANI_NFs also stabilised the bitumen surface adhesion force, determined with AFM, consequently confirming the enhanced resistance to ageing processes. In addition, changes in the carbonyl index, sulphoxide index and aromaticity of bitumen demonstrated that PANI_NFs inhibit oxidation and aromatisation reactions of its components. The tests indicated a 4-fold decrease in the degree of bitumen component oxidation after short-term ageing and a 33 % decrease after long-term ageing. FTIR analysis also showed a reduction in the degree of bitumen component aromatisation process of 79 % and 76 % for short-term and long-term ageing, respectively. The LAS and MSCR test results also showed that PANI_NFs had a beneficial impact on the resistance of the bitumen to fatigue and rutting. Overall, the study results suggest that PANI_NFs consitute a promising modifier for bitumen in terms of ageing inhibition and performance characteristics.

Effects of Waste Lubricant Oil on Rheological Properties of Asphalt Binders: Implications for Sustainable Asphalt Mixture Production

Reusing waste lubricant oil as an environmentally-friendly alternative for disposal and transforming it into a value-added product is a promising solution. This study aimed to evaluate the rheological properties of asphalt binder (PG 64-XX) modified with waste hydraulic oil. Two levels of oil content, 3% and 5% by weight of the base binder, were added. Physical and rheological tests, including penetration, softening point, rotational viscosity, and performance grade (PG) tests, were conducted before and after subjecting the samples to the Rolling Thin Film Oven (RTFO), multiple stress creep and recovery (MSCR), linear amplitude sweep (LAS), and master curve procedures. Results showed that the addition of oil decreased the stiffness of the base binder, makingit more susceptible to premature cracking and instability. However, the mixture and compaction temperatures decreased with the oil addition. Overall, considering the investigated oil contents, the asphalt binders modified with waste hydraulic oil did not exhibit satisfactory performance. It is hypothesized that incorporating residual hydraulic oil in recovered asphalt binders may yield more favorable results.

Effect of Industrial Solid Waste as Fillers on the Rheology and Surface Free Energy of Asphalt Mastic.

The continuous growth of industrial solid waste production has generated many environmental problems. We evaluated the potential of industrial solid waste as a substitute filler in asphalt mastic, with the aim of increasing the use of sustainable road construction materials. In this study, X-ray fluorescence spectroscopy (XRF) and scanning electron microscopy (SEM) were used to characterize the oxide composition and micromorphology of limestone (LS), red mud (RM), steel slag (SS), and ground granulated blast-furnace slag (GGBFS). Four asphalt mastics containing LS, RM, SS, and GGBFS with a filler-to-binder weight ratio of one were prepared. An evaluation of the rheology and wetting of the solid-waste-filler asphalt mastic was conducted using a frequency sweep, temperature sweep, linear amplitude sweep (LAS), multiple stress creep and recovery (MSCR), and surface free energy (SFE) methods. The results showed that SS increased the complex modulus, elastic component of the asphalt mastic and decreased the nonrecoverable creep compliance at stress levels of 0.1 and 3.2 kPa, which improved the rutting resistance of the asphalt mastic and reduced deformation under high-temperature conditions. The RM and GGBFS increased the fatigue performance of the asphalt mastic under strain loading, enhanced its fatigue life, and maintained good performance under long-term loading. The dispersive component of the SFE parameter of the solid-waste-filler asphalt mastic was larger than the polar component for the largest share of the surface energy composition. The SFE of the asphalt mastic prepared from the industrial solid-waste filler was reduced; however, the difference was insignificant compared to the limestone asphalt mastic. Solid-waste-filler asphalt mastic has performance characteristics, and its actual application can be based on different performance characteristics to select an appropriate solid-waste filler. The results of this study provide new technological solutions for solving the utilization rate of solid waste materials and sustainable road construction in the future.

Application of the Air-Jet Laser Detection Technology for Asphalt Binders

AbstractA fast and convenient technique for Asphalt Binders was proposed in this paper, which was based on air-jet pressurized and laser to detect the transient deformation and creep recovery of asphalt. Taking five kinds of asphalt and modified asphalt commonly used in China as the research objects, the performance of asphalt were tested and analyzed by adopting the Penetration Test, Dynamic Shear Rheological (DSR) Test, Multiple Stress Creep and Recovery (MSCR) Test and the proposed test technology. The results verified the feasibility of the proposed test technology and the correlation between the traditional tests and the proposed test technology. The results demonstrated that the proposed test technology had good discrimination ability for different kinds of asphalt and could effectively reflect the performance differences. The new test protocol was similar to the Penetration Test. There was a significant correlation between the maximum deformation index and penetration index. The correlation coefficient was above 0.8, and the p value was much less than 0.01. It could be used as a possible alternative to the Penetration Test. The proposed new test was relatively convenient and fast compared with the dynamic shear test. There was a linear correlation between the maximum deflection index and the complex shear modulus G*, and the correlation coefficient between the recovery index and the phase angle is above 0.8, which indicated that the proposed new test and the DSR test had a significant correlation. There was also a good correlation between the creep recovery index of MSCR test and the recovery data of the proposed new test method. The research results provided a new solution for the performance test and evaluation of asphalt in China.

Unraveling the critical indicators for evaluating the high-temperature performance of rejuvenator-aged bitumen blends

This study aims to systematically investigate the influence of rejuvenator type/dosage and the aging degree of bitumen on the rutting resistance, flow behavior, and elastic/creep potential of rejuvenated bitumen at high temperatures. The rutting parameter (G*/sinδ), rutting failure temperature (RFT) from Linear viscoelastic test (LVE), zero-shear viscosity (ZSV) from flow test, recovery percentage (R0.1, R3.2), creep compliance (Jnr0.1, Jnr3.2), and stress sensitivity parameters (Rdiff, Jnrslope) from multiple stress creep and recovery (MSCR) tests of rejuvenated bitumen are characterized. The results reveal that bio-oil rejuvenator weakens the high-temperature performance of aged bitumen maximally, followed by engine-oil and naphthenic-oil, while aromatic-oil rejuvenated bitumen exhibits the best rutting, flow, and creep resistance. The RFT index can most effectively evaluate and differentiate the rejuvenation efficiency of various rejuvenators on the high-temperature performance, which correlates well with ZSV, R3.2, Jnr0.1, Jnr3.2, Rdiff, and Jnrslope indices. Therefore, the RFT index is recommended as the critical indicator for evaluating the high-temperature performance of rejuvenated binders. The flow and MSCR characteristics of rejuvenated bitumen can be predicted based on RFT values. The determination of critical indicators is beneficial to compare the rejuvenation effectiveness of variable rejuvenators on the high-temperature performance of aged bitumen.

Study on optimal preparation and rheological characteristics of waste low density polyethylene (LDPE)/styrene butadiene styrene (SBS) composite modified asphalt binder

The sustainable utilization of waste low density polyethylene (LDPE) in asphalt pavements has enormous environmental and economic benefits. To enhance and benefit more from LDPE, this study deals with use of LDPE and styrene butadiene styrene (SBS) collectively for composite modification of asphalt binder. The study intends to identify the optimal blending parameters of LDPE/SBS composite modified asphalt binder by using the orthogonal experiment. The paper deals with the investigation of conventional properties and rheological properties such as Penetration, softening point, ductility, Superpave rutting parameter (G*/sinδ), failing temperature, rotational viscosity and multiple stress creep and recovery (MSCR) test parameters of the binder. Moreover, the dispersion of modifiers in asphalt binder is studied by optical microscopy. The test results point out that the optimal blending parameter for preparing LDPE/SBS composite modified asphalt is 90 min of blending at 180 °C maintaining a rate of 2500 rpm. The blending time parameter has the highest influence on the properties, with the blending temperature and blending rate having a relatively lower impact. Although, both the LDPE and SBS individually have a good impact on high temperature characteristics of asphalt binder but together as a composite, in addition to showing improved high temperature properties, they also reveal high resistance towards permanent deformation and better elastic behaviour. It is concluded that the LDPE/SBS composite modified asphalt binder performs well and is recommended better for high temperature climates. Furthermore, it is good way to enhance the application of LDPE in pavement industry and promote environmental sustainability.

Effect of superficially modified zinc oxide nanoparticles as an additive on the rheological performance of asphalt binder

The surface effect that hinders the dispersion of nanomaterials in the asphalt binder due to the large surface area and small particle size should be investigated. Thus, this study evaluates the effect of the incorporation of superficially modified zinc oxide nanoparticles (ZnO M) by 3-(2.3-epoxypropoxy)propyl trimethoxysilane (GPTMS) in the asphalt binder with 50/70 penetration index. The additive was incorporated in contents of 3%, 5%, and 7% in weight of the bind through physical and rheological tests. Penetration tests, softening point, rotational viscosity, performance grade (PG) – before and after rolling thin film oven (RTFO), multiple stress creep and recovery (MSCR), linear amplitude sweep (LAS), and master curve were performed. The addition of ZnO M nanoparticles provided the asphalt binder with more resistance to aging and oxidation in almost all properties analysed. In addition, the ZnO M increased resistance to permanent deformation, temperature field, and the integrity of the asphalt binder, thus increasing its fatigue life.

Approach for accurately characterizing nonlinear viscoelastic and nonrecoverable properties of asphalt binders based on MSCR test

The multiple stress creep and recovery (MSCR) test has been widely accepted as a more practical method for accessing the rutting performance of asphalt binders than the conventional Superpave rutting factor test. Nevertheless, there still exists a major concern that 9-s recovery time in each cycle may not guarantee a sufficient recovery of the recoverable viscoelastic strain, especially for modified asphalts, and this could result in a potential inaccuracy in characterizing rutting resistance of binders. To effectively separate the recoverable nonlinear viscoelastic (NLVE) and nonrecoverable responses in the MSCR test, this paper presents a new approach that adopts an additional one-cycle low-stress creep and recovery (LSCR) test and the Schapery’s NLVE model in analyzing the MSCR test data. The LSCR test, covering the entire duration of the MSCR test (200 s), can well determine the linear viscoelastic (LVE) recoverable properties that the Schapery’s model requires for NLVE analysis. The results show that with the recoverable and nonrecoverable responses accurately isolated, the proposed approach rigorously redefines the indicators of the percent recovery R and nonrecoverable creep compliance Jnr in the MSCR test, and therefore effectively eliminates the inaccuracy of the original indicators caused by incomplete recovery of the recoverable strain component in each cycle. Also, the developed method exactly characterizes stress dependence and permanent deformation resistance of asphalt binder, thus offering an effective and accurate approach for high-temperature performance evaluation of asphalt binders.

Enhancement of rheological performance and compatibility of tire rubber-modified asphalt binder with the addition of graphene

Rubber segregation and workability are issues associated with tire rubber powder (TRP) modified asphalt binder, restricting its widespread application. Meanwhile, graphene nanoparticles have gained considerable interest in asphalt modification due to their outstanding properties. This work has explored the influence of graphene incorporation on the compatibility and rheological behavior of TRP-modified asphalt binder. Firstly, TRP-modified asphalt and two kinds of TRP/graphene composite-modified asphalt were prepared. Then, the rheological characteristics of the asphalts were investigated using the frequency sweep, temperature sweep, multiple stress creep and recovery (MSCR), linear amplitude sweep (LAS), and bending beam rheometer (BBR) tests. The compatibility and microstructure of the different modified asphalt binders were evaluated using the cigar tube test and scanning electron microscopy. Results showed that adding graphene to the TRP-modified asphalt resulted in a notable improvement in rutting performance, as evidenced by the increase in rutting parameter (G*/sinδ) and % recovery (R) and a decrease in non-recoverable creep compliance (Jnr). The graphene addition also enhanced the anti-aging performance of TRP-modified asphalt. The results obtained from the LAS test, including the damage-characteristic curves and the number of cycles to fatigue failure, suggested that the fatigue performance of the TRP/graphene composite-modified asphalt was higher compared to the TRP-modified asphalt. Similarly, the BBR test results with 12% TRP and 0.5% graphene demonstrated that the composite-modified asphalt was more resistant to low-temperature cracking. Finally, the incorporation of graphene can potentially reduce the degree of phase separation in TRP-modified asphalt binder and improve its compatibility.

Developing deterministic and probabilistic prediction models to evaluate high-temperature performance of modified bitumens

This study aims to develop deterministic and probabilistic prediction models for the multiple stress creep and recovery (MSCR) test. For this purpose, crumb rubber, polyphosphoric acid, and styrene–butadiene–styrene bitumen modifiers have been used with different dosages to modify high-temperature performance of PG 58–28 and PG 64–22 base bitumens. The MSCR test has been performed at different temperatures. Deterministic models are developed by the multi-gene genetic programming technique for each modifier individually, and the non-recoverable creep compliance (Jnr) and percent recovery (R) parameters are predicted. The accuracy of deterministic models is suitable and the performance of R models has been better than Jnr models. Furthermore, a comprehensive probabilistic model has been developed by using the logistic regression technique to predict different traffic levels. The accuracy of the probabilistic model is 0.85. The sensitivity analysis has been performed on this model and the effect of changes in the modifier dosage and temperature on the traffic levels have been investigated. Results show that using the probabilistic model, it is possible to find a range of modifier’s dosage in which the traffic level is desired.

Rheological performance of bitumen mixed with laboratory simulated polymerized RAP binders

Researchers have mostly used three artificial aging techniques, namely pressure aging vessel (PAV) binder aging, compacted mix aging (CMA), and loose mix aging (LMA) to simulate recycled asphalt pavement (RAP) binder in the laboratory. RAP binder (RAPB) simulated using different techniques will differ in characteristics and may affect the performance of the base binder differently. Which may affect the parameters used for blending and recycling, such as the selection of base binder, rejuvenator dosage, etc. Therefore, in this study, three RAP binders, namely RAPB-P, RAPB-C, and RAPB-L, were simulated from a polymer modified binder (PMB) with 3.5% SBS content, using PAV aging (100 °C, 20 hrs, 2.1 MPa), CMA (85 °C, 5 days) and LMA (85 °C, 8 days), respectively. These polymerized RAPBs were added to an unmodified binder (AC 30) at three proportions: 15 %, 25 %, and 40 %. These RAPB and AC 30 blends were characterized in terms of their dynamic viscosity, mixing and compaction temperature, and high temperature performance grade (PG). Superpave rutting factor (|G*|/sin δ) and multiple stress creep and recovery (MSCR) test parameters were used to evaluate the rutting performance of the RAPB blended AC 30 binders. Further, resistance to yielding and elastic recovery values were evaluated using the binder yield energy test (BYET). The test results suggested that all three RAP binders affect the performance of the AC 30 binder differently, which was also confirmed by statistical analysis using one-way ANOVA. From MSCR and BYET test results, it may be stated that RAP binder simulated from standard PAV aging may mislead in predicting the high and intermediate temperature performance of AC 30 binder with RAPB. Overall, the present study is helpful for asphalt researchers and practitioners to understand how the selection of different defined aging strategies affects the performance of aged recycled PMB with unmodified base binder.