Shear Measurements Research Articles

PH-controlled-ion-mobility of Laponite-phosphate dispersion for physical hydrogel with improved mechanical properties and sensitivity to CO2

Self-assembled physical nanocomposite hydrogels based on bio-based poly(itaconic acid) and Laponite® nanoclays were prepared and tested as possible CO2 sensors in smart food packaging. The structure and mechanical properties of the fabricated hydrogels were controlled by changing the initial pH of the aqueous Laponite® dispersions stabilised by tetrasodium pyrophosphate. The dispersions were studied by SAXS and analysed using circular disc and fractal model to determine clay agglomeration tendency. Sodium and pyrophosphate ions mobility was investigated by 23Na and 31P 1D as well as spin-spin relaxation times T2 NMR measurements. The rheological behaviour of the produced hydrogels was studied by oscillatory shear measurements. It was found that decreasing the pH of the Laponite® nanodispersions up to 8 increases the strength of the physical interactions between the nanoclays, dispersant, and polyelectrolyte chains, which enables production of dimensionally stable and mechanically robust hydrogels. Their potential application as the CO2-sensitive matrix for construction of environmentally friendly colorimetric sensors was demonstrated showing the CO2 sorption capacity of 0.07 mmol CO2/g. A prototype device of hydrogel sensor was built and tested in a food packaging application to monitor the plum fruit respiration processes.

Euclid preparation. LIII. LensMC, weak lensing cosmic shear measurement with forward modelling and Markov Chain Monte Carlo sampling

is a weak lensing shear measurement method developed for and Stage-IV surveys. It is based on forward modelling in order to deal with convolution by a point spread function (PSF) with comparable size to many galaxies, sampling the posterior distribution of galaxy parameters via Markov chain Monte Carlo, and marginalisation over nuisance parameters for each of the 1.5 billion galaxies observed by We quantified the scientific performance through high-fidelity images based on the Flagship simulations and emulation of the VIS images, realistic clustering with a mean surface number density of $ arcmin^ for galaxies, and $ arcmin^ for stars, and a diffraction-limited chromatic PSF with a full width at half maximum of $ $ and spatial variation across the field of view. measured objects with a density of $ arcmin^ in $4500 deg^2 $. The total shear bias was broken down into measurement (our main focus here) and selection effects (which will be addressed in future work). We found measurement multiplicative and additive biases of $m_1=(-3.6 $, $m_2=(-4.3 $, $c_1=(-1.78 $, and $c_2=(0.09 $; a large detection bias with a multiplicative component of $1.2 $ and an additive component of $-3 $; and a measurement PSF leakage of $ $ and $ $. When model bias is suppressed, the obtained measurement biases are close to requirement and largely dominated by undetected faint galaxies ($-5 $). Although significant, model bias will be straightforward to calibrate given its weak sensitivity on galaxy morphology parameters. is publicly available at

Two-species model for nonlinear flow of wormlike micelle solutions. Part II: Experiment

Applications often expose wormlike micelle solutions to a very wide range of shear and temperature conditions. The two-species model presented in Part I [Salipante et al., J. Rheol. 68 (2024)] describes the nonlinear rheology over a wide range of shear rates. Here, we compare the model predictions to measurements using a combination of microcapillary and rotational rheology to measure the viscosity of surfactant solutions across seven decades of shear rate and five decades of viscosity. The effect of temperature is studied between 20 and 60 °C for different surfactant concentrations. Model parameters are determined from both small-amplitude shear measurements and fitting to the nonlinear data. Under shear stress, the model predicts due to hindered combination kinetics that the average micelle length decreases from several micrometers to a few hundred nanometers. At sufficiently high stress, the micelle shear rheology exhibits a transition from entangled wormlike behavior to a dilute rod rheology in agreement with the model. Transient stress-growth measurements exhibit a large overshoot, which is rather well predicted by the model with hindered combination rate. Microcapillary flow birefringence also is adequately predicted by the model, confirming the accuracy of its predicted micelle lengths and exhibiting a marked change in stress-optic response at the transition between entangled polymers and dilute rods. The relaxation of retardance after flow cessation follows model predictions that include micelle-micelle interactions, which are sensitive to the rotational diffusivity and length. These methods can be applied broadly to explore relationships between composition and performance.

Development of a high-precision long trace profiler utilizing shear measurements.

Compensating for the pitch error in the scanning movement is a fundamental issue when conducting large-scale surface shape measurements with deflectometric profilers. This paper presents a new long trace profiler employing a shearing measurement technique. In this setup, the optical head and the mirror under test are mounted on two independent parallel movable air-bearing carriages to enable shearing and scanning movements separately. The distance between the optical head and the tested mirror remains fixed, effectively minimizing the influence of system errors resulting from imperfections in optical devices. Simulation studies show that the double shear measurement method with a low-spatial-frequency filtering process can effectively mitigate high-frequency angular measurement errors introduced by the instability of the air-bearing stage. Experimental tests conducted on flat mirrors demonstrated a precision of less than 50 nrad rms, thereby confirming the robustness of the system.

Sparse regression for discovery of constitutive models from oscillatory shear measurements

We propose sparse regression as an alternative to neural networks for the discovery of parsimonious constitutive models (CMs) from oscillatory shear experiments. Symmetry and frame invariance are strictly imposed by using tensor basis functions to isolate and describe unknown nonlinear terms in the CMs. We generate synthetic experimental data using the Giesekus and Phan-Thien Tanner CMs and consider two different scenarios. In the complete information scenario, we assume that the shear stress, along with the first and second normal stress differences, is measured. This leads to a sparse linear regression problem that can be solved efficiently using l1 regularization. In the partial information scenario, we assume that only shear stress data are available. This leads to a more challenging sparse nonlinear regression problem, for which we propose a greedy two-stage algorithm. In both scenarios, the proposed methods fit and interpolate the training data remarkably well. Predictions of the inferred CMs extrapolate satisfactorily beyond the range of training data for oscillatory shear. They also extrapolate reasonably well to flow conditions like startup of steady and uniaxial extension that are not used in the identification of CMs. We discuss ramifications for experimental design, potential algorithmic improvements, and implications of the non-uniqueness of CMs inferred from partial information.

On the Relation between the Viscoelastic Properties of Granular Hydrogels and Their Performance as Support Materials in Embedded Bioprinting.

Granular hydrogels, formed by jamming microgels suspension, are promising materials for three-dimensional bioprinting applications. Despite their extensive use as support materials for embedded bioprinting, the influence of the particle's physical properties on the macroscale viscoelasticity on one hand and on the printing performance on the other hand remains unclear. Herein, we investigate the linear and nonlinear rheology of κ-carrageenan granular hydrogel through small- and large-amplitude oscillatory shear measurements. We tuned the granular hydrogel's properties by changing the stiffness (soft, medium, stiff) and the packing density of the individual microgels. Characterizations in the linear viscoelasticity regime revealed that the storage modulus of granular hydrogels is not a simple function of microgel stiffness and depends on the microgel packing density. At larger strains, increasing the microgel stiffness reduced the energy dissipation of the granular beds and increased the solid-fluid transition point. To understand how the different rheological properties of granular support materials influence embedded bioprinting, we examined the printing fidelity and cellular filament shrinkage within the granular beds. We found that microgels with low packing density diminished the printing quality, while stiff microgels promoted filament roughness. In addition, we found that highly packed stiff microgels significantly reduced the postprinting contraction of cellular filaments. Overall, this work provides a comprehensive knowledge of the rheology of granular hydrogels that can be used to rationally design support beds for bioprinting applications with specific characteristics.

Correlations between adhesion and molecular interactions at buried interfaces of model polymer systems and in commercial multilayer barrier films.

Sum frequency generation vibrational spectroscopy (SFG) was applied to characterize the interfacial adhesion chemistry at several buried polymer interfaces in both model systems and blown multilayer films. Anhydride/acid modified polyolefins are used as tie layers to bond dissimilar polymers in multilayer barrier structures. In these films, the interfacial reactions between the barrier polymers, such as ethylene vinyl alcohol (EVOH) or nylon, and the grafted anhydrides/acids provide covalent linkages that enhance adhesion. However, the bonding strengths vary for different polymer-tie layer combinations. Here, using SFG, we aim to provide a systematic study on four common polymer-tie interfaces, including EVOH/polypropylene-tie, EVOH/polyethylene-tie, nylon/polypropylene-tie, and nylon/polyethylene-tie, to understand how the adhesion chemistry varies and its impact on the measured adhesion. Our SFG studies suggest that adhesion enhancement is driven by a combination of reaction kinetics and the interfacial enrichment of the anhydride/acid, resulting in stronger adhesion in the case of nylon. This observation matches well with the higher adhesion observed in the nylon/tie systems in both lap shear and peel test measurements. In addition, in the polypropylene-tie systems, grafted oligomers due to chain scission may migrate to the interface, affecting the adhesion. These by-products can react or interfere with the barrier-tie chemistry, resulting in reduced adhesion strength in the polypropylene-tie system.

Splitting intensity tomography to image depth-dependent seismic anisotropy patterns beneath the Italian Peninsula and surrounding regions

The region between central Europe and the centre of the Mediterranean is characterised by complex tectonics and kinematics. Here, the interaction between thickened crust, subducting lithosphere and surrounding asthenosphere produces strong and pervasive anisotropy in the upper mantle. Shear wave splitting measurements, the most adopted method to image seismic anisotropy so far, when interpreted in a ray-based framework result in little or no depth resolution, hampering a correct image of the anisotropy distribution with depth. In this study, we aim to better constrain the depth-dependent seismic anisotropy beneath Italy and surrounding regions, by isolating for the first time the source region of anisotropy at different depths. To do that, we perform an anisotropy tomography, adopting the splitting intensity inversion method. It is entirely based on the finite-frequency effect in the splitting of SKS waves. We first computed the splitting intensity using SKS waves recorded at all available permanent and temporary stations over the region, obtaining a huge dataset of measurements used as an input for the tomographic inversion. The large-scale 3D model of seismic anisotropy obtained with the inversion shows a clear change of anisotropy properties in terms of fast polarisation direction and intensity for different depths, thus improving the characterization of the main sources of anisotropy in the mantle as a function of depth. Shallower layers (70–100 km depth) are characterised by a complex and variable oriented pattern of anisotropy fast direction and intensity, which becomes progressively more organised with depth (100–300 km). This pattern suggests a strong control exerted by the geometry and motion of the different slab segments and the large-scale asthenospheric flow generated by subduction and roll-back processes. The strength of anisotropy increases with depth, with high values affecting the bulge of the Alps and Apennines chains and the southern Tyrrhenian subduction system. On the contrary, weaker anisotropy characterises the transition zone from the Apennines to Alpine domains beneath the Po plain, and both the Adriatic and European domains.

Fossil Groups analysis using weak gravitational lensing

Abstract The overall objective of this study is to investigate claims found in the literature that fossil groups, characterized by a large magnitude gap between their two brightest galaxies, are darker, i.e. exhibit higher mass-to-light ratios (M/L), compared to regular groups. Specifically, we aim to measure the mass of these systems using the weak gravitational lensing technique. To achieve this, we obtained deep images of four fossil systems with the CFHT telescope in the r and g bands. Through a careful process of weak gravitational shear measurement, including corrections for the point spread function (PSF) and contamination from group and foreground galaxies, we fit NFW models and obtained mass measurements as a result. Similarly, we quantified the light distribution produced by these groups, taking into account relevant data gaps in the images due to the presence of bright stars, as well as contamination from foreground and background galaxies. We obtained masses and M/L ratios that are consistent with previous results where mass was estimated from galaxy dynamics. Indeed, the four fossil systems studied here exhibit high M/L ratios compared to the general population of systems. Drawing more generalizable conclusions from a sample of only four systems is challenging. However, the procedure outlined in this study can be applied to large image surveys, allowing for a revisiting of this question with significantly reduced statistical uncertainties. This will enable a more homogeneous comparison between fossil groups and clusters and the overall population.

Wormlike Micellar Glycerol Solutions Formed from a Double-Tailed Surfactant with Two Quaternary Ammonium Head Groups.

Herein, a quaternary ammonium surfactant with dual heads and tails, N1,N1,N1,N3,N3-pentamethyl-N3-(3-(2-tetradecylhexadecanamido)propyl)propane-1,3-diaminium dibromide, abbreviated as Di-C14-N2, was synthesized. For the first time, clear observation of aggregate structures formed by surfactants in pure glycerol systems was achieved using cryogenic transmission electron microscopy (cryo-TEM). The system's rheological properties were analyzed using both steady-state shear and oscillatory rheological measurements. The lubricating efficiency of the Di-C14-N2 glycerol solution was assessed for its tribological properties using a tribological wear tester, white light interferometer, and scanning electron microscope. In glycerol, Di-C14-N2 formed long wormlike micelles, which resulted in a glycerol solution with the zero-shear viscosity of 1013 Pa·s at 90 mM, which is the most viscous glycerol system up to now. The system displayed distinct rheological properties from the aqueous system, as evidenced by two intersections in the loss and storage moduli. The formed wormlike micelles in glycerol lead to a significant alteration in the viscoelasticity of the system, thus endowing the Di-C14-N2 glycerol solution with potential as an eco-friendly lubricant. The friction coefficient of the system was found to be 23% lower and the wear rate was 83% lower than that of pure glycerol after the addition of Di-C14-N2. This demonstrates that the addition of Di-C14-N2 greatly improves the frictional properties of pure glycerol. This study offers the possibility of directly observing the aggregate structures formed by surfactants in pure glycerol systems. It contributes to the exploration of the self-assembly behavior of surfactants in nonaqueous polar media, thereby aiding in a deeper understanding of the correlation between molecular structure, mesoscale structure, and macroscopic properties.

Detailed structural analyses and viscoelastic properties of nano-fibrillated bacterial celluloses

Nano-fibrillated bacterial cellulose (NFBC) can be prepared by cultivating a cellulose-producing bacterium in a medium containing a dispersant under agitating and aerobic conditions. Although NFBCs have various applications, their detailed structure and physical properties have not been clarified. Therefore, in this study, we performed detailed structural and physical property analyses of NFBCs to advance their potential applications. Atomic force microscopy and image analysis showed that the average fiber length of NFBCs was approximately 17 µm and fiber widths were 10–15 nm; the aspect ratios of NFBCs were > 1000, which are >10-fold higher than that of 2,2,6,6-tetramethylpioeridine-1-oxyl-oxidized cellulose nanofiber. Shear viscosity measurements showed that the NFBCs exhibited shear-thinning flow behavior even at low concentrations (0.01 wt%). Frequency sweep measurements showed that the storage modulus values were greater than the loss modulus values in the measured frequency range, indicating that the NFBCs were in a stable gel state. Thus, the NFBCs exhibited significantly longer fiber lengths, larger aspect ratios, and excellent viscoelastic properties based on these unique structural features. Our findings will help develop novel applications utilizing the ultrahigh aspect ratio unique to NFBC and its viscoelastic properties.

Shear wave measurement in slow formations for eccentric monopole acoustic logging while drilling

Abstract The use of a logging-while-drilling (LWD) monopole tool to directly measure shear (S) wave velocity in slow formations has been proven feasible under certain conditions. However, S-wave signals received in the borehole are fairly weak, which limits the application range of this measurement method. To find ways to enhance shear waves, we first explore factors sensitive to the S-wave excitation. Simulation results indicate that four parameters including the receiver-source distance, the radial distance from receiver to borehole wall, the formation S-wave velocity and source frequency, primarily influence the S-wave excitation. Shear waves can be enhanced by judiciously optimizing these parameters during tool design. We also investigate borehole wavefields with an eccentric LWD tool in both commonly slow and ultra-slow formations. Results reveal that tool eccentricity can amplify shear waves and improve its measurement accuracy, provided that waveforms received in the direction of tool movement are used. We successfully extracted the S-wave velocity of an ultra-slow formation under conditions of large eccentricity, while similar actions originally failed with a centralized instrument.

A Hierarchical Point-spread Function Reconstruction Method

Reconstruction of the point-spread function (PSF) plays an important role in many areas of astronomy, including photometry, astrometry, galaxy morphology, and shear measurement. The atmospheric and instrumental effects are the two main contributors to the PSF, both of which may exhibit complex spatial features. Current PSF reconstruction schemes typically rely on individual exposures, and their ability to reproduce the complicated features of the PSF distribution is therefore limited by the number of stars. Interestingly, in conventional methods, after stacking the model residuals of the PSF ellipticities and (relative) sizes from a large number of exposures, one can often observe some stable and nontrivial spatial patterns on the entire focal plane, which could be quite detrimental to, e.g., weak-lensing measurements. These PSF residual patterns are caused by instrumental effects, as they consistently appear in different exposures. Taking this as an advantage, we propose a multilayer PSF reconstruction method to remove such PSF residuals, the second and third layers of which make use of all available exposures together. We test our method on the i-band data of the second release of the Hyper Suprime-Cam. Our method successfully eliminates most of the PSF residuals. Using the Fourier_Quad shear measurement method, we further test the performance of the resulting PSF fields on shear recovery using the field distortion effect. The PSF residuals have strong correlations with the shear residuals, and our new multilayer PSF reconstruction method can remove most of such systematic errors related to the PSF, leading to much smaller shear biases.

High internal phase Pickering emulsion solely stabilized by low-content chitosan: Insight into relations between network microstructures and rheological properties

Nano-sized and well-dispersed chitosan particles (CSPs) are prepared by adjusting pH towards pKa of chitosan (CS) aqueous solutions. The prepared CSPs are able to stabilize high internal phase Pickering emulsions (HIPPEs) with low CSP contents, at minimum of 0.2 wt% CSP stabilizing a maximum of 85 % oil phase fraction in a near-neutral environment. It is clarified by microscopy, small amplitude oscillatory shear (SAOS) and large amplitude oscillatory shear (LAOS) measurements that CSPs act as Pickering particle emulsifiers to form a network immobilizing oil droplets in HIPPEs. Using power-law analysis on SAOS results, the solid-like but frequency-dependent rheological response is attributed to the physical connection among CSPs, while the overshoot of the loss modulus in LAOS test is assigned to the featured resistance of networks to the applied large deformation. The oil phase fraction, CSP concentration, temperature and ionic strength are found to be key factors for the rheological behavior and emulsion stability. This work is expected to guide the design and processing of HIPPE stabilized solely by polysaccharides.

Reconstructing the matter power spectrum with future cosmic shear surveys

ABSTRACT Analyses of cosmic shear typically condense weak lensing information over a range of scales to a single cosmological parameter, $S_8$. This paper presents a method to extract more information from Stage IV cosmic shear measurements by directly reconstructing the matter power spectrum from linear to non-linear scales. We demonstrate that cosmic shear surveys will be sensitive to the shape of the matter power spectrum on non-linear scales. We show that it should be possible to distinguish between different models of baryonic feedback and we investigate the impact of intrinsic alignments and observational systematics on forecasted constraints. In addition to providing important information on galaxy formation, power spectrum reconstruction should provide a definitive answer to the question of whether weak lensing measurements of $S_8$ on linear scales are consistent with the Planck Lambda cold dark matter cosmology. In addition, power spectrum reconstruction may lead to new discoveries on the composition of the dark sector.

Breaking the mass-sheet degeneracy in strong lensing mass modelling with weak lensing observations

ABSTRACT The Hubble constant ($H_0$), a crucial parameter in cosmology, quantifies the expansion rate of the universe so its precise measurement is important to understand the fundamental dynamics of our evolving universe. One of the major limitations of measuring $H_0$ using time-delay cosmography is the presence of the mass-sheet degeneracy (MSD) in the lens mass modelling. We propose and quantitatively assess the use of galaxy–galaxy shear measurements to break the MSD in the strong lensing mass modelling. We use stacked galaxy–galaxy lensing profiles and corresponding covariance matrices from Huang et al. to constrain the MSD in lens mass modelling with a highly flexible mass profile. Our analyses show that if ideally all galaxy–galaxy lensing measurements from the Hyper Suprime-Cam survey can be used to constrain the MSD, we can achieve $\sim 10~{{\ \rm per\ cent}}$ precision on the MSD constraint. We forecast that galaxy–galaxy lensing measurements from Legacy Survey of Space and Time (LSST)-like surveys can in general constrain the MSD with $\sim 1\,\mathrm{ per\,cent}-3~{{\ \rm per\ cent}}$ precision. Furthermore, if we push weak lensing measurements to a lower angular scale of $\sim 0.04\,\rm Mpc$, a survey like LSST can provide $\sim 1~{{\ \rm per\ cent}}$ precision on the MSD constraint, enabling a measurement of $H_0$ at the 1 per cent level. We demonstrate that galaxy–galaxy weak lensing can robustly constrain the MSD independent of stellar kinematics of the deflector, with wide-field survey data alone.

Physicochemical Attributes and Dynamic-Mechanical Properties of a Traditional Himalayan Cheese – Kalari

ABSTRACT Kalari is a traditionally made Himalayan cheese. It is popular in the hilly belts of Jammu and Kashmir, India, and is also known as the “Mozzarella of Kashmir.” It is prepared from raw milk by natural acidification followed by heat coagulation. The present work aims to evaluate the physicochemical and rheological characteristics of Kalari and to gain insight into its composition and functional properties. Rheological characterization based on small amplitude oscillatory shear (SAOS) measurements reveals the cheese to be a viscoelastic material, with the elastic nature dominating viscous behavior at all test conditions. Temperature sweep and Arrhenius plot also enabled to identify rheological response of Kalari at elevated temperatures, which can further elucidate its functionality. Lower values of activation energy (39.57 KJ mol−1) and phase angle (28°) reiterate that the cheese does not flow extensively but undergoes softening and slight melting on exposure to high temperatures. Physicochemical characterization revealed the cheese to possess more protein (33.8% − 42.6%) and moisture (42.9% − 48.1%) than fat (7.5% − 11.9%).

Experimental study of permeability characteristics of fracture-hosted hydrate-bearing clay sediments under triaxial shear

Reservoir permeability during the hydrate exploitation process is closely related to gas production. Fractures influence hydrate distribution and the evolution of reservoir permeability. Moreover, shear during exploitation can disturb the structure of sediments. Therefore, studying permeability and its evolution under shear in fracture-hosted hydrate-bearing sediments is significant for hydrate exploitation projects in the South China Sea. In this paper, standard sand and montmorillonite were mixed, and three different fracture angles were created to simulate sediment fracture. Consolidation, shear, and permeability measurements were employed to investigate mechanical and permeability properties. The results showed that the permeability of fracture-hosted hydrate-bearing sediments decreased and then increased with increasing hydrate saturation, both before and after consolidation. The compressibility of sediments played an important role in the permeability damage rate caused by consolidation and normalized permeability at the breaking point. Furthermore, fractures caused an undesired double peak and the disappearance of the permeability breaking point hysteresis relative to the stress breaking point. However, these effects were mitigated by increasing saturation. Lastly, the analysis of permeability sensitivity coefficients revealed that permeability was most sensitive to strain in the early shear stages. This study can guide methane hydrate exploitation in the South China Sea.

Dark scattering: accelerated constraints from KiDS-1000 with ReACT and CosmoPower

ABSTRACT We present constraints on the dark scattering model through cosmic shear measurements from the Kilo Degree Survey (KiDS-1000), using an accelerated pipeline with novel emulators produced with CosmoPower. Our main emulator, for the dark scattering non-linear matter power spectrum, is trained on predictions from the halo model reaction framework, previously validated against simulations. Additionally, we include the effects of baryonic feedback from HMCode2016, whose contribution is also emulated. We analyse the complete set of statistics of KiDS-1000, namely band powers, COSEBIs, and correlation functions, for dark scattering in two distinct cases. In the first case, taking into account only KiDS cosmic shear data, we constrain the amplitude of the dark energy–dark matter interaction to be $\vert A_{\rm ds} \vert \lesssim 20$$\rm b\,GeV^{-1}$ at 68 per cent C.L. Furthermore, we add information from the cosmic microwave background (CMB) from Planck, along with baryon acoustic oscillations (BAO) from 6dFGS, SDSS, and BOSS, approximating a combined weak lensing+CMB+BAO analysis. From this combination, we constrain $A_{\rm ds} = 10.6^{+4.5}_{-7.3}$$\rm b\,GeV^{-1}$ at 68 per cent C.L. We confirm that with this estimated value of $A_{\rm ds}$ the interacting model considered in this work offers a promising alternative to solve the $S_8$ tension.

Static- vs Impact-Ice-Shear Adhesion on Metals and a Self-Lubricating Icephobic Coating

To characterize the performance of icephobic coatings for aerospace applications, various shear-based techniques have been used. Generally, these techniques are conducted in conjunction with comparison tests on metals. In this study, a review of the various approaches for measuring adhesion for static and impact ice for metal and icephobic surfaces was done. This review indicated that many details of the test conditions either varied significantly among studies or were omitted. To address this uncertainty, new measurements were taken to examine in-situ ice-shear-adhesion strength for impact and static ice with various surfaces, using a consistent icing-research-tunnel facility with well-characterized and detailed test conditions. The results for the two different metals tested revealed a significantly higher ice adhesion for static ice compared to that for impact ice. However, the tested self-lubricated icephobic coating significantly reduced ice adhesion strength for both impact and static ice and this performance was retained after multiple icing tests. Based on the methodology review and the current experimental study results, it is recommended that future ice adhesion studies fully characterize the following: the apparatuses for shear measurement, which include protocols and procedures used; the surface chemistry and roughness; the thermal conditions of the air, water, and surface; and for impact ice, the droplet conditions such as velocity and size in order to ensure repeatability within a study and comparison across studies.