Lycopene Retention Research Articles

Deciphering the role of fruit maturity, calcium and freezing on the nutritional and textural attributes of crisps from red guava

SummaryGuava (Psidiumguajava L.), being highly nutritious possesses commercial importance in the tropical and subtropical region of the world. The climacteric guava, however, records highest postharvest loss and needs to be processed for higher shelf life and utility. This study entails evaluation of fruit maturity stage and prior freezing for development of calcium enriched guava crisps through atmospheric frying. The sliced fruits (of three maturity stages) were subjected to vacuum impregnation to infuse maltodextrin, salt, ascorbic acid and calcium lactate. Fracturability and crispness was significantly affected by fruit maturity, freezing pre‐treatment and calcium impregnation. Freezing pre‐treatment enhanced the texture, decreased toughness and gave superior crisps with crunchy mouthfeel. While browning increased due to freezing pre‐treatment, calcium impregnation led to decreased browning. More than 15‐fold increase in the calcium content of crisps was realised upon 1% calcium lactate impregnation. The average ascorbic acid and lycopene retention in the crisps was 36.18 and 37.58%, respectively. Mature guava showed highest lycopene retention (43.07%) in crisps. Based on MANOVA analysis, all the main effects, two factor interaction and three factor interaction were statistically significant at 1% level. The first three PCs could explain 73.64% variation in data. The highest ascorbic acid retention, crispiness and sensory scores were recorded for crisps from ripe stage of guava fruits given freezing and calcium infusion pre‐treatments. Thus, ripe guava fruits could be converted to shelf stable and attractive crisps, which would provide essential nutrients and potential health benefits, ensuring off‐season availability of perishable guava in the form of crisps.

Evaluating the impact of pulsed light treatment on microbial and enzyme inactivation and quality attributes in fresh‐cut watermelon

AbstractThis study investigated the impact of pulsed light (PL) applied at a fluence of 4–12 J cm−2 (complying with U.S. Food and Drug Administration standards) on fresh‐cut watermelon, focusing on its efficacy in inactivating various food‐borne pathogenic gram‐positive (Escherichia coli and Staphylococcus aureus) and gram‐negative (Listeria monocytogenes and Salmonella) bacteria. The inactivation data were used to fit the log‐linear and Weibull kinetic models. Additionally, the impact of PL on physicochemical properties, lycopene content, total phenolic content, antioxidant activity, and pectin methylesterase (PME) residual activity (RA) was studied. The results demonstrated that the inactivation rate increases with the increase in fluence. Salmonella was most sensitive to PL, resulting in a reduction of 2.55 ± 0.08 log CFU g−1 and a higher kmax, whereas S. aureus was most resistant, with a reduction of 1.87 ± 0.24 log CFU g−1 and a lower kmax. The Weibull model was the best to predict the inactivation kinetics based on standard statistics and information theory criteria. For all assayed food‐borne pathogens, the inactivation curve showed non‐linearity with upward concavity except for L. monocytogenes, which followed a concave downward curve (β >1). Results showed that PL was effective in the retention of color, firmness, pH levels, total soluble solids, and titratable acidity, and also had a positive effect on enhancing the levels of essential components such as lycopene, total phenolic compounds, and antioxidant activity. Additionally, the PME RA significantly decreased with an increase in fluence due to structural modification. Therefore, PL can be explored to enhance fresh‐cut watermelon's safety and quality attributes.Practical ApplicationsThe implementation of this research holds significant potential for practical benefits in the fresh‐cut fruit industry. The findings could revolutionize processing practices, ensuring enhanced microbial safety, enzyme inactivation, and an extended shelf‐life of fresh‐cut watermelon. The study strongly contributes to preserving the desirable texture, color, and overall quality of the product, enhancing the retention of lycopene and other valuable antioxidants by standardizing the pulsed light treatment parameters while adhering to U.S. Food and Drug Administration standards for food application. Moreover, this research will scientifically contribute to addressing the critical challenges of foodborne outbreaks in the fresh‐cut fruit sector while providing consumers with a healthy, convenient food choice.

Esterified porous starch from guinea grass seed for enhanced facile microencapsulation of bioactive materials

The present study focuses on the utilization of non-conventional starch (NS) derived from guinea grass seed to produce porous starch (PS) and octenyl succinic anhydride-modified PS (OSAPS). The study also introduces a novel approach to produce PS, aiming to overcome the high cost associated with glucoamylase. The formation of porous granules was successfully achieved through the combination of alpha-amylase and ultrasonication, as confirmed by electron micrographs and analysis of pore size and specific surface area. The results demonstrate that OSAPS exhibits superior emulsion stability, well-defined pore structures, and desirable amphiphilic characteristics. All three starches were loaded with lycopene, flaxseed oil, and a combination of both to prepare microcapsules. The presence of flaxseed oil within the starch matrix was confirmed through micrographs and functional group analysis. Notably, OSAPS exhibited the highest encapsulation efficiency at 74.80 %, along with a lycopene retention rate of up to 27.32 mg/100 g. Moreover, OSAPS showcased favorable antioxidant activity (89.29 %), phenolic content (0.45 mg GAE/g), and flavonoid content (97.61 mg QE/100 g). These findings underscore the remarkable potential of OSAPS as a delivery system for bioactive compounds, particularly for the co-encapsulation of oils and pigments.

Lycopene in hydrophobic deep eutectic solvent with natural catalysts: A promising strategy to simultaneously promote lycopene Z-isomerization and extraction.

Lycopene Z-isomerization and degradation in a series of hydrophobic natural deep eutectic solvents (HNDES) was firstly studied. The highest lycopene retention (about 84.6%) was found in HNDES composed of thymol and menthol (TM), and fatty acid-basedHNDES promoted lycopene Z-isomerization (about 70% for total Z-isomers) and degradation. The addition of allyl isothiocyanate (AITC), diallyl disulfide (DADS) and capric acid into TM promoted Z-isomerization of lycopene (80% for total Z-isomers), especially 5Z-isomer (>30%), while lycopene remaining rate in TM/-capric acid was below 20%. During lycopene extraction from tomato power and watermelon juice by TM, the ratios of Z-isomer significantly (p<0.05) increased especially with AITC and DADS (up to about 80%), and extraction yields increased even>100% with capric acid. Lycopene in TM/-capric acid extracts showed low degradation with Z-isomers increasing during storage. TM with capric acid could simultaneously promote lycopene Z-isomerization and extraction.

Effect of packaging materials on lycopene vitamin C and water activity of dried tomato (Lycopersicon esculentum Mill.) powder during storage.

In this work, a storage study was conducted to find suitable packaging material for tomato powder storage. Experiments were laid out in a single factor completely randomized design (CRD) to study the effect of packaging materials on lycopene, vitamin C moisture content, and water activity of tomato powder; The factor (packaging materials) has three levels (low-density polyethylene bag, polypropylene bottle, wrapped with aluminum foils, and packed in low-density polyethylene bag) and is replicated three times. During the study, a twin layer solar tunnel dried tomato slices of var. Galilea was used. The dried tomato slices were then ground and packed (40 g each) in the packaging materials and stored at room temperature. Samples were drawn from the packages at 2-month interval for quality analysis and SAS (version 9.2) software was used for statistical analysis. From the result, higher retention of lycopene (80.13%) and vitamin C (49.32%) and a nonsignificant increase in moisture content and water activity were observed for tomato powder packed in polypropylene bottles after 6 months of storage. For low-density polyethylene packed samples and samples wrapped with aluminum foil and packed in a low-density polyethylene bag, 57.06% and 60.45% lycopene retention and 42.9% and 49.23% Vitamin C retention were observed, respectively, after 6 months of storage. Considering the results found, it can be concluded that lycopene and vitamin C content of twin layer solar tunnel dried tomato powder can be preserved at ambient temperature storage by packing in a polypropylene bottle with a safe range of moisture content and water activity levels for 6 months.

A comparative evaluation of the phenol and lycopene content of tomato by-products subjected to different drying methods

This study is focused on exploring tomato by-products to provide ingredients rich in bioactive compounds with higher functional value through applying innovative techniques (microwave and spiral flash dryer) and conventional techniques (freeze-drying and hot air-drying) to the dehydration of industrial tomato pomace. The effect of the drying method on the bioactive composition of the tomato by-products (phenols, lycopene and soluble dietary fiber) was analyzed. The phenolic composition was determined using a targeted chromatographic approach based on UHPLC-QqQ-MS/MS. Large amounts of naringenin (194.7–949.4 mg/kg) were detected, together with quercetin, caffeic acid, coumaric acid and 4-hydroxybenzoic acid. Microwave dehydration improved the retention of flavanone-like compounds, especially naringenin, and lycopene, while tomato products dehydrated with Spiral Flash dryer showed higher concentrations of flavonols and phenolic acids. The results showed that the industrial application of drying processes using Spiral Flash, and especially with microwaves, could be promising for producing high added-value ingredients from tomato by-products.

Study on the Drying Technology of Tomato Pulp with Phytoene, Phytofluene and Lycopene Retention as Inspection Indexes.

The objective was to design a feasible drying method to increase the retention rates of phytoene (PT), phytofluene (PTF) and lycopene (LYC) in tomato powder. The method was to compare the effects of vacuum freeze-drying (FD), vacuum drying (VD) and hot-air drying (HAD) technologies on tomato pulp rich in PT, PTF and LYC. When dried by HAD, the retention rates of PT, PTF and LYC decreased significantly (p &lt; 0.05) only when the water content decreased from 30% to 3.5%. When dried by VD, the temperatures had no significant effect on the retention rates, and only alkaline conditions (pH = 9), Fe3+ and Al3+ could significantly reduce the retention rates (p &lt; 0.05). Therefore, a combined drying process (CDP) was designed: before the water content decreased to 50%, HD (60 °C) technology was used; then, the paste was dried via VD (80 °C, 0.08 MPa) technology till the water content reached 5 ± 2%; loading weight was 40 g (thinkness 5.70 mm) for each batch. Compared with VD alone, the CDP technology improved the retention rates of PT and LYC by 12% and 36%, respectively, while PTF decreased by only 6%.

Effect of Different Predrying Treatments on Physicochemical Quality and Drying Kinetics of Twin Layer Solar Tunnel Dried Tomato (Lycopersicon esculentum L.) Slices

In tomato drying, degradation in final quality may occur based on the drying method used and predrying preparation. Hence, this research was conducted to evaluate the effect of different predrying treatments on physicochemical quality and drying kinetics of twin-layer-solar-tunnel-dried tomato slices. During the experimental work, tomato slices of var. Galilea were used. As predrying treatments, 0.5% calcium chloride (CaCl2), 0.5% ascorbic acid (C6H8O6), 0.5% citric acid (C6H8O7), and 0.5% sodium chloride (NaCl) were used. The tomato samples were sliced to 5 mm thickness, socked in the pretreatments for ten minutes, and dried in a twin layer solar tunnel dryer under the weather conditions of Jimma, Ethiopia. Untreated samples were used as control. The moisture losses from the samples were monitored by weighing samples at 2 h interval from each treatment. SAS statistical software version 9.2 was used for analyzing data on the physicochemical quality of tomato slices in CRD with three replications. From the experimental result, it was observed that dried tomato slices pretreated with 0.5% ascorbic acid gave the best retention of vitamin C and total phenolic content with a high sugar/acid ratio. Better retention of lycopene and fast drying were observed in dried tomato slices pretreated with 0.5% sodium chloride, and pretreating tomatoes with 0.5% citric acid resulted in better color values than the other treatments. Compared to the control, pretreating significantly preserved the overall quality of dried tomato slices and increased the moisture removal rate in the twin layer solar tunnel dryer.

Vacuum-Assisted Osmotic Dehydration of Autumn Olive Berries: Modeling of Mass Transfer Kinetics and Quality Assessment.

Autumn olive fruits were osmo-dehydrated in sucrose solution at 70 °C under vacuum and atmospheric pressure. The mass transfer kinetics data were applied to the models of Azuara, Crank, Page, and Peleg. The Peleg model was the best-fitted model to predict the water loss and solid gain of both treatments. The vacuum application decreased the effective diffusivities from 2.19 × 10−10 to 1.55 × 10−10 m2·s−1 for water loss and from 0.72 × 10−10 to 0.62 × 10−10 m2·s−1 for sugar gain. During the osmotic dehydration processes, the water activity decreased and stabilized after 5 h, while the bulk densities increased from 1.04 × 103 to 1.26 × 103 kg/m3. Titratable acidity gradually reduced from 1.14 to 0.31% in the atmospheric pressure system and from 1.14 to 0.51% in the vacuum system. pH increased significantly in both systems. Good retention of lycopene was observed even after 10 h of treatments. For the color parameters, the lightness decreased and stabilized after 30 min. In comparison, the redness and yellowness increased in the first 30 min and gradually decreased towards the initial levels in the fresh fruit.

Physicochemical quality of twin layer solar tunnel dried tomato slices

The objective of this experimental study was to evaluate the effect of twin layer solar tunnel drying on physicochemical quality of tomato slices. The novelty of this dryer is that it has two layers of trays unlike Hohenheim solar tunnel dryer which makes it to have drying capacity of more than two times compare to type hohenheim solar tunnel dryer with equal collector area. The experiment consists of two (tray position and drying position) factors with two levels of tray position (upper tray (samples exposed to direct solar radiation) and lower tray (samples are exposed to only heated air)) and three levels of drying position (collector out let,middle of the dryer and dryer out let) with three replications. During the experiment 180 kg of Tomato slices of Galilea variety with 5mm thickness were dried in the twin layer solar tunnel dryer. Data on physicochemical quality of tomato were collected and analyzed using SAS (version 9.2). software. From the experimental result; an increase in lycopene and phenolic content retention along the length of the dryer was observed while Vitamin C retention showed a decreasing trend. Large retention of total phenol, lycopene and beta carotene content were observed for the lower tray dried tomato slices compared to the upper tray dried ones. The water activity and PH values of the solar tunnel dried tomatoes were within the safe range from microbial growth, enzymatic and non-enzymatic browning. Compared to sun drying; solar tunnel dried tomatoes showed a much better nutrient retention for all quality parameters which is comparable with the data reported for energy intensive mechanical dryers.

Supercritical CO2 Extraction and Microencapsulation of Lycopene-Enriched Oleoresins from Tomato Peels: Evidence on Antiproliferative and Cytocompatibility Activities.

Tomato peels are used as a valuable material to extract lycopene-rich oleoresins by supercritical CO2 extraction. The extraction involves continuous circling of CO2 to the extractor after removing the solute in the separators, S40 and S45, where the solvent power of the CO2 is reduced by reducing pressure down to 20 MPa in S40 and 5 MPa in S45, respectively, leading to two extracts. Lycopene is found to be the major compound, representing 93% and 76% of the total carotenoids in S40 and S45 extracts, respectively. The two extracts are microencapsulated in whey protein concentrate and acacia gum by complex coacervation and freeze-drying, leading to corresponding P40 and P45 powders, with antioxidant activity of 8.57 ± 0.74 and 9.37 ± 0.48 mMol TEAC/g DW in P40 and P45, respectively. Different structural and morphological patterns are observed, with finer microparticles of 1–2 µm in P45. Both powders show dose and time-dependent antiproliferative activity. The half-maximal inhibitory concentration values are 100 µg/mL for P40 and 750 µg/mL for P45 sample, indicating a higher antiproliferative effect of P40 over P45 in HT-29 cell culture. The powders have an extended range of cytocompatibility, up to 1000 µg/mL, in L929 normal cells, stimulating the cell growth. Lycopene retention is tested, and values of 48% and 29% in P40 and P45 are found after 21 days at 25 °C, with the degradation rate in P45 significantly higher, due to the higher content of the surface lycopene, which favored its degradation.

Impact of ultrasound processing parameters on physical characteristics of lycopene emulsion.

Using ultrasound technology for obtaining O/W lycopene emulsions needs analyzing the parameters for the enhanced application. To this end, O/W lycopene emulsions (30:70) were processed using ultrasound with powers of 240W and 360W in 5, 10, and 15min. Afterward, the poly dispersity index, droplet size, ζ-potential, turbidity, phase separation, lycopene concentration, rheological behavior, surface tension, and morphology of emulsions was investigated. The experimental results showed good emulsifying characteristics with respect to droplet size and ζ-potential. If the mean values of the droplet size were significantly reduced and the ζ-potential increased. The ultrasound application had a significant impact on emulsion stability with no phase separation and significantly high lycopene retention. Ultrasound reduced the apparent viscosity by reducing the particle size due to the energy supplied to the system. The final emulsion that was treated at 360W, and 2160J/cm3 in 10min, presented enhanced technological properties appropriate for food products.

Encapsulation of lycopene within oil-in-water nanoemulsions using lactoferrin: Impact of carrier oils on physicochemical stability and bioaccessibility

The influence of physicochemical properties of carrier oils on nanoemulsion stability and the bioaccessibility of lycopene were studied. Lycopene-loaded nanoemulsions were prepared by using sesame oil, linseed oil or walnut oil as the oil phase and lactoferrin as the emulsifier. The stability was investigated by particle size, zeta potential, pH sensitivity, thermal stability and lycopene retention. Results showed that the stability was positively correlated with oil density but negatively related to oil viscosity and unsaturation degree; the lycopene nanoemulsion prepared by sesame oil exhibited greater stability and a slower degradation rate of lycopene compared to the other nanoemulsions. In addition, the lycopene retention in sesame oil-nanoemulsions was significantly higher during the first three weeks of storage. The bioaccessibility of lycopene, as measured by a simulated gastrointestinal model, was greatly improved in the nanoemulsion system. The lycopene bioaccessibility was around 25% in sesame oil- and linseed oil-nanoemulsions, and 18% in walnut oil-nanoemulsions, showing a similar trend with their stability. This information may facilitate the design of more efficacious lycopene-fortified delivery systems.

Chemical Stability of Lycopene in Processed Products: A Review of the Effects of Processing Methods and Modern Preservation Strategies.

Lycopene, one of the most dominant carotenoids in a person's diet, is a well-known natural compound that has protective effects against chronic diseases. Industrial and domestic processing and storage conditions significantly influence retention and isomerization of lycopene; thus, in recent years, great attention has been given for their preservative effects of lycopene. This review highlights recent strategies that have been developed to preserve lycopene in processed products, especially in tomato pulp, puree, paste, and juice. The key factors influencing lycopene degradation and isomerization, such as ingredients and intensity of thermal treatments, are also discussed. Special attention was paid to the crystalline structures of lycopene which facilitate its resistance to degradation and isomerization. Emerging non-thermal processing methods, such as ultrasound and high-pressure processing (HPP), are critically evaluated for their preservation of thermo-labile compounds. Novel trends to improve lycopene stability by micro- and nanoencapsulation and addition of antioxidants are also included to examine their efficacy to protect against light, heat, oxygen, and other oxidative processes. Finally, recommended processing and storage conditions are discussed to provide strategies to retain the highest possible amount of bioactive lycopene until consumption.

The Evaluation of Dietary Addition of Palm and Coconut Oils in Steaming Tomato (Lycopersicon esculentum) Waste Powder on Digestibility of Crude Fiber and Retention of Lycopene and Nitrogen in Broiler Chickens.

The Evaluation of Dietary Addition of Palm and Coconut Oils in Steaming Tomato (Lycopersicon esculentum) Waste Powder on Digestibility of Crude Fiber and Retention of Lycopene and Nitrogen in Broiler Chickens.

Encapsulation of a lycopene-rich watermelon concentrate in alginate and pectin beads: Characterization and stability

The aim of this work was to evaluate the influence of the type of polymer and the effect of drying on the stability of lycopene-rich beads obtained by ionic gelation of a watermelon concentrate. Sodium alginate and pectin were used as polymers for encapsulation. The wet and the dried beads were characterized for lycopene retention when exposed to different thermal treatments (60 °C and 90 °C) and pHs (2, 5 and 8), as well as for particle size distribution, morphology and thermogravimetric analysis. All the particles showed high lycopene protection against the evaluated conditions of temperature and pH. Storage stability at different temperatures was also evaluated. The wet beads produced with alginate and pectin showed lycopene retention of 29 and 21%, respectively, after 8 weeks of refrigerated storage, while the dried beads were showed retentions higher than 80% above 25 °C. Ionic gelation showed to be a promising alternative to obtain stable lycopene-rich dried ingredients.

Combined effect of vacuum and different freezing methods on the quality parameters of cherry tomato (Lycopersicon esculentum var. Cerasiforme)

Freezing has been a convenient technique to maintain the shelf stable properties of tomato fruits and to permit the transportation of the products to remote markets. This study evaluated the effects of four different freezing methods on the quality of cherry tomatoes (Lycopersicon esculentum var. Cerasiforme). Fresh, whole cherry tomatoes were frozen using multistage freezing (I), vacuum pre-treatment + individual quick frozen (IQF) (II), vacuum pre-treatment + static freezing (III), and vacuum pre-treatment + multistage freezing (IV) methods, and afterward stored in polyethylene terephthalate/polyethylene terephthalate/polyethylene (PET/PET/PE) bags at -20 °C and analyzed during 5 months of storage. The percentage of skin cracking, ion leakage, pectolytic enzyme activities, colour values, and lycopene content as well as the total dry matter content and pH values of the cherry tomatoes were significantly affected by both the freezing techniques and storage period. The highest skin cracking and ion leakage and also the highest lycopene retention were found in the vacuum pre-treatment + IQF treated samples. The vacuum pre-treatment + multistage freezing resulted in the lowest skin cracking especially in the early stages of storage. The ion leakage values displayed negative correlations with colour values and lycopene contents. However, the enzyme activities exhibited significant positive correlations with both the colour values and lycopene contents. The lack of correlation between the skin cracking and enzyme activities suggest that the cracking problem is not mainly caused by pectolytic enzyme activities.

Nanoencapsulation by electrospinning to improve stability and water solubility of carotenoids extracted from tomato peels

The current study demonstrated the electrospinning technique to stabilize the carotenoids. Gelatin nanofibers containing the carotenoids extracted from tomato peel (TP) were successfully fabricated with above 90% encapsulation efficiency by electrospinning. SEM analysis revealed that the extract-loaded fibers exhibit similar morphology as the neat fibers with a bead-free, smooth, and homogeneously-distributed morphology. Thermal stability of the extract was improved by nanoencapsulation. FTIR spectra showed that the TP extract could be compatibly entrapped into the gelatin fibers. Compared to non-encapsulated extract, the encapsulated one inside gelatin fibers had better retention of lycopene and antioxidant activity during 14-days storage. More interestingly, the water solubility of the carotenoid extract was highly enhanced compared to non-encapsulated one. By this study, it was realized that nanoencapsulation by electrospinning is an effective way to stabilize carotenoids and improve their water solubility, therefore it is promising to use them in food processing, especially including aqueous food matrix.

Effect of drying methods on the retention of bioactive compounds in African eggplant.

African eggplants (Solanum aethiopicum L.) are a rich source of bioactive compounds and functional constituents that are beneficial to human health. However, the short shelf life of these vegetables can be a major cause of postharvest losses especially during peak harvesting season. Drying is one of the most convenient technologies for the production of shelf stable food products. However, drying can lead to considerable loss of the available bioactive compounds due to thermal degradation depending on the drying method and temperature conditions. This study investigated the effect of four drying methods (solar, oven, vacuum, and freeze) on the retention of total phenolics, beta‐carotene, antioxidant capacity, and lycopene in five African eggplant (S. aethiopicum) accessions (sangawili, manyire green, S00047A, AB2, and aubergine blanche). Samples were dried up to ~10% moisture content. The fresh and dried samples were analyzed for total phenolic content, antioxidant capacity, beta‐carotene content, and the lycopene content. In the fresh state, beta‐carotene, total phenolic content, and free radical scavenging activity ranged between 14.75 ± 0.50 and 29.50 ± 0.77 mg/100 g db, 751.21 ± 1.73 and 1,363.95 ± 2.56 mg/100 g GAE db, and 99.58 and 325.61 mg/ml db IC 50 value, respectively. The accession S00047 showed highest total phenolic content and lowest IC 50 value in the fresh samples. The results also showed that total phenolic content, antioxidant capacity, and beta‐carotene contents were significantly (p < .05) affected by drying method and drying temperature with freeze‐drying presenting the highest retention. Overall, 36.26%s–95.05% (total phenolics) and 31.44%–99.27% (beta‐carotene) were retained during freeze‐drying. Lycopene was only detected in the dried samples of the accession manyire green but absent in all the fresh samples of all the accessions. This study demonstrates that freeze‐drying was the most effective in retaining the highest bioactive compounds in African eggplants.

Changes in lycopene content and quality of tomato juice during thermal processing by a nanofluid heating medium

The main aim of this study was to evaluate the effects of shortening common thermal processing through nanofluids on quality of tomato juice for the first time. For this purpose, three different temperatures (between 70 and 90 °C), nanoparticle concentrations (between 0 and 4%) and time (between 30 and 90 s) were selected for thermal processing of tomato juice in a shell and tube heat exchanger through central composite design. The findings indicated that while 4% nanoflluid at 30 °C for 30 s led to the best lycopene retention (96%) of tomato juice, hot water treatment (0% nanoparticle concentration) at 90 °C for 90 s resulted in the lowest lycopene retention (67%). The durations required for product to reach a certain temperature were dwindled and treated samples experienced lower color drops when higher nanoparticle concentrations were applied; a*/b* indices at 80 °C were 1.7, 1.8 and 1.9 for 0, 2 and 4% nanoparticles, respectively; indeed, higher nanoparticle concentration, and lower temperature and time led to higher lycopene retention and, as a consequence, higher a*/b* values. The effect of time on pH and acidity indices was not significant while temperature influenced those parameters significantly. Based on the indices considered, if temperature, concentration and time are set at 70 °C, 4% and 30 s, the best responses will be obtained.