Initial Stage Of Deformation Research Articles

Large deformation of variable thickness woven composite preforms considering interlayer difference. Application: Forming simulation of a blade preform

The main objective of this work was to investigate the interlayer difference of 3D orthogonal woven fabrics (3DOWFs) during deformation. Tensile, shear, and compression tests were performed on two types of 3DOWFs with different layer numbers. To determine the variations in the deformation behavior within the fabric, a layer decomposition method was developed. This process involved the decomposition of the fabric into two layers, the inner layer and the outer layer, depending on the difference in structural features of the yarn. Then the deformation characteristics of the inner layer and outer layer were derived based on their series or parallel relationship in the load path. The results indicate that there are noticeable variations in the deformation characteristics among the layers of 3DOWF, which are associated with the interwoven structure of the yarns. In particular, in compression deformation, the difference in yarn structure causes the initial stage (Compressive strain <0.2) of fabric compression deformation to be mostly attributed to the compression of the outer layer. Subsequently, the deformations of the inner layer and outer layer gradually tend to balance. Based on a simple anisotropic hyperelasticity model, the interlayer differences were considered in the blade preform simulation. The simulation result shows a good agreement with the preforming results. The results show that the interlayer difference has a significant impact on the deformation of the blade preform, particularly in the posterior edge region, which is not strongly compressed.

Study on the extension mechanism of fissures in expansive soil based on fracture mechanics test method

Expansive soil, characterized by widespread fissures, is a special type of soil prone to localized fissure propagation, leading to failure and instability, often resulting in landslides. Numerous studies have applied fracture mechanics theory to analyze soil failure along fissures, but no standardized testing method has been established. This paper reviews existing soil fracture toughness testing methods, designs an integrated system combining digital image correlation(DIC) technique and electrical resistance testing, and employs the Cracked Chevron-Notched Brazilian Disc (CCNBD) method to assess the fracture toughness of expansive soil. The deformation and internal damage accumulation processes of the specimens were monitored. The KΙc and KΙΙc of expansive soil were tested at moisture contents of 15 %, 20 %, and 25 % using specimens with three different crack length ratios (a/R). The role of water was explored by injecting water into the fissures. The results showed that KΙc of expansive soil ranged from 10 to 36 kPa·m0.5, with a linear negative correlation to moisture content and a proportional relationship to tensile strength, having a proportionality coefficient of 0.331. The KΙΙc ranged from 20 to 70 kPa·m0.5,and it is greater than KΙc under the same conditions. Based on the load, internal damage, strain, and fissure area during the tests, the failure process of expansive soil along fissures was divided into four stages: initial deformation stage(I), quasi-elastic deformation stage(II), fissure extension stage(III), and failure stage(IV). Water injection into the fissures reduced the soil's fracture toughness, with a more significant reduction as a/R increased and the failure showed progressive behavior. The CCNBD method, combined with DIC technique and electrical resistance testing, effectively measures the fracture toughness of soil, aiding in understanding the failure mechanism along fissures and providing a basis for preventing and controlling landslides and other hazards in expansive soils.

Effect of Er on the Hot Deformation Behavior of the Crossover Al3Zn3Mg3Cu0.2Zr Alloy

The effect of an erbium alloying on the hot deformation behavior of the crossover Al3Zn3Mg3Cu0.2Zr alloy was investigated in detail. First of all, Er increases the solidus temperature of the alloy. This allows hot deformation at a higher temperature. The precipitates resulting from the Er alloying of the Al3Zn3Mg3Cu0.2Zr alloy were analyzed using transmission electron microscopy. Erbium addition to the alloy produces the formation of more stable and fine L12-(Al3(Zr, Er)) precipitates with a size of 20–60 nm. True stress tends to increase with a decline in the temperature and an increase in the deformation rate. The addition of Er leads to decreases in true stress at the strain rates of 0.01–1 s−1 due to particle-stimulated nucleation softening mechanisms. The effective activation energy of the alloy with the Er addition has a lower value, enabling an easier hot deformation process in the alloy with an elevated volume fraction of the intermetallic particles. The addition of Er increases the strain rate sensitivity, which makes the failure during deformation less probable. The investigated alloys have a significant difference in the dependence of the activation volume on the temperature. The flow instability criterion allows better deformability of Er-doped alloys and enables the alloys to be formed more easily. The evenly distributed particles prevent the formation of shear bands with elevated storage energy and decrease the probability of crack initiation during the initial stages of hot deformation when only one softening mechanism (dynamic recovery) is working. The microstructure analysis proves that dynamic recovery is the main softening mechanism.

Microstructure evolution in laser powder bed fusion melted 2205 duplex stainless steel using in-situ EBSD during uniaxial tensile testing

Compared to duplex stainless steels (DSSs) prepared by traditional methods, specimens produced through laser powder bed fusion (LPBF) exhibit excellent yield strength but lower elongation. To improve elongation, understanding microstructure evolution during uniaxial tensile testing is crucial. This study investigates the slip behavior, grain boundary evolution, and phase transformation of LPBF 2205 duplex stainless steel during tensile deformation using in-situ electron backscatter diffraction (EBSD). Results show the formation of slip bands, which increase in number as loading stress rises. The primary slip systems activated are {110}<111> in ferrite and {111}<110> in austenite. In the ferrite phase, slip dislocations accumulate and generate low-angle grain boundaries (LAGBs), which evolve into high-angle grain boundaries (HAGBs), refining the grain structure. Numerous Σ3 annealing twins form in the austenite phase, but detwinning and twinning reduce Σ3 content as deformation processes. Ferrite and austenite exhibit good stability during the initial stages of tensile deformation. However, some austenite transforms into martensite through the transformation-induced plasticity (TRIP) effect at the final stages of deformation, which helps relieve stress concentration and delays material fracture. This study provides valuable insights for optimizing microstructure to improve the mechanical properties of LPBF materials.

Analysis of spectra of external impacts, reactions to them and limit states under the non-stationary modes of loading

It is noted that under real operating conditions of technical systems the so-called non-stationary loading in which external loadings increase or decrease arbitrarily is realized most often. At the same time final ratios between strains and stresses are of practical interest to engineering calculations. It is shown that for simple cyclic loadings the state equations in final ratios which are based on the theory of small elastic-plastic strains can be used. In this case the existence of the uniform generalized deformation diagram assuming a final relation between the corresponding components of stresses and strains both for initial and cyclic stages of deformation is essential for the analysis of considered conditions of a non-stationary cyclic loading. The analysis of conditions of achieving limit states at all stages of the life cycle the criteria base and the system of the computation equations become more complicated and more saturated by the factors taken into account and among them first external and internal impacts of natural, technogenic, anthropogenous origin, load from these impacts, and the reactions of installations to such impacts and loads as well. At the same time a set of criteria defining a limit state is presented in the form of a functional dependence characterizing a set of force and deformation parameters of the state of technical system on the one hand, and, on the other hand, a complex of criterion characteristics of constructional materials taking into account their change during operation. The most important step of determining conditions for achievement of the limit state causing fracture is establishing the critical parts that determine risks of emergency and catastrophic situations in which processes of local and main fractures are initiated. In this case transition of the operated installation from design area to the area of initiation of refusals, accidents and disasters occurs when the parameters of damage, defectiveness and risk reach their critical values.

Pyramidal dislocation driven martensitic nucleation: A step toward consilience of deformation scenario in fcc materials (II)

Dislocation glides and their interactions with other defects are central to our understanding of deformation mechanism enhancing plasticity and damage tolerance. Martensitic transformation (MT) is a fascinating phenomenon overcoming strength-elongation trade-off and thus tailoring structure-property architecture. However, dislocation plasticity of Fe-based hexagonal close-packed (hcp) martensite is still challenging due to its metastability, further complicated by controversies surrounding pyramidal dislocation even in pure hcp metals. To resolve the uncertainties, we address the pyramidal-dislocation-driven plasticity in Fe-based hcp martensite by employing in-situ transmission electron microscopy (TEM) and high-resolution (HR) annular bright field (ABF) imaging together with dislocation-contrast analyses. We show that the activation and dissociation of pyramidal dislocation govern the initial stage of plastic deformation, while subsequent cross-slip by the cooperative motion of dissociated pyramidal dislocations plays a key role in nucleation of new hcp martensite. By incorporating current dislocation model into previous models coupled with stacking-fault-energy concept, we propose a synthesized deformation scenario that offers a comprehensive perspective on plasticity and transformability.

Void-induced mechanisms in tensile behavior of nickel-based single crystal superalloys

Void defects significantly impact the tensile properties of nickel-based single crystal superalloys. In this work, the dynamic response of void-included nickel-based single crystal superalloys under tensile loading was studied using molecular dynamics method. The effects of porosity and void size on the tensile behavior and the evolution of internal defects were explored from a microscopic perspective. The results indicate that the presence of voids promotes the development of internal dislocation defects and atomic phase transitions, especially in the initial stage of plastic deformation. The tensile strength decreases with increasing porosity. Plastic deformation and atomic phase transitions typically initiate between voids and continue until complete fracture, with shear strains and dislocation defects continuously concentrating around the voids. Notably, some HCP defect atoms distant from voids revert to FCC phase atoms during the tensile process, leading to a decrease in dislocation density. Additionally, the mode of fracture in the porous model is shear fracture, with shear strain and dislocation defects remaining at the fracture surface after complete fracture. The effects of void size on the tensile strength are relatively small. As the void size decreases, the shear strain bands in the models become more regular and the dislocation density decreases. However, the impact of small-sized voids on the material becomes increasingly evident with further stretching.

Achieving excellent uniform tensile ductility and strength in dislocation-cell-structured high-entropy alloys

Body-centered-cubic (BCC) high-entropy alloys (HEAs) encounter significant challenges in obtaining a high uniform tensile ductility (UTD). A dense dislocation-cell (DC) structure is produced in a heterogeneously grained HEA under tensile deformation, resulting from the anchored dislocation motion by grain interior elemental segregation. This fluctuation in elemental concentration is facilitated by thermomechanical processing. The activation of multiple-slip mechanisms, prompted by strain incompatibility among grains of varying sizes, significantly propels this process forward. This novel DC structure simultaneously increased the UTD (by 349.1 %) and yield strength (σ0.2, by 29.0 %) for a stable BCC HEA. Specifically, the single-phase alloy achieved a record-high UTD of 7.5 % and an σ0.2 of > 1,200 MPa, outperforming the counterparts of all the single-phase BCC HEAs. We employed a combination of transmission electron microscopy, in-situ scanning electron microscopy tensile testing coupled with an electron backscatter diffraction technology to investigate underlying strengthening mechanisms and identified that the serious stress concentration as a result of prevalent planar slip caused premature failure and localized strain of common BCC HEAs. At the initial stage of deformation, the DC structure promoted the activation of multiple slip systems and facilitated the extension of a plastic flow across the sample volume, effectively weakening stress concentration and premature failure. The extended plasticity zone and intensified dislocation interactions contributed to the increased UTD and σ0.2. These findings offer valuable inspiration for tailoring alloy properties via microstructure strategies and promoting their adoption in advanced manufacturing.

Achieving high ductility in Fe45Mn35Co10Cr10 metastable high entropy alloy by constructing chemical boundary with stacking fault energy heterogeneity

Additively-manufactured metastable high entropy alloys are emerging as promising alternatives for energy absorption in protective equipment due to their exceptional ductility. In this study, an elongation of over 50 % was achieved in a directed energy deposition fabricated Fe45Mn35Co10Cr10 metastable high entropy alloys (MHEAs). The inherent high cooling rate and repeated heat treatment in the directed energy deposition process were harnessed to deliberately induce an uneven distribution of Mn elements, forming a cellular structure with chemical boundary. The unique heterogeneity stacking fault energy results in a synergistic interplay of multiple deformation mechanisms such as, dislocation slip, transformation-induced plasticity (TRIP) and twinning-induced plasticity (TWIP). In the initial stage of deformation, dislocation slip and TRIP contribute to the main plasticity. Stacking faults/martensite are confined within the cellular structure with low stacking fault energy (SFE). As strain increases, TWIP and TRIP are activated in the high SFE regions. Twins and martensite across the cell wall were observed. As strains exceed 40 %, primary martensite variant and twinning with a particular intersection angle take place to further enhance the deformation ability. The chemical boundary with stacking fault energy heterogeneity not only simultaneously activates both TRIP and TWIP, but also maintains the martensite and twins at the nanoscale.

Experimental study on the effects of complex discrete joints on the mechanical behavior of rock‐like material

AbstractThe strength and failure of rock masses are ambiguous due to their complex structure. Investigating the strength and failure of jointed rock mass remains a persistent concern in mining engineering. This study aims to investigate the effects of joint dip angles of complex discrete joints on the mechanical properties and fracture evolution of rock‐like material. Rock‐like specimens with complex joints were prepared using 3D printing technology and then tested under uniaxial compression loading. The experimental results reveal the following findings: (1) The anisotropy of rock‐like material with complex joints is lower compared to the rock‐like material with simple joints. (2) The ratio of long‐term strength to uniaxial compressive strength of rock‐like material remains consistent despite changes in the dip angle of the joints. (3) Differing from intact rocks, AE events of the rock‐like material with complex joints are obvious in the initial loading stage and elastic deformation stage. (4) When the dip angle of the joint sets is 0 and 90°, fractures progressively propagate, and the failure mode of the rock‐like material demonstrates tensile failure along the pre‐existing joints. Conversely, when the dip angle of the joint sets is 45° and 135°, fractures are simultaneously initiated at various locations within the rock‐like specimen, resulting in a failure mode of rotational failure by the newly generated block.

Role of grain size in the evolution of stress-induced martensite and the tensile deformation behavior of Ti-7333 alloy

The evolution of martensite and the tensile deformation behavior of Ti-7333 alloy with different β grain size was studied. It is found that the β grain size (45–260 μm) significantly affects the triggering stress of stress-induced α″ martensite (SIMα″), and then affects the distribution and morphology of α″ martensite. At the initial stage of deformation, the larger β grain can inhibit the stress-induced secondary α″ martensitic transformation and the formation of α″ twinning. While under the same strain, the stress-induced martensite and martensite twinning can be activated simultaneously in the alloy with the smaller β grain, including {111}α″ type Ⅰ twinning, {130}<310>α″ compound twinning, <211>α″ type Ⅱ twinning, {021}<512>α″ type Ⅱ twinning, which can effectively accommodate localized strains and improve the work hardening rate of Ti-7333 alloy. When the β grain size varies in the range of 45–84 μm, there is a higher work hardening plateau in the deformation stage II of Ti-7333 alloy. The yield strength and β grain size are in accordance with the Hall-Petch relation. As the grain size increases to 128 even to 260 μm, the work hardening rate continues to decrease and the yield strength inversely increases. It is demonstrated that the triggering stress for SIMα″ exhibits U-shaped fluctuations as β grain size increases, and the inflection point of Ti-7333 alloy is between 84 μm and 260 μm.

Microstructures and mechanical properties of additively manufactured Fe–21Mn-0.6C TWIP steel using laser powder bed fusion

Twinning induced plasticity (TWIP) high manganese steel exhibits high ultimate tensile strength (UTS) and ductility, but its low yield strength restricts its applications. This research presents a Fe–21Mn-0.6C TWIP steel with enhanced mechanical properties additively manufactured using laser powder bed fusion (LPBF). The average grain size of the LPBF-fabricated Fe–21Mn-0.6C was 17.1 μm in the vertical direction, which was a quarter of that of a wrought one. The tensile yield strength was 657 MPa and the UTS was 1089 MPa with an elongation of 47.9% for the vertical direction. Compared to the wrought Fe–21Mn-0.6C, the yield strength increased by 110%. The high strength of LPBF-fabricated Fe–21Mn-0.6C is primarily attributed to solution, grain boundary and dislocation strengthening. Serrations were observed in the stress-strain curves at the initial stage of deformation, showing large stress drops. In the annealed sample, serrations appeared at a later stage of deformation with little stress drops. This difference in serration phenomenon is attributed to the varying dislocation density in the two samples.

The strength contribution via heterostructure in a Mg-Gd-Zn-Mn alloy

Deformation by extrusion is an effective means to enhance the performance of magnesium alloys. However, the resulting microstructure heterogeneity always lead to poor plasticity. Therefore, it is crucial to explicit the impact of heterogeneous structure on the deformation mechanism of the alloys. In this work, the microstructures evolution, mechanical properties, and fracture mechanism of Mg-xGd-1Zn-0.5Mn (x = 0, 2, 4, and 6) alloys were investigated. The elongation reached its maximum (40%) when the Gd content was 2%, which was attributed to the formation of the RE-texture and grain refinement. As the Gd content was further increased, the alloy developed a heterostructure consisting of both undynamic recrystallization (UDRX) grains and dynamic recrystallization grains (DRX). The exist of the heterostructures resulted in an increased strength which was attributed to the influences of texture strengthening derived from UDRX grains, the lamellar LPSO fiber strengthening and fine grain strengthening of DRX grains. At the initial stage of deformation in the heterostructure, the basal slip of DRX grains play a dominant role, while the UDRX grains strengthens the alloy effectively. The lamellar LPSO precipitated in the UDRX grains suppressed twinning effectively. As the concentrated stresses were enough to break through the barrier for twining of LPSO, numerous twins nucleated in the deformed grain thus resulting in the nucleation of cracks. During the process of tensile deformation, twins experienced greater basal slip resolved shear stress than that of the parent grains, resulting in significant basal slip activated due to twin. Consequently, there was a high stress concentration at the twin boundaries, leading to the nucleation of cracks. The varied deformation amount also resulted in the crack initiating at the interface of DRX grain and UDRX grain. This investigation provides valuable insights into the influence of a heterostructure on the deformation mechanism of Mg-Gd-Zn-Mn alloys.

Enhanced yield stress and reduced elastic modulus of metastable β Ti–Nb alloys deformed by equal channel angular pressing attributed to the Synergistic effect of deformation mechanisms

This work aims to obtain Ti–Nb alloys with a high yield stress, good plasticity, and low elastic modulus. To this end, metastable β Ti–Nb alloys were subjected to multipass equal channel angular pressing (ECAP) deformation at room temperature, and a thorough investigation of their microstructure evolution, deformation mechanisms, and strengthening/toughening mechanisms was conducted through X-ray diffraction, transmission electron microscopy, electron backscatter diffraction, and tensile tests. In the initial deformation stages, multiple deformation mechanisms are observed, including dislocation slip, {332} <113> twinning, stress-induced martensite (SIM) α″-phase, {112} <111> twinning, and stress-induced ω-phase. However, as the strain accumulates, the ω-phase disappears, the volume fraction of the SIM α″-phase gradually decreases, and the dominant deformation mechanism changes to dislocation slip and {332} <113> twinning. The ECAP deformation results in a complex-network microstructure and the precipitation of the nanoscale SIM α″-phase, which leads to the twinning-induced plasticity (TWIP) and transformation-induced plasticity (TRIP) effects. As a consequence, the Ti–Nb alloy simultaneously exhibits a high yield stress and a good plasticity. Furthermore, the high-density dislocations and interfaces generated by the ECAP deformation reduce the stability of the β-phase, and the introduced nanopores cause a decrease in density, resulting in a decrease in the elastic modulus of the alloy.

Research on the geological process of river action on the toppling deformation of rocky bank slopes in V-shaped gorge reservoirs

The toppling deformation in bank slope of V-shaped Gorge reservoirs in Southwest China is very common. After the impoundment of the reservoir, geological disasters such as collapse and landslide may occur in toppling bank slope, which poses a threat to the normal operation of hydropower projects and personnel safety. Therefore, it is of great engineering significance to study its genetic mechanism and development law. The trenching of river valley is one of the main factors of bank slope toppling deformation. In the process of river action, the free face is formed on the slope, and the rock mass is unloaded to the free face, resulting in toppling. Taking the bank slope of a reservoir in the V-shaped Gorge area on the edge of the Qinghai Tibet Plateau in Southwest China as an example, this paper studies the relationship between river action and the development of toppling. According to the seven terraces formed on both banks of the river, the trenching of the river valley is divided into seven stages. The toppling development characteristics of each stage are analyzed by discrete element method. According to the development characteristics of toppling deformation category, the toppling deformation is divided into five stages, they are initial toppling deformation stage, toppling development stage, intensified toppling deformation stage, temporary stability stage and failure stage. The research results can help to determine the development type and stage of bank slope toppling deformation in V-shaped Gorge area, so as to predict its further development deformation characteristics.

Correlation between the microstructure and deformation behavior of a PM fine-grained duplex steel

A fine-grained duplex steel with a composition of Fe–5Mn–2Al-0.6C (wt.%) was fabricated using a powder metallurgy (PM) technology of thermomechanical consolidation by hot extrusion of powder compact. The microstructure consisted of α′-martensite, residual austenite (RA), and a small amount of Al2O3 particles. Subsequent heat treatment was performed to adjust the microstructure and mechanical properties. This study focuses on the pre-and post-heat treatment microstructure of the material, elucidates the reasons for its formation, and explains how microstructural changes influence tensile deformation behavior. The results show that the heat treatment caused the precipitation of nanoscale carbide within the martensite, which significantly increased the yield strength from 792 MPa to 1078 MPa. While heat treatment altered the size and distribution of RA regions in the microstructure, the amount of RA transformed during deformation remained proportional to the flow stress in both materials, indicating that the flow stress dictates the amount of phase transformation of ultrafine grained RA. Therefore, in the heat-treated material with a higher yield strength, a larger amount of RA transformed during the initial stage of plastic deformation, leaving less RA to sustain a work-hardening rate in subsequent deformation, resulting in a decrease in ductility from 5.5 % to 3.6 % and fracture stress from 1674 to 1453 MPa. In addition, the in-situ formed Al2O3 particles facilitated grain refinement of the extruded rod, but had less effect on the microstructure and properties of the heat-treated sample. This study serves as a valuable reference for comprehending the influence of microstructural changes in PM manganese steel on tensile deformation behavior.

Hot deformation behavior of a layered heterogeneous microstructure TiAl alloy prepared by selective electron beam melting

TiAl-based alloys are known for their exceptional high-temperature properties but suffer from low hot workability. The emergence of additive manufacturing (AM) technology significantly decreases the workability requirement, while the microstructure heterogeneities in AMed TiAl are troublesome. This paper explores the hot deformation behavior and microstructure evolution of a layered heterogeneous microstructure TiAl alloy prepared by selective electron beam melting. The Arrhenius constitutive model with strain compensation was established, and hot processing maps were constructed. The microstructure showed that at the initial stage of deformation, a large number of dislocation slips occur preferentially in the soft coarse-grained layers. With the increase of strain, dislocation accumulation in heterogeneous interfaces, and dynamic recrystallization (DRX) occurs. Eventually, the coarse-grained region is constantly occupied by fine DRX grains. A high density of deformation twins at high strain rates further promotes the formation of tiny DRX grains. When the hot compression temperature reaches 1200 °C, the initial alternative fine-grained and coarse-grained hetero-structure transforms into duplex (DP) and near-lamellar (NL) microstructure, and microstructure heterogeneity is eliminated. The results enhance understanding of the hot deformation behavior of heterogeneous microstructure TiAl alloys.

The failure evolution of hydraulic asphalt concrete under different tensile fatigue loading

The fracture and damage evolution patterns of hydraulic asphalt concrete (HAC) under cyclic tensile loading determine the performance of asphalt concrete impermeable structures in embankment dams under seismic loading. Therefore, in this study, the whole fatigue tensile damage process of HAC under different loading conditions was studied with the help of acoustic emission (AE) technique. The results indicated that the fatigue behaviors of the HAC and AE signals follow the same evolutionary pattern, experiencing the initial deformation stage, the stability stage, the acceleration stage, and the failure stage. The b value, obtained from the least square fit between AE event number and magnitude, decreases to its lowest point upon specimen failure, and this decrease corresponds to a sudden increase in the peak frequency of the AE. The parametric analysis of relative amplitude-average frequency values classified for different cracking modes revealed that the tensile cracking dominates during the fatigue damage process, while the proportion of shear cracking events increases during the failure stage. Moreover, the peak value of the proportion of shear cracking events appears within the range near the point of failure, making it a useful indicator for providing critical warnings of HAC fatigue damage.

Tensile and High Cycle Fatigue Performance at Room and Elevated Temperatures of Laser Powder Bed Fusion Manufactured Hastelloy X.

The application potential of additive manufacturing nickel-based superalloys in aeroengines and gas turbines is extensive, and evaluating their mechanical properties is crucial for promoting the engineering application in load-bearing components. In this study, Hastelloy X alloy was prepared using the laser powder bed fusion process combined with solution heat treatment. The tensile and high cycle fatigue properties were experimentally investigated at room temperature as well as two typical elevated temperatures, 650 °C and 815 °C. It was found that, during elevated-temperature tensile deformation, the alloy exhibits significant serrated flow behavior, primarily observed during the initial stage of plastic deformation at 650 °C but occurring throughout the entire plastic deformation process at 815 °C. Notably, when deformation is small, sawtooth fluctuations are significantly higher at 815 °C compared to 650 °C. Irregular subsurface lack of fusion defects serve as primary sources for fatigue crack initiation in this alloy including both single-source and multi-source initiation mechanisms; moreover, oxidation on fracture surfaces is more prone to occur at elevated temperatures, particularly at 815 °C.

Plastic deformation of dry fine-grained olivine aggregates under high pressures

Abstract This study investigates the effect of pressure on diffusion creep of dry San Carlos and synthetic (prepared by sol-gel method) olivine. We prepared dry (water content &amp;lt; 9 ppm wt) fine-grained (&amp;lt; 1 μm grain-size) olivine and deformed the samples (both San Carlos and solgel olivine in the same assembly) in the same sample assembly under high-pressure (P = 2.9–8.8 GPa) and modest temperatures (T = 980–1250 K) at a fixed strain-rate. Evolution of strength was studied using the radial X-ray diffraction from various diffraction planes. We found that San Carlos and sol-gel olivine show similar rheological behaviour (when normalized to the same grain-size). Stress estimated by the radial X-ray diffraction increases with time and initially shows similar values for all diffraction planes. In many cases, stress values start to depend on the diffraction planes in the later stage and time dependence becomes minor. The micro-structural observations show that grain-size increases during an experiment. The results are interpreted using a theory of radial X-ray diffraction and the theoretical models of diffusion and dislocation creep. We conclude that the initial stage of deformation is by diffusion creep, but deformation in the later stage is by dislocation creep. For dislocation creep, our results are in reasonable agreement with previous low temperature dislocation creep results after a correction of temperature effect. For diffusion creep, we obtain an activation volume of 7.0 ± 2.4 cm3/mol that is substantially smaller than the values reported on dislocation creep but agrees well with the results on grain-growth. By comparing the present results on dry olivine with the previous results on wet (water-saturated) olivine, we found that water enhances diffusion creep but only modestly in comparison to dislocation creep. The difference in the pressure and water content dependence between diffusion and dislocation creep has an important influence on the dominant deformation mechanisms of olivine in the upper mantle.