MPa Effective Normal Stress Research Articles

Activation of Dissolution‐Precipitation Creep Causes Weakening and Viscous Behavior in Experimentally Deformed Antigorite

AbstractAntigorite occurs at seismogenic depth along plate boundary shear zones, particularly in subduction and oceanic transform settings, and has been suggested to control a low‐strength bulk rheology. To constrain dominant deformation mechanisms, we perform hydrothermal ring‐shear experiments on antigorite and antigorite‐quartz mixtures at temperatures between 20 and 500°C at 150 MPa effective normal stress. Pure antigorite is strain hardening, with frictional coefficient (μ) > 0.5, and developed cataclastic microstructures. In contrast, antigorite‐quartz mixtures (10% quartz) are strain weakening with μ decreasing with temperature from 0.36 at 200°C to 0.22 at 500°C. Antigorite‐quartz mixtures developed foliation similar to natural serpentinite shear zones. Although antigorite‐quartz reactions may form mechanically weak talc, we only find small, localized amounts of talc in our deformed samples, and room temperature friction is higher than expected for talc. Instead, we propose that the observed weakening at temperatures ≥200°C primarily results from silica dissolution leading to a lowered pore‐fluid pH that increases antigorite solubility and dissolution rate and thus the rate of dissolution‐precipitation creep. We suggest that under our experimental conditions, efficient dissolution‐precipitation creep coupled to grain boundary sliding results in a mechanically weak frictional‐viscous rheology. Antigorite with this rheology is much weaker than antigorite deforming frictionally, and strength is sensitive to effective normal stress and strain rate. The activation of dissolution‐precipitation in antigorite may allow steady or transient creep at low driving stress where antigorite solubility and dissolution rate are high relative to strain rate, for example, in faults juxtaposing serpentinite with quartz‐bearing rocks.

Frictional stability and hydromechanical coupling of serpentinite-bearing fault gouge

SUMMARY Observations of slow earthquakes and tremor have raised fundamental questions about the physics of quasi-dynamic rupture and the underlying fault zone processes. The presence of serpentinite at P-T conditions characteristic of deep tremor and slow earthquakes suggests that it plays an important role in controlling complex fault slip behaviour. Here, we report on experiments designed to investigate the frictional behaviour of serpentinite sampled from outcrop exposures (SO1 and SO2) of altered ultramafic rocks present at depth, and recovered from the SAFOD borehole (G27). XRD analyses reveal the presence of chrisotyle, lizardite, kaolinite, talc in SO1; lizardite, clinochlore and magnetite in SO2; and lizardite, quartz and calcite in G27. We sheared fault gouge in a double-direct shear configuration using a true triaxial deformation apparatus. The effective normal stress was varied from 2 to 40 MPa. We conducted velocity stepping tests and slide-hold-slide (SHS) tests in each experiment to characterize frictional stability and healing. At the end of each experiment, post-shear permeability was measured and the samples were recovered for microstructural analysis. The steady-state friction coefficient was μ = 0.17 for SO1, μ = 0.33 for SO2 and μ = 0.53 for G27. Overall, the gouges exhibit velocity strengthening behaviour, and become nearly velocity neutral at 40 MPa effective normal stress. SHS tests show positive healing rates for SO2 and G27, whereas SO1 exhibits zero or negative healing rates. Permeability decreases with increasing σn’, with SO1 (k = 10–20 m2) showing the lowest values. Microstructural observations reveal a well-developed R-Y-P fabric in SO1, which is not observed in SO2 and G27. We posit that the development of shear fabric controlled by mineralogy governs frictional and hydrological properties. In this context, when serpentinite is associated with other weak phyllosilicate minerals, frictional stability and hydrological properties can vary greatly, with a potential control on the mode of fault failure.

Frictional slip weakening and shear-enhanced crystallinity in simulated coal fault gouges at slow slip rates

Abstract. Previous studies show that organic-rich fault patches may play an important role in promoting unstable fault slip. However, the frictional properties of rock materials with nearly 100 % organic content, e.g., coal, and the controlling microscale mechanisms remain unclear. Here, we report seven velocity stepping (VS) experiments and one slide–hold–slide (SHS) friction experiment performed on simulated fault gouges prepared from bituminous coal collected from the upper Silesian Basin of Poland. These experiments were performed at 25–45 MPa effective normal stress and 100 ∘C, employing sliding velocities of 0.1–100 µm s−1 and using a conventional triaxial apparatus plus direct shear assembly. All samples showed marked slip-weakening behavior at shear displacements beyond ∼ 1–2 mm, from a peak friction coefficient approaching ∼0.5 to (nearly) steady-state values of ∼0.3, regardless of effective normal stress or whether vacuum-dry or flooded with distilled (DI) water at 15 MPa pore fluid pressure. Analysis of both unsheared and sheared samples by means of microstructural observation, micro-area X-ray diffraction (XRD) and Raman spectroscopy suggests that the marked slip-weakening behavior can be attributed to the development of R-, B- and Y-shear bands, with internal shear-enhanced coal crystallinity development. The SHS experiment performed showed a transient peak healing (restrengthening) effect that increased with the logarithm of hold time at a linearized rate of ∼0.006. We also determined the rate dependence of steady-state friction for all VS samples using a full rate and state friction approach. This showed a transition from velocity strengthening to velocity weakening at slip velocities >1 µm s−1 in the coal sample under vacuum-dry conditions but at >10 µm s−1 in coal samples exposed to DI water at 15 MPa pore pressure. The observed behavior may be controlled by competition between dilatant granular flow and compaction enhanced by the presence of water. Together with our previous work on the frictional properties of coal–shale mixtures, our results imply that the presence of a weak, coal-dominated patch on faults that cut or smear out coal seams may promote unstable, seismogenic slip behavior, though the importance of this in enhancing either induced or natural seismicity depends on local conditions.

Healing Behavior of Simulated Fault Gouges From the Groningen Gas Field and Implications for Induced Fault Reactivation.

We investigated the frictional strength recovery (healing) and subsequent reactivation and slip‐weakening behavior of simulated fault gouges derived from key stratigraphic units in the seismogenic Groningen gas field (N. E. Netherlands). Direct‐shear, slide‐hold‐slide (SHS) experiments were performed at in situ conditions of 100 °C, 40 MPa effective normal stress and 10–15 MPa pore fluid pressure (synthetic formation brine). Sheared gouges were allowed to heal for periods up to 100 days before subsequent reshearing. The initial coefficient of (steady) sliding friction μ was highest in the Basal Zechstein caprock (μ = 0.65 ± 0.02) and Slochteren sandstone reservoir (μ = 0.61 ± 0.02) gouges, and the lowest in the Ten Boer claystone at the reservoir top (μ = 0.38 ± 0.01) and in the Carboniferous shale substrate (μ ≈ 0.45). Healing and subsequent reactivation led to a marked increase (∆μ) in (static) friction coefficient of up to ~0.16 in Basal Zechstein and ~0.07 in Slochteren sandstone gouges for the longest hold periods investigated, followed by a sharp strength drop (up to ~25%) and slip‐weakening trajectory. By contrast, the Ten Boer and Carboniferous gouges showed virtually no healing or strength drop. Healing rates in the Basal Zechstein and Slochteren sandstone gouges were significantly affected by the stiffness of different machines used, in line with the Ruina slip law, and with a microphysical model for gouge healing. Our results point to marked stratigraphic variation in healed frictional strength and healing rate of faults in the Groningen system, and high seismogenic potential of healed faults cutting the reservoir and Basal Zechstein caprock units, upon reactivation.

Frictional properties of simulated shale-coal fault gouges: Implications for induced seismicity in source rocks below Europe's largest gas field

We report 21 frictional sliding experiments performed on simulated fault gouges prepared from shale-coal mixtures. Our aim was to investigate the effects of local coal seam smearing on the frictional properties and induced seismogenic potential of faults cutting the Upper Carboniferous source rocks underlying the Groningen gas reservoir (Netherlands). We used shale/siltstone core recovered from beneath the Groningen reservoir plus Polish bituminous coal of similar age and origin to coals locally present in the Groningen source rocks. We performed friction experiments in velocity stepping, constant velocity, slide-hold-slide (SHS) and slide-unload-slide (SUS) modes, under near in-situ conditions of 100 °C and 40 MPa effective normal stress, employing sliding velocities of 0.1–100 μm/s and a variety of pore fluids. Samples with 0–50 vol% coal showed friction coefficients ~0.45, with minor slip weakening. Samples with ≥50 vol% coal showed marked slip-weakening from peak friction values of ~0.47 to ~0.3, regardless of experimental conditions, presumably reflecting strain localization in weak coal-rich shear bands, possibly accompanied by changes in coal molecular structure. However, re-sliding experiments (SUS) showed that slip-weakening is limited to small initial displacements (2–3 mm), and does not occur during slip reactivation. At (near) steady state, almost all experiments performed at in-situ stress, pore water pressure (15 MPa) and temperature conditions exhibited stable, velocity strengthening behaviour, regardless of coal content. By contrast, under dry and gas-saturated (CH4, Argon) conditions, or using water at 1 atm, 50:50 (vol%) shale-coal mixtures showed velocity-weakening and even stick-slip. Our results imply that faults in the Groningen Carboniferous shale-siltstone sequence are not prone to induced earthquake nucleation at in-situ conditions, even when coal-bearing or coal-enriched by smearing. However, the mechanisms controlling coal friction remain unclear at the sliding velocities studied, and the evolution of coal friction at seismic slip velocities remains unknown.

Lower crustal earthquakes in the East African Rift System: Insights from frictional properties of rock samples from the Malawi rift

Earthquakes in the southern part of the East African Rift System (EARS) occur at depths up to 45 km in the lower crust, unusually deep for an extensional regime. Typically, earthquakes in continental crust nucleate at temperatures <350 °C, the temperature at which crystal plastic creep in quartz becomes efficient, corresponding to a depth of ~15 km with an average continental geothermal gradient. Several hypotheses have been proposed to explain the deep seismicity in the EARS, including the presence of high-viscosity mafic material, an abnormally low geotherm, locally elevated strain rates, or high fluid pressures. Here, we provide frictional properties of simulated fault gouges to address the seismic behavior of felsic and mafic crystalline basement rocks from the amagmatic Malawi Rift at the southern, propagating end of the EARS. Rotary shear experiments are conducted at 100, 200, and 250 MPa effective normal stress, a fluid pressure of 100 MPa and from room temperature to 700 °C. The friction of the felsic sample (58% plagioclase) is fairly constant up until 400 °C, after which it decreases. At temperatures of 600 °C and above, the relation between shear stress and effective normal stress deviates from linearity. The friction coefficient of the mafic sample is nearly constant in the considered range of temperature and normal stress and the sample shows a linear relation between normal stress and shear stress. The mafic sample also has negative, and decreasing, (a-b) values at temperatures >400 °C. These results are consistent with earthquake nucleation in mafic material, if present, at lower crustal P-T conditions. On the other hand, the data indicate that earthquake nucleation is unlikely in felsic material at temperatures above 500 °C, unless effective normal stress is low and strain rate is elevated by several orders of magnitude.

Frictional Properties of Simulated Fault Gouges from the Seismogenic Groningen Gas Field Under In Situ P–T ‐Chemical Conditions

AbstractWe investigated the frictional properties of simulated fault gouges derived from the main lithologies present in the seismogenic Groningen gas field (NE Netherlands), employing in situ P–T conditions and varying pore fluid salinity. Direct shear experiments were performed on gouges prepared from the Carboniferous shale/siltstone substrate, the Upper Rotliegend Slochteren sandstone reservoir, the overlying Ten Boer claystone, and the Basal Zechstein anhydrite–carbonate caprock, at 100°C, 40 MPa effective normal stress, and sliding velocities of 0.1–10 μm/s. As pore fluids, we used pure water, 0.5–6.2 M NaCl solutions, and a 6.9 M mixed chloride brine mimicking the formation fluid. Our results show a marked mechanical stratigraphy, with a maximum friction coefficient (μ) of ~0.66 for the Basal Zechstein, a minimum of ~0.37 for the Ten Boer claystone, ~0.6 for the reservoir sandstone, and ~0.5 for the Carboniferous. Mixed gouges showed intermediate μ values. Pore fluid salinity had no effect on frictional strength. Most gouges showed velocity‐strengthening behavior, with little systematic effect of pore fluid salinity or sliding velocity on (a–b). However, Basal Zechstein gouge showed velocity weakening at low salinities and/or sliding velocities, as did 50:50 mixtures with sandstone gouge, tested with the 6.9 M reservoir brine. From a rate and state friction viewpoint, our results imply that faults incorporating Basal Zechstein anhydrite–carbonate material at the top of the reservoir are the most prone to accelerating slip, that is, have the highest seismogenic potential. The results are equally relevant to other Rotliegend fields in the Netherlands and N. Sea region and to similar sequences globally.

Conversion of Wet Glass to Melt at Lower Seismogenic Zone Conditions: Implications for Pseudotachylyte Creep

AbstractCoseismic frictional melting and the production of quenched glass called pseudotachylyte is a recurring process during earthquakes. To investigate how glassy materials affect the postseismic strength and stability of faults, obsidian gouges were sheared under dry and wet conditions from 200°C to 300°C at ~150 MPa effective normal stress. Dry glass exhibited a brittle rheology at all conditions tested, exhibiting friction values and microstructures consistent with siliciclastic materials. Likewise, wet glass at 200°C exhibited a brittle rheology. In contrast, wet gouges at 300°C transitioned from brittle sliding to linear‐viscous (Newtonian) flow at strain rates &lt;3 × 10−4 s−1, indicating melt‐like behavior. The viscosity ranged from 2 × 1011 to 7.8 × 1011 Pa‐s. Microstructures show that viscous gouges were fully welded with rod‐shaped microlites rotated into the flow direction. Fourier transform infrared spectroscopy along with electron backscatter imaging demonstrate that hydration of the glass by diffusion of pore water was the dominant process reducing the viscosity and promoting viscous flow. As much as 5 wt % water diffused into the glass. These results may provide insight into postseismic‐slip behaviors and challenge some interpretations of fault kinematics based on studies assuming that pseudotachylyte formation and flow is solely coseismic.

Interseismic re-strengthening and stabilization of carbonate faults by “non-Dieterich” healing under hydrothermal conditions

Friction experiments, consisting of a “velocity stepping” stage, a “slide-hold-slide” (SHS) stage and a second “velocity stepping” stage, have been performed to study the frictional healing behavior of carbonate fault gouge, and the effects of healing on the velocity dependence of friction, at 20–140 °C and at 50 MPa effective normal stress. Dry experiments show classical Dieterich healing characterized by a transient peak in friction after each hold period, with no effects of SHS testing on steady-state friction or velocity dependence. By contrast, the wet tests show 1) an increase in apparent steady-state friction upon re-sliding after a hold period, and 2) a pronounced increase in the velocity dependence parameter, (a−b), after the SHS stage. While the first of these “non-Dieterich-type” healing effects has been observed in previous hydrothermal experiments on simulated quartz gouges, it has not been reported previously for carbonate gouges. The observed effect of SHS-testing on (a−b) has never been reported. Our findings suggest that, under in-situ hydrothermal conditions, interseismic fluid-assisted deformation processes, such as pressure solution, can significantly promote fault re-strengthening in carbonates and can cause slip stabilization. If the results are applicable to active faults in carbonate terrains, they have important implications for understanding how the extent of the seismogenic zone, and how earthquake magnitude and aftershock distributions, may evolve with repeated cycles of natural seismicity and interseismic healing.

Effective strength of incoming sediments and its implications for plate boundary propagation: Nankai and Costa Rica as type examples of accreting vs. erosive convergent margins

The location of the seaward tip of a subduction thrust controls material transfer at convergent plate margins, and hence global mass balances. At approximately half of those margins, the material of the subducting plate is completely underthrust so that no accretion or even subduction erosion takes place. Along the remaining margins, material is scraped off the subducting plate and added to the upper plate by frontal accretion. We here examine the physical properties of subducting sediments off Costa Rica and Nankai, type examples for an erosional and an accretionary margin, to investigate which parameters control the level where the frontal thrust cuts into the incoming sediment pile. A series of rotary-shear experiments to measure the frictional strength of the various lithologies entering the two subduction zones were carried out. Results include the following findings: (1) At Costa Rica, clay-rich strata at the top of the incoming succession have the lowest strength (μres = 0.19) while underlying calcareous ooze, chalk and diatomite are strong (up to μres = 0.43; μpeak = 0.56). Hence the entire sediment package is underthrust. (2) Off Japan, clay-rich deposits within the lower Shikoku Basin inventory are weakest (μres = 0.13–0.19) and favour the frontal proto-thrust to migrate into one particular horizon between sandy, competent turbidites below and ash-bearing mud above. (3) Taking in situ data and earlier geotechnical testing into account, it is suggested that mineralogical composition rather than pore-pressure defines the position of the frontal thrust, which locates in the weakest, clay mineral-rich (up to 85 wt.%) materials. (4) Smectite, the dominant clay mineral phase at either margin, shows rate strengthening and stable sliding in the frontal 50 km of the subduction thrust (0.0001–0.1 mm/s, 0.5–25 MPa effective normal stress). (5) Progressive illitization of smectite cannot explain seismogenesis, because illite-rich samples also show velocity strengthening at the conditions tested.

Physical properties of surface outcrop cataclastic fault rocks, Alpine Fault, New Zealand

We present a unified analysis of physical properties of cataclastic fault rocks collected from surface exposures of the central Alpine Fault at Gaunt Creek and Waikukupa River, New Zealand. Friction experiments on fault gouge and intact samples of cataclasite were conducted at 30–33 MPa effective normal stress (σn′) using a double‐direct shear configuration and controlled pore fluid pressure in a true triaxial pressure vessel. Samples from a scarp outcrop on the southwest bank of Gaunt Creek display (1) an increase in fault normal permeability (k = 7.45 × 10−20 m2 to k = 1.15 × 10−16 m2), (2) a transition from frictionally weak (μ = 0.44) fault gouge to frictionally strong (μ = 0.50–0.55) cataclasite, (3) a change in friction rate dependence (a‐b) from solely velocity strengthening, to velocity strengthening and weakening, and (4) an increase in the rate of frictional healing with increasing distance from the footwall fluvioglacial gravels contact. At Gaunt Creek, alteration of the primary clay minerals chlorite and illite/muscovite to smectite, kaolinite, and goethite accompanies an increase in friction coefficient (μ = 0.31 to μ = 0.44) and fault‐perpendicular permeability (k = 3.10 × 10−20 m2 to k = 7.45 × 10−20 m2). Comminution of frictionally strong (μ = 0.51–0.57) cataclasites forms weaker (μ = 0.31–0.50) foliated cataclasites and fault gouges with behaviors associated with aseismic creep at low strain rates. Combined with published evidence of large magnitude (Mw ∼ 8) surface ruptures on the Alpine Fault, petrological observations indicate that shear failure involved frictional sliding within previously formed, velocity‐strengthening fault gouge.

Comparison of frictional strength and velocity dependence between fault zones in the Nankai accretionary complex

Accretionary complexes host a variety of fault zones that accommodate plate convergence and internal prism deformation, including the décollement, imbricate thrusts, and out‐of‐sequence thrusts or splays. These faults, especially the décollement and major splay faults, are considered to be candidates for hosting slow slip events and large magnitude earthquakes, but it is not clear what modes of slip should be expected at shallow levels or how they are related to fault rock frictional properties. We conducted laboratory experiments to measure the frictional properties of fault and wall rock from three distinct fault zone systems sampled during Integrated Ocean Drilling Program Expedition 316 and Ocean Drilling Program Leg 190 to the Nankai Trough offshore Japan. These are (1) a major out‐of‐sequence thrust fault, termed the “megasplay” (Site C0004), (2) the frontal thrust zone, a region of diffuse thrust faulting near the trench (Site C0007), and (3) the décollement zone sampled 2 km from the trench (Site 1174). At 25 MPa effective normal stress, at slip rates of 0.03–100 μm/s, and in the presence of brine as a pore fluid, we observe low friction (μ ≤ 0.46) for all of the materials we tested; however, the weakest samples (μ ≤ 0.30) are from the décollement zone. Material from the megasplay fault is significantly weaker than the surrounding wall rocks, a pattern not observed in the frontal thrust and décollement. All samples exhibit primarily velocity‐strengthening frictional behavior, suggesting that earthquakes should not nucleate at these depths. A consistent minimum in the friction rate parameter a‐b at sliding velocities of ∼1–3 μm/s (∼0.1–0.3 m/d) is observed at all three sites, suggesting that these shallow fault zones may be likely to host slow slip events.

Effect of clay content and mineralogy on frictional sliding behavior of simulated gouges: Binary and ternary mixtures of quartz, illite, and montmorillonite

We investigated the frictional sliding behavior of simulated quartz‐clay gouges under stress conditions relevant to seismogenic depths. Conventional triaxial compression tests were conducted at 40 MPa effective normal stress on saturated saw cut samples containing binary and ternary mixtures of quartz, montmorillonite, and illite. In all cases, frictional strengths of mixtures fall between the end‐members of pure quartz (strongest) and clay (weakest). The overall trend was a decrease in strength with increasing clay content. In the illite/quartz mixture the trend was nearly linear, while in the montmorillonite mixtures a sigmoidal trend with three strength regimes was noted. Microstructural observations were performed on the deformed samples to characterize the geometric attributes of shear localization within the gouge layers. Two micromechanical models were used to analyze the critical clay fractions for the two‐regime transitions on the basis of clay porosity and packing of the quartz grains. The transition from regime 1 (high strength) to 2 (intermediate strength) is associated with the shift from a stress‐supporting framework of quartz grains to a clay matrix embedded with disperse quartz grains, manifested by the development of P‐foliation and reduction in Riedel shear angle. The transition from regime 2 (intermediate strength) to 3 (low strength) is attributed to the development of shear localization in the clay matrix, occurring only when the neighboring layers of quartz grains are separated by a critical clay thickness. Our mixture data relating strength degradation to clay content agree well with strengths of natural shear zone materials obtained from scientific deep drilling projects.

An experimental investigation of the development and permeability of clay smears along faults in uncemented sediments

The generation of clay smears along faults in uncemented sediments has been studied through laboratory experiments in a newly developed high stress ring shear apparatus. The main objective is to investigate basic mechanisms involved in the deformation process of sediments during faulting and formation of clay smears. The experimental test program comprises ring shear tests on sand with embedded clay segments (sand–clay sequence) under constant effective normal stress. Visual inspection of the samples after testing, analyses of thin sections and permeability measurements across the shear zone are used to characterise geometrical continuity, thickness and sealing potential of the smear. Deformation processes such as grain reorientation, clay smear and cataclasis are identified from the tests. The complexity of the shear zone is observed to increase with the effective normal stress applied to the specimen and the number of clay segments used in the ring (multilayered sand–clay sequences). At low effective normal stress, in clay-rich sediments, clay smear is the most efficient mechanism for permeability reduction. The permeability across the smear decreases with ring rotation (or shear displacement) and effective normal stress. A maximum decrease of two orders of magnitude compared to the permeability of the surrounding sand is observed after 90° rotation under 10.5 MPa effective normal stress. Sand–sand juxtaposition shear is dominated by grain rolling causing only minor permeability reduction. At high effective normal stress, permeability measurements across clay smear and sand–sand juxtaposition yield similar values indicating that the permeability reduction is dominated by grain size reduction in the sand.

Frictional and hydrologic properties of a major splay fault system, Nankai subduction zone

We report on laboratory experiments examining the frictional and hydrologic properties of fault gouge and wall rock along a borehole transect that crosses a major out‐of‐sequence thrust splay fault within the Nankai accretionary complex. At 25 MPa effective normal stress, the fault zone material is frictionally weak (μ ≤ 0.44) and exhibits low permeability after shearing (k &lt; 5.5 × 10−20 m2). Fault zone samples are weaker and less permeable than the surrounding wall rocks, consistent with their slightly higher clay abundance. All samples exhibit velocity‐strengthening frictional behavior over most of the experimental conditions we explored, consistent with aseismic slip at shallow depths. The fault and wall rock both exhibit prominent minima in the friction rate parameter (a − b) for sliding velocities of 1–10 μm/s (∼0.1–1.0 m/day), comparable to rates for slow slip events. This suggests that the frictional properties of fault zone material play a central role in governing the mode of slip on subduction megathrusts.

Frictional sliding of gabbro gouge under hydrothermal conditions

We investigated the frictional sliding behaviour of gabbro gouge under hydrothermal conditions. Experiments were performed on 1-mm-thick gabbro gouge sandwiched between country rock pieces (with gouge inclined 35° to the sample axis) in a triaxial testing system with argon gas as the confining medium. In the first series, experiments were conducted under effective normal stresses of 200 MPa and 300 MPa respectively, with pore pressure of 10 MPa. For temperature over 400 °C, pore pressure of 30 MPa was also applied to implement supercritical water conditions. At temperatures up to 615 °C, slip rate steps ranging from 0.0488 μm/s to 1.22 μm/s were applied to obtain the rate dependence of friction. At 200 MPa effective normal stress and a pore pressure of 10 MPa, the steady state rate dependence a– b shows velocity-weakening behaviour for temperatures between ∼ 200 and ∼ 310 °C. The higher temperature limit for velocity-weakening behaviour to occur extends up to ∼ 510 °C under supercritical water conditions with a pore pressure of 30 MPa. For the limited sliding distance in our experiments, only velocity-strengthening behaviour occurred at 300 MPa effective normal stress. Considering the limited displacement (< 3.5 mm), velocity-weakening behaviour may not be excluded in the high effective normal stress case for temperature below ∼ 510 °C. The coefficient of friction shows an increasing trend with increasing temperature in the low temperature range. The cut-off temperatures for the increasing trend are ∼ 250 °C and ∼ 440 °C, respectively for the 200 MPa and 300 MPa effective normal stress cases. Above the cut-off temperatures, the coefficient of friction at 1.83 mm permanent displacement varies around an average of 0.73, which is identical to the average for the oven-dried case [He, C., Yao, W., Wang, Z., Zhou, Y., 2006. Strength and stability of frictional sliding of gabbro gouge at elevated temperatures. Tectonophysics 427, 217–229, doi:10.1016/j.tecto.2006.05.023]. Together with the small value of rate dependence ( a– b < 0.0073) for the whole temperature range, these results indicate the absence of fluid-assisted creep. With the result of our experiments as a constraint on strength of frictional sliding, comparison between converted strength for strike–slip faults and creep strength of gabbro-like rocks implies fracturing and faulting behaviours in the lower crust of a cool area (Zhangbei) in North China.

Comparative Deformation Behavior of Minerals in Serpentinized Ultramafic Rock: Application to the Slab-Mantle Interface in Subduction Zones

The layer-structure minerals serpentine, brucite, and talc are postulated to form in the mantle wedge above a subducting slab as a result of progressive hydration and silica metasomatism. Tectonic mixing at the slab-mantle interface generates serpentinite mélanges that contain blocks of high-pressure (HP) or ultrahigh-pressure (UHP) metamorphic rock derived from the subducting slab. Such serpentinite mélanges may provide a means of exhumation of HP/UHP metamorphic rocks, and may define the lower limit of locked regions on the subduction interface that fail in large earthquakes. We review recently obtained frictional strength data for brucite and talc over the temperature range 25-400°C at 100 MPa effective normal stress and compare them with new data for antigorite. These minerals respond to heating in different ways, causing their frictional strengths to diverge. Water-saturated antigorite strength increases toward the fixed dry value of μ ≈ 0.75-0.80 with heating: μ ≈ 0.50 at 25°C and μ > 0.60 at 400°C. The difference in μ between dry and watersaturated talc gouge also decreases with increasing temperature, but both the dry and watersaturated values of μ are lower at elevated temperatures. For dry talc, μ decreases from 0.35 to 0.25 between 25° and 300°C, whereas for water-saturated talc, μ is approximately 0.20 at 25°C and 0.10-0.15 at elevated temperatures. Weakening of the interlayer bond of talc with heating may be responsible for the overall reduction in its frictional strength. The strength of dry brucite also is fixed at μ = 0.45-0.50, but the water-saturated value of μ decreases from ≈0.30 at 25°C to 0.20-0.25 at 200°-400°C. The water-saturated brucite gouge has extensively recrystallized along the shear surfaces, and its weakening may be attributable to solution-transfer processes. Because the serpentine minerals become stronger at elevated temperatures, to achieve low frictional strength in a serpentinized mantle wedge or serpentine-rich mélange would require some other cause such as nearly lithostatic fluid pressures or the addition of lower-strength minerals. Increasing abundance of brucite and talc in serpentinite at constant physical conditions would progressively reduce its frictional strength. The concentration of talc along a metasomatic front at the edge of the mantle wedge or in reaction zones surrounding HP/UHP blocks in serpentinite mélange should tend to localize shear in this extremely weak material.

Hydraulic in situ investigations of an artificial fracture in the Falkenberg granite

The paper describes the results of hydraulic experiments on a large fracture produced by hydraulic fracturing in the Falkenberg granite. The friction pressure losses in the fracture were investigated for laminar and turbulent flow. Other experiments examined the pressure dependency of fracture transmissivity, fracture width and fracture storage coefficient. The following results were obtained: the friction losses in the fracture in the vicinity of the borehole increase non-linearly with the flowrate for flowrates higher than a critical value of about 0.51/sec. Injecting and venting results differed only slightly in the range of flowrate investigated (0.1–71/sec) but the difference seems to increase at higher flowrates. The observed relation between friction losses and flowrate is explained by assuming a turbulent region around the boreholes, expanding with an increasing flowrate. Fracture transmissivity and fracture width changed non-linearly with increasing and decreasing fluid pressure. Fracture transmissivity increased from a few D·m (Darcy·m) at hydrostatic pressure (corresponding to 1.9 MPa effective normal stress) to some 100 D·m at frac-extension pressure (corresponding to −0.3 M Pa effective normal stress). Fracture width ranged from 0.2–0.5 mm in the different boreholes at hydrostatic pressure to 1.0–2.0 mm at frac-extension pressure. The storage coefficient was S = 10−10 m/Pa at hydrostatic pressure and S = 10−9 m/Pa near frac-extension pressure.