The article presents a unique method of modifying the surface layer properties of low‐alloy steels. This method consists of the simultaneous saturation of the surface layer with aluminum and carbon. A hybrid heat treatment process is used, which integrates diffusion metallization with low‐pressure carburizing (LPC). An aluminum coating is applied to the surface of the steel by physical vapour deposition or slurry method to saturate the surface layer with aluminum. The steel is then annealed to create a diffusion layer and subjected to LPC. Gas quenching in nitrogen and low‐temperature tempering are performed after carburization. This surface treatment tenfold reduces the amount of retained austenite in the carburized layer. This is particularly critical for carburized steels that include austenite‐stabilizing elements, such as nickel and manganese. This causes an increase in surface hardness. It also changes the state of residual stress compared to ordinary LPC to one that is more favorable from the point of view of operation—compressive stresses are generated in the technological surface layer.