The objective of this work is to create and analyze composites made of kenaf fibers and epoxy polymer, which are strengthened by the addition of Acacia concinna pod (ACP) powder. These composites are intended for use in electrical insulation applications. The study investigated the impact of alkali treatment using a 6% NaOH solution on kenaf fiber. The effects were analyzed in relation to the dielectric and dynamic mechanical properties, while also considering the addition of different quantities of ACP powder (0%, 4%, and 8%). The composites were produced using the hand layup method, and the dielectric constant, dissipation factor, storage modulus, loss modulus, and damping factor were assessed. The study demonstrated that NaOH-treated kenaf fiber composites displayed considerably lower dielectric constant values than untreated composites, due to increased fiber crystallinity and decreased moisture absorption. Dynamic Mechanical Analysis (DMA) found that untreated composites had greater storage modulus and glass transition temperature (Tg) due to reduced segmental motion at the fiber-matrix interface. SEM research indicated better fiber-matrix bonding in treated composites, with decreased voids and robust interlocking, notably in those containing 4% Acacia concinna (ACP) filler. These findings show that NaOH treatment substantially enhances the performance of hybrid composites for electrical insulating applications.
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