In this paper, a method for measuring properties of ceramic materials with relative dielectric constant value of 20-150 is proposed. It permits us to eliminate the operating TM/sub 01/spl delta//-mode degeneration due to its frequency coincidence with other modes, including ones of higher order. Both that fact and the possibility of precise calculation of an unloaded quality factor for a cavity permit one to execute the accurate measurements of loss tangent values as low as (1/spl divide/0, 5)/spl times/10/sup -4/, the error of dielectric constant measurement being equal to or less than 1%. The feasibility of precise measurement of the loaded Q-factor of a cavity by the readings of micrometric probe makes the use of frequency meters unnecessary.