Generation Of Lossy Mode Resonances Research Articles

Lossy mode resonance generation with perovskite-coated photonic crystal fiber for sensing applications

Two-dimensional polymer perovskite (CH3NH3PbI3) has very potential properties in sensing applications. Hence, for high sensitivity, a lossy mode resonance refractive index sensor based on perovskite coating is proposed. The sensor uses a photonic crystal fiber (PCF) with three air holes and a polished surface. Perovskite is deposited on the PCF plane to form the Kretschmann structure. We analyzed its sensing characteristics by using the finite element method. A significant advantage of the sensor is its strong tunability, allowing it to be used in various operating environments by controlling the thickness of the film. In addition, two sharp resonant peaks in the loss spectrum can realize double resonant peak sensing and increase measurement accuracy. Numerical results show that the maximum sensitivity of the two resonant peaks is 36400 nm/RIU and 15400 nm/RIU, respectively, and the corresponding refractive index range is 1.39–1.43. The results also show that small structural changes do not cause a change in performance, meaning that the sensor has a high fault tolerance rate. The high sensitivity response with adjustable detection range makes the proposed sensor distinct. It has a good application prospect in water quality monitoring and biomolecular detection.

Development of a Temperature-Controlled Optical Planar Waveguide Sensor with Lossy Mode Resonance for Refractive Index Measurement

The generation of lossy mode resonances (LMR) with a metallic oxide film deposited on an optical fiber has attracted the attention of many applications. However, an LMR-based optical fiber sensor is frangible, and therefore it does not allow control of the temperature and is not suited to mass production. This paper aims to develop a temperature-controlled lossy mode resonance (TC-LMR) sensor on an optical planar waveguide with an active temperature control function in which an ITO film is not only used as the LMR resonance but also to provide the heating function to achieve the benefits of compact size and active temperature control. A simple flat model about the heat transfer mechanism is proposed to determine the heating time constant for the applied voltages. The TC-LMR sensor is evaluated experimentally for refractive index measurement using a glycerol solution. The heating temperature functions relative to the controlled voltages for water and glycerol are obtained to verify the performance of the TC-LMR sensor. The TC-LMR sensor is a valuable sensing device that can be used in clinical testing and point of care for programming heating with precise temperature control.

Subtle Application of Electrical Field-Induced Lossy Mode Resonance to Enhance Performance of Optical Planar Waveguide Biosensor.

Many studies concern the generation of lossy mode resonances (LMRs) using metallic oxide thin films that are deposited on optical fiber. However, the LMR-based optical fiber sensors are frangible, do not allow easy surface modification, and are not suited to mass production. This study proposes an electrical field-induced LMR-based biosensor with an optical planar waveguide to replace surface modification and allow the mass production of protein biosensors and accelerate the speed of the analyte to decrease the detection time. Experimentally, the biosensor is evaluated using charged serum albumin molecules and characterized in terms of the LMR wavelength shift using an externally applied voltage for different durations. The externally applied voltage generates a significant electric field, which drives the non-neutralized biomolecules and increases the LMR wavelength shift. Our experimental results demonstrate that there are two different mechanisms of adsorption of serum albumin molecules for short-term and long-term observations. These are used to calculate the sensitivity of the biosensor. This electrical field-induced method is highly significant for the development and fabrication of LMR-based biosensors.

Generation of lossy mode resonances in a broadband range with multilayer coated coverslips optimized for humidity sensing

Coverslips deposited with a metallic oxide can be employed for generating lossy mode resonances by lateral incidence of light on the coverslip. Here it is demonstrated that with copper oxide the fading observed with other materials in the near infrared (NIR) wavelength range is avoided and LMRs can be obtained in a broadband range from 400 to 1700 nm, which permitted to observe the better performance in the NIR region compared to the visible region: the sensitivity to humidity is improved by more than a factor of two. However, copper oxide is not adequate for sensing humidity. The sensitivity of the device was optimized initially with a tin oxide coating and later with an additional layer of agarose, specifically adequate for the detection of humidity. The best performance was obtained with an agarose concentration 1% w/v, which permitted to observe a 10-fold sensitivity increase compared to the same device without agarose. This opens the path towards the development of environmental, chemical or biological sensors with an optimized sensitivity to a specific parameter to detect.

Effect of thermal annealing on sensing properties of optical fiber sensors coated with indium tin oxide nano-overlays

In this work we discuss an effect of thermal annealing on optical and electrical properties of indium tin oxide (ITO) thin films deposited on a short section of multimode polymer-clad silica (PCS) optical fiber core. ITO films were deposited using different configuration of high power impulse magnetron sputtering (HiPIMS) and radio frequency magnetron sputtering (RF MS) cathodes. Due to tuned ITO film thickness it was possible to observe for these structures a lossy-mode resonance (LMR) and trace changes in properties of the films. Electrical resistance of the ITO overlays was also measured. Both optical and electrical measurements were repeated after annealing at 200°C in a tube furnace and nitrogen atmosphere. The measurements have shown that thermal annealing changes optical response to external refractive index (RI) of the fiber sensor and also changes the ITO layer resistivity. As an effect of thermal annealing we observed a shift of the LMR towards longer wavelengths. In addition as a result of annealing, the resistivity of the ITO layer was reduced. Full Text: PDF ReferencesM. Sobaszek et al., "Optical monitoring of thin film electro-polymerization on surface of ITO-coated lossy-mode resonance sensor", Proc. SPIE, vol. 10323, pp. 103234W, 2017. CrossRef I. Del Villar et al., " Generation of lossy mode resonances by deposition of high-refractive-index coatings on uncladded multimode optical fibers", J. Opt., vol. 12, no. 9, pp. 95503, 2010. CrossRef M. Śmietana et al., "Simultaneous optical and electrochemical label-free biosensing with ITO-coated lossy-mode resonance sensor", Biosensors and Bioelectronics, vol. 154, pp. 112050, 2020. CrossRef P. Niedziałkowski et al., " Electrochemical performance of indium-tin-oxide-coated lossy-mode resonance optical fiber sensor", Sensors and Actuators B: Chemical, vol. 301, no. 12, pp. 1-10, 2019. CrossRef V. Stranak et al., "Effect of mid-frequency discharge assistance on dual-high power impulse magnetron sputtering", Surface & Coatings Technology, vol. 206, no. 11-12. pp. 2801-2809, 2012. CrossRef I. Del Villar et al., "Design rules for lossy mode resonance based sensors", Appl. Opt., vol. 51, no. 19, pp. 4298-4307, 2012. CrossRef W. F. Wu and B. S. Chiou, "Effect of annealing on electrical and optical properties of RF magnetron sputtered indium tin oxide films", Appl. Surf. Sci., vol. 68, no. 4, pp. 497-504, 1993. CrossRef M. Smietana et al., "Optical Monitoring of Electrochemical Processes With ITO-Based Lossy-Mode Resonance Optical Fiber Sensor Applied as an Electrode", J. Light. Technol., vol. 36, no. 4, pp. 954-960, 2018. CrossRef M. Śmietana et al., "Study on Combined Optical and Electrochemical Analysis Using Indium‐tin‐oxide‐coated Optical Fiber Sensor", Electroanalysis, vol. 31, no.2, pp. 398-404, 2019. CrossRef

Generation of lossy mode resonances with different nanocoatings deposited on coverslips.

The generation of lossy mode resonances (LMRs) with a setup based on lateral incidence of light in coverslips is a simple platform that can be used for sensing. Here the versatility of this platform is proved by studying the deposition of different coating materials. The devices were characterized with both SEM and AFM microscopy, as well as ellipsometry, which allowed obtaining the main parameters of the coatings (thickness, refractive index and extinction coefficient) and relating them with the different sensitivities to refractive index attained with each material. In this way it was possible to confirm and complete the basic rules observed with lossy mode resonance based optical fiber sensors towards the design of simpler and more compact applications in domains such as chemical sensors or biosensors.

Lossy Mode Resonance Generation on Sputtered Aluminum-Doped Zinc Oxide Thin Films Deposited on Multimode Optical Fiber Structures for Sensing Applications in the 1.55 µm Wavelength Range

In this work, we demonstrated lossy mode resonance (LMR) generation in optical fiber structures based on multimode fibers coated with aluminum-doped zinc oxide (AZO) films. AZO thin films were deposited by using radio frequency magnetron sputtering. In order to exhibit the usefulness of the LMR effect for sensing applications in optical fiber based systems, the deposition conditions of the AZO film coatings were set to obtain the second LMR order within the 1.55 µm wavelength range. An optical transmission configuration setup was used to investigate the LMR effect on fiber structures based on the use of no-core and cladding-removed multimode fibers coated with AZO films synthesized from metallic sputtering targets with different proportions of Zn:Al, 92:8% and 98:2%, at atomic concentrations. The optical and electrical/chemical features of the AZO films were characterized with UV–vis and XPS spectroscopy, respectively. The optical response of the proposed sensing configuration to refractive index (RI) variations was experimentally demonstrated. For the best approach, the sensitivity of wavelength displacement to RI variations on the liquid surrounding media was found to be 1214.7 nm/RIU.

Lossy Mode Resonance Generation by Graphene Oxide Coatings Onto Cladding-Removed Multimode Optical Fiber

In this paper, we have studied the suitability of graphene oxide-based thin films to be not only excellent sensitive coatings but also lossy mode resonance (LMR)-generating materials. Thin films of graphene oxide (GO) and polyethylenimine (PEI) fabricated by means of layer-by-layer assembly were selected in this paper. Two optical fiber devices with 8 and 20 bilayers of the LMR-generating coating were fabricated and characterized as refractometers. Both devices show no hysteresis and high sensitivity, improving previously reported values. This paper opens very promising and exciting possibilities in the field of optical fiber sensors based on LMR, strategically including specific recognition groups to the device surface to exploit this high sensitivity for monitoring a range of target analytes. The carboxylate functional groups at the edges of the GO sheets should provide excellent attachment sites for the required coupling chemistry to realize such devices.

Generation of Lossy Mode Resonances in Planar Waveguides Toward Development of Humidity Sensors

Lossy mode resonances (LMRs) are typically obtained with optical fibre. The Kretschmann configuration is an alternative but LMRs are generated with angles approaching grazing incidence. In this work, a new setup is explored, based on the lateral incidence of light on conventional planar waveguides such as glass slides or coverslips. Indium tin oxide was deposited onto both types of waveguides generating LMRs. The results of the simulations carried out agree well with the experimental results. As an example of the potential of this new and simple optical configuration, a humidity sensor with a sensitivity of 0.212 nm/% relative humidity (RH) in the range from 65% to 90% of RH was developed, which expedites the development of other types of sensors already explored with LMR-based optical fibre sensors.

Aluminum doped zinc oxide (AZO) coated optical fiber LMR refractometers—An experimental demonstration

This work presents the experimental demonstration of lossy mode resonance generation by means of aluminum doped zinc oxide thin-films. The use of such material may allow to optimize the performance of LMR-based sensors, obtaining good sensitivity at lower costs than other overlays, such as those including indium. The refractometric response of the fabricated devices is explored in different spectral regions. One refractometer working in the near infrared region was fabricated, obtaining a sensitivity of 2280 nm/RIU. A second refractometer working in the visible light spectrum was also fabricated. This second device allows to observe rough refractive index variations with the naked eye as a change of the color of the light propagating through the fiber, simplifying the setup needed for its use.

Femtomolar Detection by Nanocoated Fiber Label-Free Biosensors.

The advent of optical fiber-based biosensors combined with that of nanotechnologies has provided an opportunity for developing in situ, portable, lightweight, versatile, and high-performance optical sensing platforms. We report on the generation of lossy mode resonances by the deposition of nanometer-thick metal oxide films on optical fibers, which makes it possible to measure precisely and accurately the changes in optical properties of the fiber-surrounding medium with very high sensitivity compared to other technology platforms, such as long period gratings or surface plasmon resonances, the gold standard in label-free and real-time biomolecular interaction analysis. This property, combined with the application of specialty structures such as D-shaped fibers, permits enhancing the light-matter interaction. SEM and TEM imaging together with X-EDS tool have been utilized to characterize the two films used, i.e., indium tin oxide and tin dioxide. Moreover, the experimental transmission spectra obtained after the deposition of the nanocoatings have been numerically corroborated by means of wave propagation methods. With the use of a conventional wavelength interrogation system and ad hoc developed microfluidics, the shift of the lossy mode resonance can be reliably recorded in response to very low analyte concentrations. Repeated experiments confirm a big leap in performance thanks to the capability to detect femtomolar concentrations in human serum, improving the detection limit by 3 orders of magnitude when compared with other fiber-based configurations. The biosensor has been regenerated several times by injecting sodium dodecyl sulfate, which proves the capability of sensor to be reused.

Indium tin oxide refractometer in the visible and near infrared via lossy mode and surface plasmon resonances with Kretschmann configuration

An indium tin oxide (ITO) refractometer based on the generation of lossy mode resonances (LMRs) and surface plasmon resonances (SPRs) is presented. Both LMRs and SPRs are excited, in a single setup, under grazing angle incidence with Kretschmann configuration in an ITO thin-film deposited on a glass slide. The sensing capabilities of the device are demonstrated using several solutions of glycerin and water with refractive indices ranging from 1.33 to 1.47. LMRs are excited in the visible range, from 617 nm to 682 nm under TE polarization and from 533 nm to 637 nm under TM polarization, with a maximum sensitivity of 700 nm/RIU and 1200 nm/RIU, respectively. For the SPRs, a sensing range between 1375 nm and 2494 nm with a maximum sensitivity of 8300 nm/RIU is measured under TM polarization. Experimental results are supported with numerical simulations based on a modification of the plane-wave method for a one-dimensional multilayer waveguide.

Spectral width reduction in lossy mode resonance-based sensors by means of tapered optical fibre structures

This contribution pursues the goal of achieving an optical fibre-based platform to detect anti-gliadin antibodies (AGAs), in order to early diagnose celiac disease. To this purpose, the generation of lossy mode resonances (LMRs) in several evanescent field optical structures was studied both theoretically and experimentally. LMRs were obtained by adsorbing a polymeric thin-film onto the optical structures using the layer-by-layer assembly technique. The LMR shape depends on the geometry of the optical structure and its attenuation was controlled just by tuning the length of the device. The best performance was obtained with tapered single-mode optical fibres, which provided more than a 50% reduction in the spectral width of the LMR by using a shorter device. This improvement was successfully applied to detect anti-gliadin antibodies (AGAs) in 5ppm concentration, what can be used to diagnose celiac disease, and shows the potential of this technology to address biosensing applications.

Experimental demonstration of lossy mode resonance generation for transverse-magnetic and transverse-electric polarizations

This Letter, presents the fabrication of lossy mode resonance (LMR) devices based on titanium dioxide (TiO2)/ poly(sodium 4-styrenesulfonate) (PSS) coatings deposited on side-polished D-shaped optical fibers. TiO2 thin films have been obtained by means of the layer-by-layer (LbL) self-assembly technique. LbL enables us to produce smooth and homogeneous coatings on the polished side of the fiber. This permits us to couple light from the waveguide to the TiO2-coating/external medium region at specific wavelength ranges. The generation of LMRs depends on the coating thickness, so that thicker coatings can produce more resonances. LMRs are sensitive to the external medium refractive index, which allows its utilization as refractometers. The characteristic D-shaped architecture of the devices employed in this Letter enables us to distinguish TE and TM polarizations, which had not been possible before with regular optical fibers due to their cylindrical symmetry. The results presented here show for the first time the experimental demonstration of the generation of LMRs produced by both TM and TE polarizations. More specifically, for these TiO2/PSS thin films, the TM and TM modes of the LMRs show a wavelength shift of 226 nm for the first-order LMR and 56 nm for the second-order LMR.

Generation of Lossy Mode Resonances With Absorbing Thin-Films

The generation of lossy mode resonances with absorbing thin-films is analyzed with electromagnetic theory. The main differences with surface plasmon resonances are presented and some rules are given towards an optimum design of sensing devices based on absorbing thin-film coated silica substrates. The material selected for the absorbing thin-film is ITO, which is adequate for supporting both surface plasmon resonances and lossy mode resonances.

Generation of lossy mode resonances by deposition of high-refractive-index coatings onuncladded multimode optical fibers

A comparative study of lossy mode resonances generated by depositing twodifferent materials is presented. The two materials selected are indium tinoxide (ITO) and indium oxide. The two materials present different dielectricdispersion, which leads to the generation of single-peak lossy mode resonanceswith the ITO coated optical fibers and dual-peak lossy mode resonances with theIn2O3 coated optical fibers. The obvious advantage of a dual-peak based measurement in thesensors field is enhanced by a sensitivity increase observed in sensors based onIn2O3 if compared with those based on ITO. These characteristics are analyzed both theoreticallyand experimentally.

Lossy Mode Resonance Generation With Indium-Tin-Oxide-Coated Optical Fibers for Sensing Applications

<para xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink"> Surface plasmon resonances and lossy mode resonances (LMRs) can be generated with indium tin oxide (ITO) coated optical fibers. Both phenomena are analyzed and compared. LMRs present important advantages: they do not require a specific polarization of light, it is possible to generate multiple attenuation bands in the transmission spectrum, and the sensitivity of the device to external parameters can be tuned. The key parameter is the thickness of the ITO coating. The study is supported with both theoretical and experimental results. The main purposes are sensing and generation of multiple-wavelength filters. </para>