Lower Surface Roughness Values Research Articles

Thermal damage diagnosis in micro grinding processes based on raw acoustic emission signals and convolution neural networks

A micro-grinding process is usually the last machining operation among the various processes employed in the manufacturing of metallic components. It is generally the first option when the manufactured products require a combination of low surface roughness values and narrow dimensional tolerances. However, one of the main challenges of a micro-grinding process is avoiding high specific energy and the corresponding intense heat generation, as this can damage the workpiece. The energy consumed during micro-grinding is almost entirely converted into heat, making the component susceptible to thermal damage. As the occurrence of this damage compromises the service life of manufactured components, the implementation of monitoring systems is essential to guarantee the quality of the manufactured products improving process efficiency. In this study, a new approach based on convolution neural networks (CNNs) is proposed to predict the occurrence of thermal damage in the micro-grinding process. This approach uses raw acoustic emission (AE) signals as inputs into CNN, which is a more technically feasible approach to performing real-time monitoring. To obtain the AE data, micro-grinding experiments were conducted on N2711 grade steel (which is susceptible to thermal damage) under different cutting conditions (ae = 5–50 µm). The obtained AE signals were labeled based on the offline analyses performed on the workpieces, which identified the occurrence of thermal damage through visual inspections, microhardness, and microstructural analysis. For the conditions employed in this work, thermal damage was obtained after grinding with depth of cut values > 10 µm. Total 3960 AE signals were obtained of which 2200 of them were associated with thermal damage. The results depict that the proposed CNN model was able to successfully classify normal and thermal damage AE signals reaching an accuracy of 98.6% over the dataset (0.4% false positives and 1.0% false negatives).

Effect of Graphene Oxide Nanoparticles Incorporation on the Mechanical Properties of a Resin-Modified Glass Ionomer Cement.

The objective of this study was to evaluate the effect of incorporating different concentrations of graphene oxide (GO) nanoparticles on the mechanical properties of a resin-modified glass ionomer cement (RMGIC). A commercial RMGIC (Resiglass R, Biodinâmica) was modified by incorporating 0.1% and 0.5% (by weight) of GO into the powder's material. An unmodified RMGIC was used as a control group. Powder samples were characterized using Scanning Electron Microscopy (SEM) and Energy Dispersive Spectroscopy (EDS). Specimens were fabricated and subjected to flexural strength (n = 15), modulus of elasticity (n = 15), Vicker's microhardness (n = 10), and surface roughness tests (n = 10). Data were analyzed using one-way ANOVA and Tukey's post hoc test (α = 5%). Experimental groups' powder demonstrated a homogeneous dispersion of GO. No statistically significant difference was observed in flexural strength (p = 0.067) and modulus of elasticity (p = 0.143) tests. The groups containing 0.1% and 0.5% GO showed significantly higher microhardness and lower surface roughness values (p < 0.001) compared to the control group. The incorporation of GO nanoparticles at concentrations of 0.1% and 0.5% improved the microhardness and surface roughness without negatively affecting the flexural strength and modulus of elasticity of an RMGIC.

Atomic scale smoothing of nanoscale quartz mold using amorphous carbon films

Abstract Surface roughness control of end products is increasingly becoming significant, especially with the miniaturization trends in the semiconductor industry. Ultra-thin amorphous carbon (a-C) films offer a prime solution to optimize surface roughness due to their outstanding characteristics. In this study, hydrogenated a-C films are deposited on two-dimensional quartz plates and three-dimensional quartz molds to evaluate the growth mechanisms and changes in the surface roughness, which is supported by molecular dynamics simulations. Results reveal that surface roughness encounters multiple variations until it reaches stable values. These fluctuations are categorized into four different stages which provide a concrete understanding of various growing mechanisms at each stage. Different behavior of the atoms in the top layers is recorded in the cases of normal and grazing incidents of carbon atoms. Lower surface roughness values are obtained at low-angle deposition. Interestingly, surface smoothing is attained on the sidewalls of the nanotrench mold where the deposition occurs with high incident ion angles.

An Investigation of the Effect of Novel Mono/Bi-Layered PVD-Coated WC Tools on the Machinability of Ti-5Al-5V-5Mo-3Cr.

The Ti-5Al-5V-5Mo-3Cr (Ti-5553) alloy is a relatively novel difficult-to-cut material with limited machinability and tool life analysis available in the literature, and hence requires further investigation. This study focuses on the machining and tribological performance of Ti-5553 under high-speed finish turning (150 m/min, 175 m/min, and 200 m/min) via novel mono/bi-layered PVD-coated WC tools. A base AlTiN coating is used as the reference monolayer coating, with AlCrN, diamond-like ta-C, and TiAlSiN coatings each deposited on top of a base AlTiN coating, totaling four separate coated tools (one monolayer and three bi-layer). Tool life, cutting forces, workpiece surface quality, and tribological chip analysis are among the subjects of investigation in this study. Overall, the AlTiN/AlCrN coated tool outperformed all the other combinations: an improvement of ~19% in terms of tool life in reference to the base AlTiN coating when averaging across the three speeds; lowest surface roughness values: ~0.30, 0.33, and 0.64 µm; as well as the lowest chip back surface roughness values: ~0.80, 0.68, and 0.81 µm at 150, 175, and 200 m/min, respectively. These results indicate that the AlTiN/AlCrN coating is an excellent candidate for industrial applications involving high-speed machining of Ti-5553.

Subnanoscale Ion Beam Modification-Assisted Smoothing of Heterostructure Surfaces.

Glass ceramic (GC) is the most promising material for objective lenses for extreme ultraviolet lithography that must meet the subnanometer precision, which is characterized by low values of high spatial frequency surface roughness (HSFR). However, the HSFR of GC is typically degraded during ion beam figuring (IBF). Herein, a developed method for constructing molecular dynamics (MD) models of GC was presented, and the formation mechanisms of surface morphologies were investigated. The results indicated that the generation of the dot-like microstructure was the result of the difference in the erosion rate caused by the difference in the intrinsic properties between ceramic phases (CPs) and glass phases (GPs). Further, the difference in the microstructure of the IBF surface under different beam angles was mainly caused by the difference in the two types of sputtering. Quantum mechanical calculations showed that the presence of interstitial atoms would result in electron rearrangement and that the electron localization can lead to a reduction in CP stability. To obtain a homogeneous surface, the effects of beam parameters on the heterogeneous surface were systematically investigated based on the proposed MD model. Then, a novel ion beam modification (IBM) method was proposed and demonstrated by TEM and GIXRD. The range of ion beam smoothing parameters that could effectively converge the HSFR of the modified surface was determined through numerous experiments. Using the optimized beam parameters, an ultrathin homogeneous modified surface within 3 nm was obtained. The HSFR of GC smoothed by ion beam modification-assisted smoothing (IBMS) dropped from 0.348 to 0.090 nm, a 74% reduction. These research results offer a deeper understanding of the morphology formation mechanisms of the GC surfaces involved in ion beam processing and may point to a new approach for achieving ultrasmooth heterostructure surfaces down to the subnanometer scale.

Effects of grinding mode on grinding performance of anisotropic CF/PEEK composites

AbstractGrinding could be used to enhance accuracy and quality of carbon fiber‐reinforced poly‐ether‐ether‐ketone (CF/PEEK) composites. However, the grinding mode, namely up‐grinding (UG) or down‐grinding (DG), is usually neglected while unbefitting grinding mode choice may cause inferior surface quality. To investigate effects of grinding modes on grinding performance of anisotropic CF/PEEK, grinding experiments in UG and DG were carried out under different fiber orientation angles θ. Experimental results indicated that maximum grinding temperatures and normal grinding forces in UG were lower than DG regardless of the abrasive grit sizes. Material removal mechanisms of CF/PEEK affected by grinding mode were revealed by analyzing morphologies of surface, chip and grinding wheel. When θ = 0°, the dominant mechanisms in DG were extrusion fracture and fiber deformation, while they were interface shear debonding and bending fracture in UG. When θ = 90°, the dominant mechanisms in DG included interface layer separation and bending fracture, while they were shear and extrusion fracture of well‐supported fibers in UG. Thus, UG was more favorable for material removal, obtaining lower surface roughness values, fewer machining defects and less wheel wear than DG. This study will provide technical guidance for high‐quality grinding of carbon fiber‐reinforced thermoplastic composites.Highlights The effects of grinding modes (DG and UG) on the grinding performance of anisotropic CF/PEEK composites were investigated. Material removal mechanisms of CF/PEEK affected by grinding mode were revealed under different fiber orientation angles. The maximum grinding temperatures and normal grinding forces in UG were lower than DG. UG was more favorable for material removal in grinding, and could produce better ground surface quality than DG.

Effect of polymerization methods on surface roughness and hardness of commercially available self-curing acrylic resins: a comparative study

Purpose This paper aims to compare the surface roughness and hardness of three commercially available self-curing acrylic resins for dental use, under different polymerization conditions. Design/methodology/approach A comparative in vitro study was conducted using a convenience sample of 12 × 5 × 2 mm blocks with n = 40 for each material (Nic Tone, Arias Plus and Orthocryl®), with subgroups according to the polymerization method: conventional (C) and polymerization under ambient conditions (A). The surface roughness of the materials was measured using a profilometer; hardness was measured with a portable hardness tester. Additionally, surface morphology as well as particles size and morphology were evaluated with scanning electron microscopy. Findings There were significant differences in roughness and hardness values between the three self-curing acrylic resins (p &lt; 0.05), as well as within each self-curing acrylic resin according to the polymerization method used (p &lt; 0.05). The samples polymerized with the conventional method presented lower surface roughness and hardness values. Originality/value This study provides scientific evidence of values not provided by manufacturers in relation to the surface roughness and hardness of these materials, and all of them met the ideal minimum values of surface roughness, regardless of the polymerization technique used.

Machinability and pulse characteristics of Ti-16Al-14Nb (α/β) alloy in wire-electric discharge machining process: A surface integrity study

The goal of the present work is to produce the efficient cutting of Ti-16Al-14Nb (α/β) alloy through wire-electric discharge machining and contemplate the terminologies such as machining ability, surface integrity and material removing capability. For this, the experimentation has been designed by considering three process parameters, pulse-on time ( Ton), pulse-off time ( Toff) and peak current ( Ip) at three significant levels (low, high, intermediate) in L27 order designed from design of experiments. The effect of these process variables on pulse characteristics, surface roughness ( Ra), kerfwidth ( Kw) and material removal rate ( MRR) is analyzed and mathematically modeled with analysis of variance. The results state that the highest MRR (0.521, 0.51, 0.506 mm3/sec) and low surface roughness (8.91, 8.89, 8.68 µm) values are observed at the highest level (110 µs, 15 µs, 8 A). If the pulse duration is kept at low ( Ton = 40µs, Toff = 3µs), the increase in peak current from 3 A to 8 A leads to a 64.54% increase in MRR and a 52.9% increase in Ra values. ANOVA results stated that Ton has contributed 20.4%, 35.8% and 19.3%, and Ip has contributed 43.1%, 30.5% and 46.6% influence on MRR, Kw and Ra respectively. The voltage–current characteristics studies confirmed that the strong intense pulses at a higher peak current (8 A) resulted in the increased MRR (0.521 mm3/sec) and Ra (8.43 µm) leading to the formation of swages and ridges. The surface integrity analysis derived from Abbott–Firestone curve agreed that the lowest level has shown better skewness ( Rsk = −0.274) and at highest level showed a larger deviation in skewness ( Rsk = +2.672) signifies that higher asymmetry (poor) of the surface.

Effects of abrasive grain size of flexible body-armor-like abrasive tool (BAAT) on high-shear and low-pressure grinding for zirconia ceramics

Zirconia ceramics exhibit remarkable performance. However, the high hardness and brittleness poses enormous challenges for machining. This study is integrally focused on preparing a flexible body-armor-like abrasive tool (BAAT) with enhanced tangential-to-normal force ratio. The rheological characteristics of the BAAT abrasive system with different abrasive grain were investigated. A series of grinding tests were conducted on a precision grinding machine. The grinding performance of the BAAT with different abrasive grain sizes was examined. Surface roughness (Ra) variation and tangential-to-normal force ratio were analyzed, together with the investigation of the three-dimensional surface morphology and surface hydrophilicity. It was found that smaller abrasive grain sizes ultimately generated lower surface roughness values after grinding. Under the optimal grinding conditions, the surface roughness (Ra) of zirconia ceramics decreased from 102 nm to 1.7 nm after 5 grinding strokes (∼1 min). Meanwhile, uniform grinding textures were obtained.

Fused filament fabrication using stainless steel 316L‐polymer blend: Analysis and optimization for green density and surface roughness

AbstractThis study is centered on the analysis of composite component additive manufacturing, via fused filament fabrication (FFF), comprising of 316L stainless steel particles in a polymer matrix. It examines the impact of several process factors of FFF, including extrusion speed, layer height, and extrusion temperature, on the density and surface roughness with the goal to minimize porosity. The independent and interaction impacts of these parameters were investigated using a central composite design technique. The technique of analysis of variance was utilized to determine the influence of relevant factors. Regression analysis was used to establish statistical models linking the parameters to green density and surface roughness. The green density was enhanced by reducing the layer height from 0.2 to 0.1 μm and decreasing the nozzle speed from 100 to 20 mm min−1. The surface roughness was improved by using a slow printing speed and minimum layer height. The ideal temperature range for producing favorable results in terms of green density and surface roughness during extrusion was found to be between 235 and 240°C. Significant correlations were found between the parameters and the green density and surface roughness. A genetic algorithm was used as an optimisation tool to determine the thresholds that would provide the highest green density and the lowest surface roughness values. The porosity of the samples generated with the optimized settings was evaluated using microtomography scans. The methodology presented here can be applied to composite and standard polymeric filament printing to determine optimal printing parameters.Highlights Blend of stainless steel 316L and polymer was used for fused filament fabrication. Printing speed and layer height were the dominating for density and roughness. Height 0.2 mm, speed 20 mm s−1, and temperature 239°C resulted 4.73 g cm−3 density and 21.09 μm roughness Microtomography revealed porosity of 1.7% in the optimized sample.

The effect of different liquids on the surface roughness and color stability of single shade and nanohybrid resin composites: An AFM and SEM analysis.

The aim of this study is to evaluate the surface roughness (SR) and color changes of single-shade and nanohybrid resin-based restorative materials (RBC) after immersion in liquids at different pH values. For RBCs, a total of 120 specimens, 30 for each material, were prepared using 10 mm diameter and 2 mm thick molds. For flowable bulk fill RBC, a total of 40 specimens, 10 for each material, were prepared using 10 mm diameter and 4 mm thick molds (n = 10). After initial color and SR measurements, samples were stored in the liquids for 14 days and all of the measurements were repeated on 14th days. Scanning electron microscopy and atomic force microscopy analyzes were performed in all groups. When SR results are examined; among all liquids, the highest SR value was observed in the Carisma Diamond One (CDO) group, while the lowest SR value was observed in the Omnichroma Flow Bulk (OMF) group (p < .05). When the color changes (ΔE) results are examined; it was observed that CDO group had highest color change and OMF group had the lowest values. It has been observed that among the liquids, the liquids that affect the ΔE values of the materials the most are coffee and cola. When the ΔE values of the subgroups of the materials were examined, there was a statistically significant difference in all subgroups of RBCs (p < .05). While acidic liquids increased the SR of RBCs, coffee more affected the color change of RBCs. RESEARCH HIGHLIGHTS: Clinicians should keep in mind that the RBCs tested may change their surface properties and colors when exposed to various liquids. People who have RBCs should pay attention to the consumption of acidic and highly pigmented liquids.

Deep-reactive ion etching of silicon nanowire arrays at cryogenic temperatures

The pursuit of sculpting materials at increasingly smaller and deeper scales remains a persistent subject in the field of micro- and nanofabrication. Anisotropic deep-reactive ion etching of silicon at cryogenic temperatures (cryo-DRIE) was investigated for fabricating arrays of vertically aligned Si nanowires (NWs) of a large range of dimensions from micrometers down to 30 nm in diameter, combined with commonly used wafer-scale lithography techniques based on optical, electron-beam, nanoimprint, and nanosphere/colloidal masking. Large selectivity of ∼100 to 120 and almost 700 was found with resists and chromium hard masks, respectively. This remarkable selectivity enables the successful transfer of patterned geometries while preserving spatial resolution to a significant extent. Depending on the requirements by applications, various shapes, profiles, and aspect ratios were achieved by varying process parameters synchronously or asynchronously. High aspect ratios of up to 100 comparable to the best result by metal-assisted wet-chemical etching and sub-μm trenches by DRIE were obtained with NW diameter of 200 nm, at an etch rate of ∼4 μm/min without being collapsed. At the same time, low surface roughness values were maintained on the NW top, sidewall, and bottom surface of ∼0.3, ∼13, and ∼2 nm, respectively, as well as high pattern fidelity and integrity, which were measured using angle-resolved Fourier microscopy, combined atomic force, and scanning electron microscopy on selected NWs. This work establishes the foundation in the controllable development of Si nanoarchitectures, especially at sub-100 nm structures, for energy-harvesting and storage, damage-free optoelectronics, quantum, photovoltaics, and biomedical devices.

Effect of the incorporating of refractory NbC precipitates in intermetallic iron-aluminide coatings on corrosion and high-temperature oxidation behavior

This study aims to investigate the effects of growing niobium carbide (NbC) particles into intermetallic iron-aluminide (FeAl) coatings on ductile cast iron (SGI) by thermo-reactive diffusion technique (TRD). The study compares the corrosion and oxidation behavior of the FeAl-NbC coatings with SGI, FeAl, and NbC coatings. Corrosion tests were conducted through polarization tests in a 3.5 wt% NaCl solution, while oxidation tests were performed at 900 °C for 4, 16, and 64 h. Before and after corrosion and oxidation tests, the coatings were examined using scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS), and X-ray diffraction (XRD). The findings show that FeAl coatings with NbC particles had lower graphite nodules, porosity, and surface roughness values compared to FeAl coatings. FeAl-NbC composite coatings provided better corrosion and oxidation resistance compared to untreated SGI, FeAl, and NbC coatings. The results of the comparative analysis of FeAl-NbC, FeAl, NbC, and untreated SGI specimens indicate that corrosion resistance in a 3.5 wt% NaCl solution and oxidation resistance at 900 °C followed the order FeAl-NbC > FeAl > NbC > SGI.

Effect of pulse time (Ton), pause time (Toff), peak current (Ip) on MRR and surface roughness of Cu–Al–Mn ternary shape memory alloy using wire EDM

Shape memory and super elasticity are two outstanding properties of Cu–Al–Mn SMAs together with additional copper-based shape memory alloys that make them superior to NiTi alloys. It's quite hard to machine Cu–Al–Mn SMA. The machinability properties of Cu–Al–Mn SMAs during Wire Electrical Discharge Machining (WEDM) were experimentally investigated using molybdenum wire as the electrode material. Material Removal Rate (MRR) and Surface Roughness (SR) are two machining qualities that are studied in relation to the combinational values of pulse time (Ton), pause time (Toff), and peak current (Ip), which are selected as the changeable input process factors. From the experimental investigation, it was found that both MRR and Ra values were increased with an increase in pulse on time(Ton), pulse off time(Toff), and peak current (IP)values. Because the wire electrode contains maximum current under these conditions, it is easy to remove more material at the tool and work material interface, resulting in moderate surface finish. Surface quality was higher on samples machined at low energy input than it was on samples machined at high energy input. This SEM micrograph clearly shows that a lower pulse on time produces a superior surface quality.SEM images and the analysis of the machined surface morphology on the surface of the CAM7 alloy clearly showed that the machined surface of the alloy had a lower surface roughness value at a lower Ip-2A and was associated with a higher surface roughness value at a higher Ip-6A, as well as a lot of uncleared debris and blow holes.

Development and electrochemical investigations of enhanced corrosion-resistant Polyvinylcarbazole-TiO2 hybrid nanocomposite coatings on 316L SS for marine applications

The present study focuses on evaluating the corrosion resistance of 316L stainless steel substrates with Polyvinylcarbazole (PVK)/TiO2 hybrid nanocomposite coatings (HNC). Using the chronoamperometry approach, the HNC were electrochemically synthesized on 316L stainless steel substrates, incorporating various weight (%) 1 %, 2 %, 3 % of TiO2 nanoparticles into the PVK matrix. The findings of the surface morphology investigation verified that the 316L SS had a dense and smooth PVK/TiO2 coating. A low surface roughness and high contact value of the PVK/TiO2 coatings are also responsible for the decrease in corrosion rate of the 316L SS. The corrosion protection efficiency of the PVK/TiO2 HNC were investigated through open circuit potential (OCP) measurement, potentiodynamic polarization and electrochemical impedance spectroscopy (EIS) analysis in 3.5 wt% NaCl solution. The corrosion rate obtained from the polarization studies of the HNC coatings as follows PVKT-2 < PVKT-3 < PVKT-1 < PVK < 316L SS. Results revealed that an optimal loading of 2 wt% TiO2 nanoparticles significantly enhanced the corrosion resistance of the coating. The enhanced electrochemical impedance response for PVK/TiO2 coatings was verified by EIS experiments. The study demonstrates that the incorporation of TiO2 nanoparticles into the PVK matrix effectively creates a barrier layer at the coating-metal interface, inhibiting the entry of aggressive ions. Microhardness studies revealed the increase in hardness value of the PVK and PVK/TiO2 coatings indicated the protective nature of the coating and provided high mechanical strength to 316L SS. The tape adhesion tests carried out on the coated specimens also indicated a good adhesion of the PVK/TiO2 on the 316L SS surface.

Experimental and statistical investigation of electro-erosion machining performance of cryogenic treated hardened AISI H13 hot work tool steel

This study investigated the machinability of AISI H13 hot work tool steel with a hardness of 54 HRC, which has been deep cryogenically treated using the electro-erosion machining technique, one of the unconventional manufacturing methods. The machinability parameters used in the study were determined as current (4, 8 and 12 A), pulse time (200, 300 and 400 µs) and three different electrodes (Copper, Graphite and Tuncop). The experimental design was designed according to the Taguchi L27 model, and machinability tests were carried out to examine the results obtained from the experimental study both experimentally and statistically. When the literature was examined, it was seen that cryogenic treatment was generally applied to electrode materials, and only surface roughness and material wear amounts were examined as output parameters. The original value of the study is the interpretation of the results by applying cryogenic treatment to the test material and exploring the surface roughness and material wear amount, as well as the hole diameters and criterion diameters formed on the treated surfaces after the EDM process. As a result of the study, it was observed that the surface roughness value, the hole diameter, the amount of material wear, and the crater diameter increased with the increase in ampere and impact time. The lowest surface roughness value was 2.266 µm in the graphite electrode material at 4 amps and 200 µs impact time and the highest wear amount was realized as 0.555 g in the copper electrode material 12 amps and 400 µs impact time. The smallest hole diameter was 12.254 mm with a tuncop electrode with a pulse duration of 4 amps and 200 µs, and the lowest crater diameter was 127.301 µm with a graphite electrode at a current of 4 amps and a pulse duration of 200 µs. When the signal-to-noise ratios were examined, the optimum machining parameters for surface roughness, hole diameter, material wear amount, and crater diameter were determined as A2B1C1, A1B3C3, A3B1C1, and A3B1C1, respectively. When the ANOVA results are examined, it is determined that the most effective parameter for the surface roughness is of the current value with 86.54%, the most effective parameter for the hole diameter is the electrode material with 85.20%, the most effective parameter for material wear amount is the electrode material with 45.67% and the most effective parameter for the crater diameter is current value with 75.35%.

Influence of Milling Feed Rate on Surface Roughness of Natural Fiber Composite

The influence of feed rate parameter of milling on natural fiber surface is investigated with constant 1700 rpm spindle speed. In this study, a surface texture-measuring instrument and optical microscope are used as measurement equipments. Ramie fiber composite samples are machined at 2, 4 and 6 mm/min feed rates each. The results shows that the sample machined at 4 mm/min feed rate has the lowest surface roughness value and its surface has a harmonious structure. In addition, many cracks and fractures appeared on the sample surface which machined at 6 mm/min feed rate due to the impact of the cutting edges.

Effect of Incorporation of Poly Vinyl Pyrrolidone on Transverse Strength, Impact Strength and Surface Roughness of Autopolymerizing Acrylic Resin

Autopolymerizing acrylic resin is one of the most frequently used materials in dentistry, but it has relatively poor mechanical properties This study investigated the effect of the addition of poly vinyl pyrrolidone on transverse strength, impact strength and surface roughness of autopolymerzing acrylic resin. A total of 60 specimens were prepared, 30 specimens of each conventional and modified autoplymerizing acrylic.20 specimens of each groups were fabricated with dimensions of (64×10×2.5) mm to conduct the transverse strength and surface roughness tests, while the remaining 10 specimens of each group were fabricated with dimensions of (80×10×4) mm to perform the impact strength test. The results of this study showed that the modified autopolytmerized acrylic had significantly higher transverse strength, and significantly lower surface roughness values while there was no significant differences in impact strength value. It can be concluded that addition of Polyvinylpyrrolidone can improve transverse strength and surface roughness of autopolymerizing acrylic resin.

Osteoblast Attachment on Bioactive Glass Air Particle Abrasion-Induced Calcium Phosphate Coating.

Air particle abrasion (APA) using bioactive glass (BG) effectively decontaminates titanium (Ti) surface biofilms and the retained glass particles on the abraded surfaces impart potent antibacterial properties against various clinically significant pathogens. The objective of this study was to investigate the effect of BG APA and simulated body fluid (SBF) immersion of sandblasted and acid-etched (SA) Ti surfaces on osteoblast cell viability. Another goal was to study the antibacterial effect against Streptococcus mutans. Square-shaped 10 mm diameter Ti substrates (n = 136) were SA by grit blasting with aluminum oxide particles, then acid-etching in an HCl-H2SO4 mixture. The SA substrates (n = 68) were used as non-coated controls (NC-SA). The test group (n = 68) was further subjected to APA using experimental zinc-containing BG (Zn4) and then mineralized in SBF for 14 d (Zn4-CaP). Surface roughness, contact angle, and surface free energy (SFE) were calculated on test and control surfaces. In addition, the topography and chemistry of substrate surfaces were also characterized. Osteoblastic cell viability and focal adhesion were also evaluated and compared to glass slides as an additional control. The antibacterial effect of Zn4-CaP was also assessed against S. mutans. After immersion in SBF, a mineralized zinc-containing Ca-P coating was formed on the SA substrates. The Zn4-CaP coating resulted in a significantly lower Ra surface roughness value (2.565 μm; p < 0.001), higher wettability (13.35°; p < 0.001), and higher total SFE (71.13; p < 0.001) compared to 3.695 μm, 77.19° and 40.43 for the NC-SA, respectively. APA using Zn4 can produce a zinc-containing calcium phosphate coating that demonstrates osteoblast cell viability and focal adhesion comparable to that on NC-SA or glass slides. Nevertheless, the coating had no antibacterial effect against S. mutans.

Analysis of Polyurethane Foam Machining Parameter Influence: Current Status and Perspective

Nowadays, polyurethane (PU) foam has successfully replaced various engineering materials in many applications due to its many advantages in mechanical and thermal properties. In various applications, PU foam must be formed into various 3-dimensional models according to user requirements by utilizing CAM software and CNC milling machining to manufacture a product. Thus, the selection of cutting parameters in the milling machining process in terms of the nature and character of the material and cutting tools is essential and significantly influences the geometric structure and surface roughness of the PU foam products produced. Based on the review of this article, several machining parameters must be appropriately considered, including spindle rotation speed, depth of cut, cutting tool selection, and feed rate. Vibration will increase as the spindle rotation speed increases, which brings cutting tools but results in better surface quality. Continuous chip formation can be achieved by selecting the proper cut depth and producing low surface roughness values. Selecting suitable cutting tools and geometries that match the material characteristics can reduce the risk of material damage during the machining process, thereby reducing the surface roughness value. Finally, a low cutting rate will minimize surface roughness but increase the risk of cutting-edge wear.