Hot Forming Research Articles

An innovative strategy against oxide spallation of hot formed steels

Hot forming is a prominent technique to produce lightweight automotive steels. However, the generation of a weakly adhering oxide scale during hot forming and the subsequent post-processing of the scale pose a great threat to the shape precision of the product. Here, we propose a cost-effective solution to the spallation issue by incorporating minor silicate-molybdate additives into the rinse following pickling. The pre-deposited film serves as an effective barrier against high-temperature oxidation. Our innovative strategy enables the formation of an oxide scale that sticks to the substrate and paint layer, potentially eliminating the necessity for scale removal in industrial settings.

Towards microstructure control in forging and rolling: combining AI with process models for closed-loop property control

Abstract Metal forming processes like open-die forging or hot rolling are well-established for the production of key components in various industries. Nevertheless, the control of the final microstructure and hence mechanical properties is not yet common. To achieve this, the authors propose and discuss a control concept based on reinforcement learning, fast process models (FPM) and an “operator in the loop” approach. The concept is explained and tested using deviating initial ingot temperatures as idealized process disruptions. RL algorithms are trained for both processes and transferred into the controllers that are connected to a simulative environment based on FPM. Within this framework, the online adaption is possible in ∼2 s in rolling and 4–6 s in forging. This highlights the concepts suitability to be used for property control in hot metal forming.

Texture evolution induced by extrusion parameters and its effect on strengthening-toughening mechanisms of Al-Mg-Si-Cu-Mn alloys

In this study, extrusion experiments were carried out on Al-Mg-Si-Cu-Mn alloys with different extrusion ratios (ERs), extrusion temperatures (ETs), and extrusion speeds (ESs). By using electron backscatter diffraction (EBSD) analysis, tensile testing, and other analytical means, the evolution of microstructure, texture, and properties of the extruded alloys was systematically investigated, and the strengthening-toughening mechanism induced by the extrusion parameters was revealed. It was found that the strength of the extruded alloy shows a tendency to first increase and then decrease with the increase of the ER and ES, and the ‘critical ER' and ‘critical ES' are 29.5 and 2.5 mm/s, respectively; the strength of the extruded alloy gradually increases with the increase of the ET. The alloy achieved excellent strength-toughness matching at the ER of 29.5, ET of 480 °C, and ES of 2.5 mm/s. The yield strength (YS), ultimate tensile strength (UTS), and elongation (EL) of the extruded alloy at this condition were ∼169.58 MPa, ∼314.36 MPa, and ∼16.57 %, respectively. This excellent strength-toughness matching is mainly related to the following aspects: 1) grain refinement provides high grain boundary strengthening effect and appropriate work hardening ability; 2) <111>//ED texture has a strong preferential orientation; 3) the variation trend of dislocation density is importantly related to <111>//ED and EXa{011}<111> textures; 4) Cube{001}<100> and Goss{011}<100> textures have a softening effect. The above findings provide new insights into the potential mechanisms of hot extrusion forming of aluminum alloys, which are of important guiding for the design and development of aluminum alloys with excellent strength-toughness combinations.

Experimental and modeling study of the interfacial and convective heat transfer coefficients of 6061 aluminum alloy in hot gas forming

Experimental and modeling study of the interfacial and convective heat transfer coefficients of 6061 aluminum alloy in hot gas forming

A novel integrated hot forming with in-situ stress relaxation-aging for titanium alloy thin-walled components

The simultaneous achievement of high strength and precision in the fabrication of titanium alloy thin-walled components is a long-standing issue. This work proposes a novel integrated forming process, named Hot Forming with In-situ Stress Relaxation-Aging (short for HF-ISRA) to solve the special issue. In contrast to usual isothermal forming, the forming temperature in the proposed process is raised to the solution treatment temperature. Dies at a lower temperature realize in-situ stress relaxation-aging after hot forming. The role of the dies, in addition to forming, is also achieved post-forming heat treatment. This novel process comprises three main steps: solution heat treatment, rapid forming at solution temperature, and in-situ stress relaxation-aging. An experimental prototype of HF-ISRA was developed for V-bending test, in which a sheet blank was rapidly heated using electric current and the forming die was heated using heating rods. The process window of the proposed HF-ISRA was established based on the V-bending and uniaxial tensile tests of the TA15 titanium alloy. The results showed that compared with cold forming, the springback angle obtained using the optimized HF-ISRA decreased by 97.8 %, from 9°06′ to only 12′. The tensile strength at room temperature and 500 °C was improved by 4.4 % and 10.9 % compared with the as-received material, respectively. The relaxation mechanisms of αs were the precipitation, growth, and then globularization. The relaxation mechanism of αp was dislocation movements. The strength improvement in HF-ISRA was due to the formation of αs and dislocations strengthening. The stress-induced twinning in αs was also a contributor. The proposed novel process provides a new route for the fabrication of titanium alloy thin-walled components with high precision and strength.

Towards optimizing the microstructure of magnesium alloy during hot forming: Pre-deformation at cryogenic temperature

The preparation of massive twins by pre-deformation at cryogenic temperature (−196 °C) is expected to induce dynamic recrystallization (DRX) during hot forming, thereby optimizing the microstructure of hot-deformed alloys. In this study, Mg-5.5Gd-3Y-0.5Zr alloy was pre-deformed at room and cryogenic temperatures, respectively. Then, hot compression was carried out on the pre-deformed samples. The results indicate that the alloy fabricated by room-temperature pre-deformation (RT-PD) and then hot deformation (RT-HD) contains many initial grains which have not been refined, while the microstructure and mechanical properties of the alloy prepared through cryogenic-temperature pre-deformation (CT-PD) and then hot deformation (CT-HD) are improved significantly. There are only a few 101‾2 tension twins (TTWs) formed in RT-PD sample, so the sites for twin-induced dynamic recrystallization (TDRX) grains during subsequent hot deformation are limited. However, the number of twins in the alloy after CT-PD increases significantly, including 101‾1-101‾2 double twins (DTWs) and 101‾2-011‾2 twin-twin interactions, which facilitates the promotion of the TDRX and reduction of average grain size in the microstructure. In addition, a weak texture can be generated in CT-HD sample, primarily owing to the orientation inheritance of TDRX grains from various twins in CT-PD sample.

Activation mechanisms of slip systems during hot single point incremental forming of AA2024 sheet

Activation mechanisms of slip systems during hot single point incremental forming of AA2024 sheet

Flow Stress Models for 40Cr10Si2Mo Steel and Their Application in Numerical Simulation of Hot Forming

Flow Stress Models for 40Cr10Si2Mo Steel and Their Application in Numerical Simulation of Hot Forming

An Internal-State-Variable-Based Continuous Dynamic Recrystallization Model for Thermally Deformed TC18 Alloy.

Continuous dynamic recrystallization (CDRX) is widely acknowledged to occur during hot forming and plays a significant role in microstructure development in alloys with moderate to high stacking fault energy. In this work, the flow stress and CDRX behaviors of the TC18 alloy subjected to hot deformation across a wide range of processing conditions are studied. It is observed that deformation leads to the formation of new low-angle grain boundaries (LAGBs). Subgrains rotate by absorbing dislocations, resulting in an increase in LAGB misorientation and the transition of some LAGBs into high-angle grain boundaries (HAGBs). The HAGBs migrate within the material, assimilating the (sub)grain boundaries. Subsequently, an internal state variable (ISV)-based CDRX model is developed, incorporating parameters such as the dislocation density, adiabatic temperature rise, subgrain rotation, LAGB area, HAGB area, and LAGB misorientation angle distribution. The values of the correlation coefficient (R), relative average absolute error (RAAE), and root-mean-square error (RMSE) between the anticipated true stress and measured stress are 0.989, 6.69%, and 4.78 MPa, respectively. The predicted outcomes demonstrate good agreement with experimental findings. The evolving trends of the subgrain boundary area under various conditions are quantitatively analyzed by assessing the changes in dynamic recovery (DRV)-eliminated dislocations and misorientation angles. Moreover, the ISV-based model accurately predicts the decreases in grain and crystallite sizes with higher strain rates and lower temperatures. The projected outcomes also indicate a transition from a stable and coarse-grained microstructure to a continuously recrystallized substructure.

Critical state-of-the-art literature review of surface roughness in incremental sheet forming: A comparative analysis

Incremental sheet forming (ISF) is a controlled and die-less forming process that can produce customized products from the sheets layer by layer using the same setup, i.e., forming tools and machine. This novel and emerging forming technique can potentially be useful as a green aspect of manufacturing by reducing the required power and by saving the resources for producing the components of lightweight materials because material is deformed locally during ISF. The surface quality of the formed parts from sheet material affects the aesthetics aspects, stress concentration, fatigue life and their applicability. This review article aims to provide a state-of-the-art review for various aspects and parameters of ISF process that affect the surface roughness significantly by conducting literature survey quantitatively. Furthermore, the techniques of ISF and roles of various parameters responsible for affecting the surface quality of parts have also been explored for providing the critics for existing literature and setting the further guidelines for the researchers. Various instruments used for measuring the surface roughness of parts formed by ISF has also been discussed. Comparative analysis of exiting literature available in the context of various process parameters, ISF hardware, and surface roughness makes this study comprehensive and exhaustive for the researchers to find the gaps and challenges in this field. The relationship of wall angle with other process parameters can be explored in the future to obtain the desired surface quality of a particular material. Significant parameters responsible for the surface quality have also been discussed critically. Further, the new tool paths can be developed for high surface quality and low forming time. A study on the selection of feed rate for various applications and relation with other parameter is also recommended for the future work. The lubricants with additives can further be tested for high surface quality of ISF. Further, significant study on surface roughness is not conducted on hybrid sheet forming and other advanced variants of ISF (like hot forming, friction stir assisted incremental forming, waterjet forming). It is required to develop the comparisons between the different techniques of ISF. Results also showed that majority of researchers used SPIF technique followed by DSIF and hybrid ISF.

TFE Terpolymers: Once Promising - Are There Still Perspectives in the 21st Century: Synthesis, Characterization, and Properties-Part I.

Polytetrafluoroethylene (PTFE) exhibits outstanding properties such as high-temperature stability, low surface tension, and chemical resistance against most solvents, strong acids, and bases. However, these traits make it challenging to subject PTFE to standard polymer processing procedures, such as thermoforming and hot incremental forming. While polymer processing at temperatures above the melting point of PTFE is already demanding, the typically large molar mass of PTFE results in extremely high melt viscosities, complicating the processing of PTFE. Also, PTFE tends to decompose at temperatures close to its melting point. Therefore, fluoropolymers obtained by copolymerizing tetrafluoroethylene (TFE) with various co-monomers are studied as alternatives to PTFE (e.g., fluorinated ethylene-propylene (FEP)), combining its advantages with better processability. TFE terpolymers have emerged as desirable PTFE alternatives. This review provides an overview of the synthesis with various comonomers and microstructural analysis of PTFE terpolymers and the relationships between the microstructures of TFE terpolymers and their properties.

Dynamic recrystallisation: A quantitative study on grain boundary characteristics and dependence on temperature and strain rate in an aluminium alloy

Dynamic recrystallisation (DRX) usually occurs during hot forming of metallic materials, significantly impacting the mechanical properties of the final parts. Although DRX has been studied for decades, the types of DRX that occurs in high stacking fault energy (SFE) materials like aluminium alloys are still controversial, and their dependence on both temperature and strain rate is surprisingly missing. To fill these gaps, in the present study, uniaxial compression tests on an aluminium alloy AA6061 were carried out at different temperatures from 250 to 475 °C and strain rates from 0.01 to 1 s-1. The grain orientation and misorientation before and after the hot deformation were quantitively characterised using high-resolution Electron Backscatter Diffraction (EBSD) with a misorientation resolution of 0.05°, enabling high-angle grain boundaries (HAGBs), low-angle grain boundaries (LAGBs) and geometrically necessary dislocations (GNDs) to be accurately quantified and correlated against temperature and strain rate. Results reveal that both continuous dynamic recrystallisation (CDRX) and geometric dynamic recrystallisation (GDRX) occurred concurrently, resulting in the formation of discontinuous HAGBs and fine equiaxed grains, respectively. The misorientation angle distributions of the discontinuous HAGBs exhibit an opposite trend compared to those of the fine grains’ HAGBs. Both temperature and strain rate significantly affect the density of HAGBs formed by DRX, but have little effect on their misorientation angle distributions. This study sheds light on the fundamental understanding of DRX and provides comprehensive experimental data for future modelling of DRX processes in high SFE materials.

Continuous Dynamic Recrystallization and Deformation Behavior of an AA1050 Aluminum Alloy during High-Temperature Compression

Continuous dynamic recrystallization (CDRX) forms a new recrystallized microstructure through the progressive increase in low-angle boundary misorientations (LAGBs) during the hot forming of metallic materials with high stacking fault energy (SFE), such as aluminum alloys. The present work investigates the effect of deformation parameters on the evolution of the dynamic recrystallization microstructures of an AA1050 aluminum alloy during compression at elevated temperatures. The alloy microstructure is investigated at deformation temperatures and strain rates in the range of 300 °C to 500 °C and 0.001 to 0.8 s−1. A well-defined substructure and subsequent DRX grains provide indication that recrystallization can proceed with continued strain under high-temperature compression. At a strain rate of 0.1 s−1, the DRX fraction is observed to be 0.25 at a temperature of 300 °C. This fraction increases to 0.32 as the temperature rises to 400 °C. The recrystallization mechanism is identified by analyzing the flow stress, the evolution of the subgrain misorientation angle, and the distribution of recrystallized grains. The observations of discontinuous dynamic recrystallization (DDRX) and CDRX under various deformation parameters are discussed. Moreover, the main substructure evolution laws observed from the high-temperature compression of an AA1050 Al alloy are summarized.

Comparison and evaluation of different constitutive models for predicting the hot deformation behavior of Mg-Gd-Y-Zr alloy

The popular constitutive models used in the field of hot forming of magnesium alloys can be divided into phenomenological models, machine learning models, and internal state variables (ISV) models based on physical mechanisms. Currently, there is a lack of comparison and evaluation regarding the suitability of different types of models. In this study, Mg-Gd-Y-Zr alloy is taken as the research object. The hot deformation behavior of the alloy was studied systematically. Subsequently, Arrhenius model with strain compensation, artificial neural network (ANN) model, and ISV model involving dynamic recrystallization (DRX), dislocation density and grain size evolution were established. ANN model demonstrates a higher level of accuracy in fitting the original stress-strain curves compared to both ISV model and modified Arrhenius model, but ANN model is not suitable for predicting the experimental results outside of the initial database. ISV model considers the impact of microstructure evolution history on stress, making it highly effective in reflecting the mechanical responses under complex loading condition. The established ISV model is embedded in the ABAQUS software, which shows good ability in calculating the mechanical response, dimension, and microstructure evolution information of the component during hot forming.

Process window and mechanical properties for thin magnesium- and zinc-wires in dieless wire drawing

Due to their biodegradable properties, magnesium- and zinc-based alloys are in the focus of interest for numerous medical applications, e.g. in the form of thin wires. To achieve improved processability by using hot forming and to obtain higher diameter reductions per pass, the dieless wire drawing process is presented in this paper. In order to investigate the processability and the resulting mechanical properties, a selection of magnesium- and zinc-alloys as well as process parameters are chosen, and wire manufacturing is carried out using the dieless drawing process. The resulting process windows and mechanical properties for the selected materials are discussed. It is found that the length of the forming zone is an important indicator for the process window and the cross-sectional area reduction accuracy in the dieless wire drawing process. Furthermore, process parameter variations result in a distinct variation of the mechanical properties of the wires, whereas process temperatures close to the wire extrusion temperature result in mechanical properties similar to the as-extruded wires. Good localization of the deformation is found for forming zones of 25–75 mm length at elevated temperatures and cross-sectional area reductions of up to 30% are possible for Z1 and ZX10 in one drawing step.Graphical

Study on microstructure evolution mechanism and inhomogeneous characteristic of 2219 aluminum alloy in hot flow forming

In order to reveal the evolution mechanism of the deformation microstructure of 2219 aluminum alloy tube under compression-shear stress, in this paper, flow forming tests and their numerical simulations were carried out, respectively, at temperatures from 250 °C to 400 °C. Meanwhile, a midrange layer index was proposed to analyze the gradient of deformation microstructure. The results show that multiple recrystallization mechanisms of the 2219 aluminum alloy are presented simultaneously during hot flow forming. The shear stress during forming is the main factor that generated the microstructure gradient along the thickness direction, and the recrystallization level is higher with higher shear strain. In addition, it is beneficial to improve microstructure homogeneity and mechanical properties by increasing thickness reduction or decreasing the temperature. This study provides guidance for microstructure control of the 2219 aluminum alloy tube flow forming process.

Formation of near core-shell-like structure and dual-phase nanoprecipitation behavior in Nb–Si–Ti based alloys

Dual-phase metal materials can usually take into account the advantages of both phases, but the heterogeneity of dual-phase properties will cause flow instability. Therefore, it is difficult to further improve the microstructure and properties of Nb–Si–Ti based alloys containing ductile Nbss and hard silicides through hot working. Here, we propose a method for interface modification by precipitating an intermediate phase and forming a core-shell-like structure with silicides. A novel near core-shell structure (β-Nb5Si3/Nb4FeSi) is obtained in Nb–Si–Ti based alloy by deep cryogenic quenching and annealing. The precipitation of Nb4FeSi is closely related to stacking faults, where high-density stacking faults can develop into the nanotwins during annealing at 1200 °C. In addition, two types of nanoprecipitation behaviors are observed in the Nbss and β-Nb5Si3. The nanoscale plate-like δ-Nb11Si4 is precipitated along the [100]Nbss and [010]Nbss in the Nbss matrix, while the precipitation of granular Nb4FeSi from β-Nb5Si3 satisfies (1‾10)β//(01‾0)Nb4FeSi. In addition to the twinning induced plasticity of Nb4FeSi (shell), a phase transformation from β-Nb5Si3 to α-Nb5Si3 and Nbss that occurs within the core-shell structure is beneficial for the hot forming of the alloy.

A VFM-based identification method for anisotropic thermal-mechanical properties of sheet metals using the digital image correlation and infrared thermography assisted heterogeneous test

The accurate characterization of the anisotropic thermal-mechanical constitutive properties of structural sheet metals at elevated temperatures and under nonuniform stress/strain states is crucial for the precise hot plastic forming and structural behavior evaluation of an engineering sheet part. Traditional thermal-mechanical testing methods rely on the assumption of states homogeneity, leading to a large number of tests required for the characterization of material anisotropy and nonlinearity at various high temperatures. In this work, a highly efficient identification method is proposed that allows the simultaneous characterization of the anisotropic yielding, strain hardening and elasto-plasticity thermal softening material properties using the minimum number of tests, releasing the limitations of traditional identification methods. This is implemented by performing a digital image correlation and infrared thermography assisted heterogeneous high temperature test and processing the full-field measurement data based on the principle of virtual work. A double-notched tensile specimen configuration combined with a center-to-periphery temperature gradient is designed first to enable the high heterogeneity of stress/temperature states. Simulations of the heterogeneous tests are then performed to supply idealized reference data that can be used to evaluate the identification sensitivity of the proposed identification algorithm. After the numerical validation of the methodology, it is then applied to the TC4 titanium alloy sheet specimen using the self-developed experimental setup. The experimental identification results verify that the multiple anisotropic thermal-mechanical elasto-plasticity constitutive parameters can be accurately identified from the heterogeneous test with high computation efficiency, significantly simplifying the testing process in comparison to applying multiple traditional homogeneous tests. The current work provides an effective and convenient alternative to high temperature identification strategies used by the material processing community.

An Experimental Study on the Frictional Behavior of Ultrathin Metal Sheets at Elevated Temperatures.

Hot forming is an effective approach for improving the formability of ultrathin metal sheets, such as those made of stainless steel and pure titanium. However, the increased friction coefficient between the tool and the high-temperature metal sheet negatively affects material flow during hot forming, potentially resulting in severe local thinning or even cracking. This study explores the frictional behavior of 0.1 mm thick ferritic stainless steel (FSS) and commercially pure titanium (CP-Ti) sheets at elevated temperatures. A friction testing apparatus was developed to measure the friction coefficients of these metal sheets from room temperature (25 °C) up to 600 °C. The friction coefficient of the FSS sheet increased monotonically with temperature, whereas that of the CP-Ti sheet first increased and then decreased. Post-friction testing microscopic examination demonstrated that built-up edges formed on the surfaces of the friction blocks when rubbed against the stainless steel, contributing to the higher friction coefficients. This study provides a foundation for understanding frictional behavior during the hot forming of ultrathin metal sheets.

Evolution and formation mechanism of residual stress in Al-Cu alloy rings during ring rolling and quenching

The large-scale ring components, as thin-walled structures, are prone to unpredictable machining deformation due to the initial residual stresses introduced by rolling and quenching, which seriously affect the dimensional accuracy and service life of the ring components. Therefore, the relief and homogenization of residual stress inside large-scale ring components is crucial. However, the existing studies rarely involve the essential causes and the evolution laws of residual stresses during the manufacturing of ring components, which are indispensable for understanding the failure mechanisms of components caused by residual stresses and specifying relevant protective measures. Therefore, the evolution and distribution laws of stress-microstructure-property non-uniformity during the hot forming (ring rolling) and heat treatment (quenching) of 2219 Al-Cu alloy rings were precisely and deeply explored using scaled experiments in this paper. The relationship between non-uniform deformation and residual stresses was analyzed, and the basic equation that residual stresses must satisfy was established. Furthermore, the concept of the “non-coordination coefficient” was proposed, revealing the physical mechanism of residual stresses induced by non-uniform deformation. In addition, the influencing factors and formation mechanisms of residual stresses in the rolled and quenched state of rings were studied, and the essential reasons for the differences in residual stresses between the rolling and quenching processes were obtained. The experimental results indicate that the circumferential and axial residual stresses increased from 1.48 and 0.51 MPa to −142.68 and −122.31 MPa, respectively. The standard deviation changed from 13.47 and 33.52 MPa to 63.42 and 61.61 MPa, respectively. The maximum range of tensile strength, yield strength and elongation rates of the rolling and quenched state is 12.82 and 20.16 MPa, 17.49 and 22.14 MPa, and 8.62 % and 7.56 %, respectively. All fractures are microporous aggregation ductile, including dimple transgranular fracture and intergranular fracture. The quenched state exhibits a significantly larger grain size compared to the rolled state. The appearance of residual stress is essentially to force the inconsistent deformation of various parts inside the object to maintain its integrity and continuity, which leads to a local mismatch of micro-elements inside the ring and further induces non-uniform strain and stress. The difference in the severity of “penetrability” induced by different temperature gradients determines the difference in residual stress between rolled and quenched rings, larger rings have higher and more non-uniform residual stress than smaller rings under the same process conditions. The above results deepen the theoretical understanding of residual stress formation mechanisms and lay a theoretical foundation for the comprehensive evaluation of performance degradation and service failure analysis of large ring components.