• The iQC Al 13 Cr 2 phase single crystal synthesized by Al/self-flux method. • XRD confirms needle shaped crystal which adopts monoclinic structure. • Electrical resistivity at low temperature exhibits fermi liquid behavior. • The magnetic property needs more study to declare its intrinsic to iQC Al 13 Cr 2 phase. We report the synthesis of icosaherdral quasicrystal (iQC) Al 13 Cr 2 phase single crystal via Al self-flux method. Powder X-ray diffraction study shows that it crystallizes in a monoclinic structure (space group C 2/ m ) with a unit cell of a = 25.3420 (5) Å, b = 7.6134 (5) Å, c = 11.0559 (5) Å, and β = 128.9°. Electrical resistivity of iQC Al 13 Cr 2 phase single crystal decreases with decreasing temperature, showing a metallic behavior. At low temperatures, it is reasonably fitted with T 2 dependence, implying the Fermi liquid behavior. The T 2 -coefficient A of the resistivity is 0.00182 μΩ cm/K 2 , leading to the estimated Sommerfeld coefficient γ of 13.49 mJ/molK 2 from Kadowaki-Woods relation. DC calorimetry measurements show that the specific heat divided by temperature ( C/T ) at T = 0 K is approximately 16.26 mJ/molK 2 , which is comparable with that estimated from resistivity data. We note that, unlike Al 14 Cr 2 compound with an AFM order, magnetization data of Al 13 Cr 2 phase single crystal showed is almost independent of temperature over the wide range of temperature, indicating that moments from Cr ions are screened.