Measurement Methodology Research Articles

Combined Impedance and Electron Paramagnetic Resonance Spectroscopy for Investigating the Dynamics of Li/Solid Li‐ion Conductor Interfaces

AbstractElectrochemical impedance spectroscopy (EIS) is a widely used tool for the electrochemical characterization of all‐solid‐state batteries (ASSBs) with Li‐metal anodes. However, an unambiguous interpretation of the observed impedance response often requires additional independent information on the actual interfacial phenomena obtained. The measurement methodology presented in this study allows to conduct electron paramagnetic resonance (EPR) spectroscopy and EIS concurrently. Therefore, the informative power of EIS experiments can be significantly improved via monitoring of structural changes of paramagnetic lithium at the electrochemical interface. As the solid‐electrolyte‐lithium interface is a critical part of all‐solid‐state batteries, this study employs a model oxide solid electrolyte in contact with lithium metal. During the polarization of the cell with thin evaporated lithium electrodes, the ratio between positive and negative peaks (a/b) of the EPR signal momentarily rises, which indicates an accumulation of lithium on one side of the electrolyte. The peak ratio a/b then drops abruptly, accompanied by current irregularities. Both are indicative of a diminishing contact area, and as a result, finer lithium morphologies form. Shortly after that, a contact loss is observed. The change of the EPR signal shape before cell breakdown can hence be associated with the worsening Li‐electrolyte contact, providing a tool for physical in‐situ cell diagnostics.

The Notable Role of Telomere Length Maintenance in Complex Diseases

Telomere length function serves as a critical biomarker for biological aging and overall health. Its maintenance is linked to cancer, neurodegenerative conditions, and reproductive health. This review mainly examines genetic variations and environmental influences on telomere dynamics, highlighting key regulatory genes and mechanisms. Advances in telomere measurement methodologies are also reviewed, underscoring the importance of precise telomere assessment for disease prevention and treatment. Telomerase activation offers potential for cellular lifespan extension and anti-aging effects, whereas its inhibition emerges as a promising therapeutic approach for cancer. Regulatory mechanisms of tumor suppressor genes on telomerase activity are analyzed, with a comprehensive overview of the current state and future potential of telomerase inhibitors. In addition, the association between telomeres and neurodegenerative diseases is discussed, detailing how telomere attrition heightens disease risk and outlining multiple pathways by which telomerase protects neurons from damage and apoptosis.

A comparison of measurement methodologies for the assessment of E-field level radiated by 5G NR base station

A comparison of measurement methodologies for the assessment of E-field level radiated by 5G NR base station

CONCEPTUALISING FACTORS AFFECTING PERFORMANCE IN ORGANISATIONAL ECOSYSTEM

Performance, as a significant construct, reflects the desire to fulfill specific needs and serves as a fundamental component in the workplace, and is regarded as a multifaceted concept that encompasses various aspects, including processes, behavioral engagements, and outcomes, specifically related to job behavior. Task performance requires specific behaviors and advanced cognitive abilities, categorised into technical-administrative and leadership responsibilities. Job performance prompts behavior associated with achievement that includes evaluative aspects. Research highlights the significance of autonomous and intrinsic motivation, indicating that individuals guided by inherent values and behaviors achieve optimal performance. The present conceptual study aims to identify and understand the principal factors affecting employee performance and to illustrate the connections among these components through a literature review on performance. Evaluating employee performance is the most complex and hardest soft skill, requiring the incorporation of additional factors. The predicted finding and discussion of this study allows us to draw inferences about the elements affecting projected performance within an inclusive organisational environment, such as the Police Department, and to provide suggestions for future research. This conceptual piece concludes a conceptual framework regarding staff development, measurement methodologies, and the factors influencing staff performance assessment. Understanding these characteristics will facilitate the assessment of staff performance and clarify the factors that enable an employee to succeed in meeting an organization's objectives.

Unmanned Aerial Vehicle Photogrammetry for Monitoring the Geometric Changes of Reclaimed Landfills

Monitoring reclaimed landfills is essential for ensuring their stability and monitoring the regularity of facility settlement. Insufficient recognition of the magnitude and directions of these changes can lead to serious damage to the body of the landfill (landslides, sinkholes) and, consequently, threaten the environment and the life and health of people near landfills. This study focuses on using UAV photogrammetry to monitor geometric changes in reclaimed landfills. This approach highlights the advantages of UAVs in expanding the monitoring and providing precise information critical for decision-making in the reclamation process. This study presents the result of annual photogrammetry measurements at the Słabomierz–Krzyżówka reclaimed landfill, located in the central part of Poland. The Multiscale Model to Model Cloud Comparison (M3C2) algorithm was used to determine deformation at the landfill. The results were simultaneously compared with the landfill’s reference (angular–linear) measurements. The mean vertical displacement error determined by the photogrammetric method was ±2.3 cm. The results showed that, with an appropriate measurement methodology, it is possible to decide on changes in geometry reliably. The collected 3D data also gives the possibility to improve the decision-making process related to repairing damage or determining the reclamation direction of the landfill, as well as preparing further development plans.

Modeling and Measurement of Tool Wear During Angular Positioning of a Round Cutting Insert of a Toroidal Milling Tool for Multi-Axis Milling

The aim of this study was to develop a concept for an angular positioning method for a round cutting insert in a torus cutter body dedicated to the multi-axis milling process under high-speed machining cutting conditions. The method concept is based on a developed wear model using a non-linear estimation method adopting a quasi-linear function. In addition, a tool life model was developed, taking into account the cutting blade work angle parameter, the laser marking method for the round cutting insert, and a wear measurement methodology. The developed tool wear model provides an accuracy of 90% in predicting the flank wear of the cutting blade. The developed procedure for angular positioning of the round cutting insert enables the entire cutting edge to be fully utilized, extending the total tool life. In addition, the measured largest defect values between the worn cutting edge and the nominal outline of the round cutting insert indicate the location of notching-type wear.

Methodology Used in Studies Aimed at Measuring Fetal Soft Tissues by 2D Ultrasound for the Screening of Large for Gestational Age Fetuses: A Systematic Review.

Management of suspected large for gestational age (LGA) fetuses remains unclear because ultrasound-estimated fetal weight (EFW) is not accurate. This was a systematic review of observational studies on fetal soft tissues measurements used alone or in combination to create a new EFW formula, to improve the screening for LGA fetuses. Studies were scored using a predefined set of independently agreed methodological criteria and an overall quality score was assigned for study design, statistical analysis, and reporting methods. There is a need to standardize methodologies for soft fetal tissue measurements. We propose a set of suggestions for this purpose.

New Vistas for the Relationship between Empathy and Political Ideology.

The study of ideological asymmetries in empathy has consistently yielded inconclusive findings. Yet, until recently these inconsistencies relied exclusively on self-reports, which are known to be prone to biases and inaccuracies when evaluating empathy levels. Very recently, we reported ideological asymmetries in cognitive-affective empathy while relying on neuroimaging for the first time to address this question. In the present investigation which sampled a large cohort of human individuals from two distant countries and neuroimaging sites, we re-examine this question, but this time from the perspective of empathy to physical pain. The results are unambiguous at the neural and behavioral levels and showcase no asymmetry. This finding raises a novel premise: the question of whether empathy is ideologically asymmetrical depends on the targeted component of empathy (e.g., physical pain vs cognitive-affective) and requires explicit but also unobtrusive techniques for the measure of empathy. Moreover, the findings shed new light on another line of research investigating ideological (a)symmetries in physiological responses to vicarious pain, disgust, and threat.Significance Statement In this study, we challenge the historically inconclusive findings on ideological asymmetries in empathy. By employing neuroimaging techniques, we demonstrated that ideological asymmetry in physical pain empathy is absent. This research underscores the importance of considering various facets of empathy, societal contexts, and unbiased measurement methodologies, such as neuroimaging techniques, in the assessment of empathic responses.

Fundamentals of Flexoelectricity, Materials and Emerging Opportunities Toward Strain-Driven Nanocatalysts.

Flexoelectricity, an intrinsic property observed in materials under nonuniform deformation, entails a coupling between polarization and strain gradients. Recent catalyst advancements have reignited interest in flexoelectricity, particularly at the nanoscale, where pronounced strain gradients promote robust flexoelectric effects. This paper comprehensively examines flexoelectricity, encompassing methodologies for precise measurement, elucidating its distinctions from related phenomena, and exploring its potential applications in augmenting catalytic properties. So far, the greatest potentials are based on lead strontium titanate (PST) and other metallic titanates such as titania (TiO2), strontium titanate (STO), barium strontium titanate (BST) sulfates (MoS2, ZnS)and halide perovskites (with archetype XPbI3). This review explores the promise of flexoelectric properties in addressing material and photocatalytic challenges, such as charge carrier recombination and ineffective surface charge separation. Additionally, it sheds light on the synergy with emerging paradigms like photo-flexo catalysis and synergistic flexo-piezo catalysis, specifically focusing on selective chemical transformations like green hydrogen production. Current limitations related to the usage of photoflexoelectricity for photocatalysis are mostly the stability of the used substance (susceptibility to photodegradation) or the voltage values, which represent the inferior potential for specific practical applications. This work underscores the indispensable role of flexoelectricity in catalysisand its capacity to steer future researchand technological advancement.

Measuring the outcomes of support provided to people after a suicide or other sudden bereavement: A scoping review

Systematic collection of outcome measures within suicide bereavement support is vital in building the sector’s evidence base. However, there is currently limited understanding around the appropriate and sensitive use of outcome measures. Following the scoping review methodology, a literature review was undertaken to map how programs and interventions that assist individuals bereaved by suicide or other sudden, traumatic deaths gather outcome measures. The search strategy identified 1145 papers, of which 49 met the inclusion criteria. The review identified many ways that outcomes are captured, with custom tools being commonplace. Among standardized tools, the Grief Experience Questionnaire (GEQ) and Beck Depression Inventory (BDI-II) emerged as frequently used. Most articles provided some form of justification for their chosen outcome measure methodology, often citing psychometric robustness over consideration of the impact on service users. The review underscores the need for careful consideration when selecting outcome measure tools or approaches in sudden death bereavement interventions.

Talent Measurement Model of Islamic Banking: Theoretical and Practice Perspectives

Talent measurement is a crucial component of talent management (TM). It involves the application of various measurement methodologies to assess the current and long-term potential, competencies, and contributions of employees in their roles. This study explores and integrates the theory of talent measurement from previous research with the practice of talent measurement model in Islamic banking. This study uses personal interview with the experts from selected Islamic banking in Indonesia, provides insights into how the traditional nine-box grid model is adapted within the context of Islamic banking, incorporating the principles of Maqāṣid al-Sharīʿah to ensure alignment with Islamic values. The findings suggest that integrating ethical dimensions into talent evaluation enhances fairness, employee engagement, and long-term organizational sustainability. Furthermore, the study highlights the importance of addressing talent risk factors and suggest strategies to improve talent retention in Islamic banking. This research offers valuable contribution to both theory and practice, proposing a more holistic and values-driven approach to talent management in the Islamic financial sector.

Changes in Acromiohumeral Distance With Clinician-Applied and Self-Applied Inferior Glenohumeral Joint Mobilizations Measured Using Ultrasound Imaging

OBJECTIVE: To measure the change in acromiohumeral distance during clinician-applied and self-applied manual shoulder joint mobilization. We hypothesized that the acromiohumeral distance would be significantly greater with clinician-applied manual joint mobilizations (MJM) than with self-applied joint mobilization. DESIGN: Within-subject, repeated measures design METHODS: Nineteen healthy adults (mean age: 22.9 ± 1.2 years) participated. A traction force of 15% body weight was applied during MJM and self-applied joint mobilization (SJM). Acromiohumeral distance was measured via ultrasound imaging at rest (baseline) and during the two test conditions (2 trials each) to quantify inferior accessory motion. The transducer was placed at the anterolateral border of the acromion and the subacromial space was clearly visualized for acromiohumeral distance measurements. RESULTS: The ICC for acromiohumeral distance measurements ranged from 0.876 to 0.963. Changes in acromiohumeral distance during MJM (3.90 ± 0.51mm) were significantly greater than SJM (1.68 ± 0.49mm, p<0.001). AHD changes between sexes: MJM (female: 3.16 ± 0.58mm, male: 5.15 ± 0.90mm, p=0.060); SJM (female: 0.88 ± 0.51 mm, male 3.05 ± 0.90mm, p=0.029). CONCLUSIONS: Our acromiohumeral distance measurement methodology had excellent test-retest reliability. There was significantly more inferior humeral accessory motion with MJM than SJM. The acromiohumeral distance was 132% greater during MJM and was unchanged or less than resting baseline measurements in almost a third of participants during SJM.

Maternal Parity Effect on Spine Posture Changes and Back Pain During Pregnancy

Background: Pregnancy can significantly alter posture and stability, thereby affecting spine curvatures. A positive relationship between the number of full-term pregnancies and the prevalence of low back pain (LBP) has been reported previously. This study aimed to analyze the impact of pregnancy on spine posture and LBP. Methods: Thirty pregnant females who were nulliparous (Group 1, n = 15) or had one or two pregnancies (Group 2, n = 15) were examined using the photogrammetric method in the first, second, and third trimesters of pregnancy. Further, a correlation analysis was conducted among the body mass index (BMI), pain intensity (VAS scale), and spine posture parameters. Results: The parous groups did not differ significantly in the parameters of the spinal posture. The thoracic angle decreased in trimester II compared to trimester I (157.77° vs. 160.55°, p = 0.004), which, according to the measurement methodology used, means that the thoracic kyphosis curvature increased. BMI was associated with the angle of trunk inclination in trimester I in Group 1 (r = 0.54, p = 0.04), as well as with the thoracic angle in trimesters II and III in Group 2 (r = 0.54–0.62, p < 0.05). A statistically significant correlation between pain intensity and spine posture parameters was more frequently observed in Group 2. Conclusions: Parity does not affect spine posture during pregnancy or pain intensity. The intensity of LBP was associated with spine posture changes during pregnancy, but the character of association differs between groups of parity. Alterations in spine posture should be monitored during pregnancy to prevent back pain.

Influence of parameter variation and interlayer temperature control in wall angle, curvature and measurement methodology of ER70S-6 parts obtained by WAAM

Wire and Arc Additive Manufacturing is characterized for the high deposition rates, enabling the manufacturing of big, complex parts, with smaller relative production cost. However, once the part receives high heat inputs, leading to geometry variation and deformations, it is important to properly measure the part characteristics. Therefore, this work contributes with a measurement methodology for inclined walls deposited by Wire and Arc Additive Manufacturing and its application on walls deposited with different parameters. The main parameter of influence was the use of interlayer temperature control, which increased the angle in 71.0%, and the curvature in 90.3%, lower part.

Методика фотограмметричного вимірювання люфтів та пружних податли-востей в шарнірних вузлах транспортних маніпуляторів та штанг косміч-них апаратів

The experimental study on multi-link structures and their components is of extreme relevance and importance to modern science and technology. These structures are widely used in various fields, including the aerospace and the automotive industry, robotics, and construction. The presence of numerous interconnected components makes their behavior complex and nonlinear. The accuracy and reliability of such systems depend on their dynamic characteristics, which are difficult to predict theoretically due to numerous factors, such as the material compliance, hinge backlashes, and intercomponent interaction. This study presents the authors’ verified methodology for experimentally determining backlashes and elastic compliances in hinges of transport manipulators and spacecraft booms, which is based on the photogrammetric method. The versatility of the method as applied to different types of mechanical experiments was analyzed. The obtained measurement accuracy and applicability to various structures under heterogeneous conditions make the methodology substantially universal. The methodology was tried out using a two-link fragment of a transport manipulator designed by the authors. A computational scheme was constructed to determine the effect of a hinge backlash. The scheme was used to obtain rotation trajectories of the manipulator section for different backlash values. It was found that photogrammetry can be used to determine the trajectories of each control marker on the hinge throughout its operational time. This allows one to refine computational schemes with calculated backlash values. The proposed methodology can easily be adapted to studying the elastic compliance of multi-link structure components in local stiffness reduction zones, such as flange connections and auxiliaries-to-link attachment points. The measurement methodology may be used in studying the dynamics of multi-link and ultralong structures by synchronizing several digital cameras. This enables remote monitoring of moving structures in space.

Effects of cardiac resynchronization therapy and physiologicaL pacing on left atrioventricular coupling index: the REPHYL-LACI study

Abstract Introduction Cardiac dyssynchrony and right ventricular pacing are associated with left atrial (LA) remodeling and atrioventricular uncoupling. Cardiac resynchronization therapy -CRT and conduction system pacing –CSP are important therapeutic options. Left atrioventricular coupling index (LACI) is a novel imaging parameter useful to describe the relationship between LA and left ventricle (LV). It could be measured as the ratio between LA end-diastolic volume (EDV) and the LV EDV or, alternatively, as the LA volume indexed for body surface area (LAVi) divided for a’ measured by tissue Doppler imaging (TDI) at medial mitral annulus level. Higher values indicate greater impairment of atrioventricular coupling. However, LACI has not been investigated in patients treated with CRT or CSP, and there is no comparison data about the two different measurement methodologies with echocardiography. Purpose To study the effects of CRT/CSP on LACI. Methods We retrospectively collected clinical, ECG and echocardiographic data of patients treated with standard CRT or CSP. Changes between baseline and follow-up (i.e. before and after CRT/CSP) were tested for significance. Baseline features were compared with these of a control group of patients without established major cardiovascular diseases. Results We enrolled fifty-six patients (median age at first echo 78[72.5-82]years; males 70%) and 56 controls (median age 77[72.5-83]years, p=0.974; males 57%, p= 0.170). Main clinical/instrumental data are shown in Table 1 and 2. In patients treated with CRT/CSP baseline LACIv (LAVid/LV EDV) was significantly lower than in controls (31[21-44]%vs34[29-48]%, p=0.040), despite higher LAVi and LV volumes in the first group (p<0.0001 for both). Conversely, LACId (LAVi/TDI-a’) was significantly higher in the CRT/CSP (4.48[2.81-8.28]vs2.89[2.36-3.67]mlxsecond/cm-1, p<0.0001). After a median follow-up of 515[282-1326]days, patients treated with CRT/CSP showed a significant increase of both LACIv (40[29-50]%, p=0.004) and LACId (4.95[3.77-9.89], p<0.0001). This worsening of atrioventricular coupling was accompanied by a trending LA dilatation with significant reduction of its reservoir function compared to baseline (expansion index 0.58[0.38-1.30]vs0.43[0.29-0.58], p=0.0002), despite a tendency toward stability or improvement of LV size and systolic/diastolic parameters. Conclusions In patients treated with CRT/CSP there is a worsening of LACI over time. We can speculate that the detrimental effects of artificial pacing might not be adequately counterbalanced by CRT/CSP, or that LV and LA pathology follow alternative trajectories with different responses to treatments. Moreover, the measurement of LACId should be probably avoided in patients with conduction disorders or paced. Further larger case-control studies are needed to clarify the usefulness of LACI as a valid parameter to assess atrioventricular coupling and its changes over time in patients treated with CRT/CSP.

Suitability of UR5 Robot for Robotic 3D Printing

The present paper describes the measurement of the drift of unidirectional pose accuracy, repeatability, and static compliance of a collaborative robot employing a measurement methodology that relies on the description of a virtual ISO cube placed in the robot’s workspace. The measurements aimed to investigate and assess the suitability of the UR5 six-axis collaborative robot for its application in robotic 3D printing. An experimental laboratory measurement workstation was constructed to perform the measurements, and control measurements were performed. The measurements involved describing the TCP point of the robot tool at five measurement points located in a virtual ISO cube during a minimum of 30 repeated measurement cycles. A camera and six linear incremental sensors with assessment units were used for the measurements. The measurements were performed in compliance with the regulations of STN ISO 9283 standard for this type of measurement. As a result of the measurements, the technical specifications of the drift and static compliance of the controlled robotic arm were verified, and the results were compared with the values specified by the manufacturer. Following the measurements and assessment of the results, it was possible to assess the suitability of the used UR5 robotic arm for its application in robotic 3D printing and to propose possible recommendations for the calibration of the robot and the process settings of the printing system for the production of objects using FDM technology.

Power-Law Modeling for Swift Viscoelastic Assessment in Biological Soft Tissues

In addressing the viscoelastic behavior of biological soft tissues, the precise and expeditious measurement methodologies hold paramount significance, given the intrinsic softness and heightened aqueous content of such substrates. We have introduced an expeditious modality for the characterization of viscoelasticity in biological soft tissues, hinged upon a power-law model. This method has been rigorously validated through ramp–hold tests conducted on mechanically stable hydrogels. Notably, during the Ramp phase, the viscoelastic parameters of the material can be readily extracted. Furthermore, we applied unconfined compression stress-relaxation/creep tests with three different ramp–strain rates, namely [Formula: see text], on both white and gray matter to enable rapid quantification. The results indicate that the predicted curves during the Hold phase exhibit notable consistency with experimental data. Moreover, under quasi-static loading conditions, an increase in strain rate significantly enhances the predictive adaptability. Nonetheless, it is crucial to be mindful of the sensitivity to initial stress conditions. This study offers a promising avenue for the expeditious characterization of soft tissue viscoelasticity. It underscores the feasibility of mechanical characterization metrics from a phenomenological model for the assessment of physiological variations and pathological mechanisms in tissue states.

Novel approach for in-line process monitoring during ultrasonic metal welding of dissimilar wire/terminal joints based on the thermoelectric effect

AbstractUltrasonic metal welding (USMW) is a manufacturing technique widely employed in the automotive and aerospace industries due to its efficiency in joining similar as well as dissimilar metals. Despite its prevalence, the lack of effective in-line process monitoring methods has resulted in high scrap rates, product recalls due to unrecognized scrap or financial losses due to pseudo-scrap, limiting its application in more sensitive industries. This paper presents a novel thermoelectric effect-based method for in-line process monitoring of USMW processes. This approach utilizes the thermoelectric properties, that manifest at the junctions of dissimilar metals during welding to accurately measure the temperature of the weld zone without the need of additional thermocouples, pyrometers or infrared cameras. An experimental setup was developed to validate the thermoelectric-based temperature measurement methodology. Key to this approach is the detection of thermoelectric voltage developed due to thermo diffusion when dissimilar materials are joined. The experiments showed a strong correlation between the thermoelectric voltage and the mechanical strength of the welds, suggesting that this parameter can effectively predict the quality of the weld. In the trials, a series of welded samples was created under controlled conditions to measure the generated thermoelectric voltage and correlate it with ultimate tensile strength tests. The data were analyzed using Spearman’s correlation coefficients to determine the correlation of the thermoelectric signals and joint strength. Results indicate that the thermoelectric voltage measurements correlate highly with the joint strength, with a Spearman’s correlation coefficient of over 0.94, thereby providing a promising predictive metric for assessing weld quality.

Direct Current to Digital Converter (DIDC): A Current Sensor.

This paper introduces a systematic approach to the design of Direct Current-to-Digital Converter (DIDC) specifically engineered to overcome the limitations of traditional current measurement methodologies in System-on-Chip (SoC) designs. The proposed DIDC addresses critical challenges such as high power consumption, large area requirements, and the need for intermediate analog signals. By incorporating a current mirror in a cascode topology and managing the current across multiple binary-sized branches with the Successive Approximation Register (SAR) logic, the design achieves precise current measurement. A simple comparator, coupled with an isolation circuit, ensures accurate and reliable sensing. Fabricated using the TSMC 180 nm process, the DIDC achieves 8-bit precision without the need for nonlinearity calibration, showcasing remarkable energy efficiency with an energy per conversion of 1.52 pJ, power consumption of 117 µW, and a compact area of 0.016 mm². This innovative approach not only reduces power consumption and area, but also provides a scalable and efficient solution for next-generation semiconductor technologies. The ability to conduct online measurements during both standard operations and in-field conditions significantly enhances the performance and reliability of SoCs, making this DIDC a promising advancement in the field.